Agilent Technologies 1100 Series Manual de usuario

Agilent 1100 Series

Binary Pump

Reference Manual

Agilent G1312A Bin Pump

Asset # 304023

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Germany

Copyright Agilent

Technologies 1999

Reproduction, adaption,

or translation without

prior written permission

is prohibited, except as

allowed under the

Part No. G1312-90003

Edition 01/00

Printed in Germany

Warranty

The information

contained in this

document is subject to

change without notice.

Agilent Technologies

makes no warranty of

any kind with regard to

this material,

including, but not

limited to, the implied

warranties or

merchantability and

fitness for a particular

purpose.

Agilent Technologies

shall not be liable for

errors contained herein

or for incidental or

consequential damages

in connection with the

furnishing, performance,

or use of this material.

WARNING

For details of safety,

see Safety Information

on page 270.

Warning Symbols Used

In This Book

The apparatus is marked

with this symbol when

the user should refer to

the instruction manual

in order to protect the

apparatus against

damage.

Reference Manual

Agilent 1100 Series Binary Pump

In This Book

This manual contains technical reference information about the Agilent 1100 Series

binary pump. The manual describes the following:

• installation,

• optimizing performance,

• troubleshooting,

• repairing,

• parts and materials,

• introduction and theory of operation,

• screens of local control module and

• specifications.

Contents

1 Installing the Pump

How to install the binary pump 13

Site Requirements 14

Unpacking the Binary Pump 17

Optimizing the Stack Configuration 19

Installing the Binary Pump 21

Flow Connections of the Binary Pump with Solvent Selection

Valve 24

Flow Connections of the Binary Pump without Solvent Selection

Valve 27

Priming and Purging the System 30

2 Optimizing Performance

How to optimize the binary pump to achieve best chromato-

graphic results 33

Hints for Successful Use of the Binary Pump 34

Solvent Information 36

Prevent Blocking of Solvent Filters 37

When to Use a Vacuum Degasser 39

When to Use the Continuous Seal Wash Option 40

When to Use Alternative Seals 41

When to Remove the Static Mixer 42

How to Optimize the Compressibility Compensation Setting 43

3 Troubleshooting and Test Functions

The binary pump’s built-in troubleshooting and test

Contents

functions 45

Status Indicators 48

Power Supply Indicator 49

Instrument Status Indicator 49

Error Messages 50

Timeout 51

Shutdown 52

Remote Timeout 53

Synchronization Lost 54

Leak 55

Leak Sensor Open 56

Leak Sensor Short 57

Compensation Sensor Open 58

Compensation Sensor Short 59

Fan Failed 60

Open Cover 61

Restart Without Cover 62

Zero Solvent Counter 63

Pressure Above Upper Limit 64

Pressure Below Lower Limit 65

Pressure Signal Missing 66

Valve Failed 67

Missing Pressure Reading 68

Pump Configuration 69

Valve Fuse 70

Inlet-Valve Fuse 71

Temperature Out of Range 72

Temperature Limit Exceeded 73

Motor-Drive Power 74

Contents

Encoder Missing 75

Inlet-Valve Missing 76

Servo Restart Failed 77

Pump Head Missing 78

Index Limit 79

Index Adjustment 80

Index Missing 81

Stroke Length 82

Initialization Failed 83

Wait Timeout 84

Pressure Test 85

Running the Pressure Test 87

Evaluating the Results 89

Leak Test 91

Description 92

Running the Leak Test 94

Evaluating the Results 96

4 Repairing the Pump

Instructions on simple, routine repair procedures as well as

more extensive repairs requiring exchange of internal

parts 103

Cleaning the Binary Pump 105

Using the ESD Strap 106

Overview 107

Contents

Simple Repair Procedures 108

Exchanging the Active Inlet Valve Cartridge or the Active Inlet

Valve 109

Exchanging the Outlet Ball Valve Sieve or the Complete

Valve 112

Exchanging the Purge Valve Frit or the Purge Valve 114

Exchanging the Solvent Selection Valve 117

Removing and Disassembling the Pump Head Assembly 119

Exchanging the Pump Seals and Seal Wear-in Procedure 121

Exchanging the Plungers 124

Installing the Continuous Seal Wash Option 125

Exchanging the Wash Seals 127

Reassembling the Pump Head Assembly 129

Exchanging the Optional Interface Board 131

Exchanging Internal Parts 132

Removing the Top Cover and Foam 133

Exchanging the High Pressure Pump Main Board (HPM

Board) 136

Exchanging the Damper 143

Exchanging the Fan 145

Exchanging a Pump Drive 148

Exchanging the Power Supply 151

Exchanging the Leak Sensor 156

Exchanging Status Light Pipe 158

Assembling the Main Cover 159

Replacing the Top Cover and Foam 160

Contents

5 Parts and Materials

Detailed illustrations and lists for identification of parts and

materials 163

Control Module(B-Version) 167

Solvent Cabinet 168

Bottle-Head Assembly 169

Hydraulic Path with Solvent Selection Valve 170

Hydraulic Path without Solvent Selection Valve 172

Cover Parts 174

Sheet Metal Kit 175

Foam Parts 176

Power and Status Light Pipes 177

Leak Parts 178

Pump-Head Assembly 179

Pump-Head Assembly with Seal Wash 181

Outlet Ball Valve Assembly 183

Purge-Valve Assembly 184

Active Inlet Valve Assembly 185

Accessory Kit G1311-68705 186

Seal Wash Option 01018-68722 187

Cable Overview 188

Analog Cables 190

Remote Cables 192

BCD Cables 197

Auxiliary Cable 199

CAN Cable 199

External Contact Cable 200

RS-232 Cable Kit 201

LAN Cables 202

Contents

6 Introduction to the Binary Pump

An introduction to the pump, instrument overview, theory of

operation, external communication and internal

connectors 203

Introduction to the Binary Pump 204

Electrical Connections 210

Instrument Layout 212

Early Maintenance Feedback (EMF) 213

The Electronics 215

Firmware Description 221

Optional Interface Boards 223

Agilent 1100 Series Interfaces 225

Setting the 8-bit Configuration Switch 230

The Main Power Supply Assembly 235

7 Control Module Screens for the Binary Pump

Screens available from the Analysis screen 239

Screens available from the System screen 248

Screens available from the Records screen 250

Diagnostics and Tests 256

8 Specifications

Performance specifications of the binary pump 259

Performance Specifications 260

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