Agilent Technologies Cary 3500 Manual de usuario

Agilent Cary 3500 UV-Vis Spectrophotometer

User’s Guide

2 Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide

Notices

Manual Part Number

5994-0319EN

Edition 2, December 2018

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

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by United States and international

Agilent Technologies Australia [M] Pty

Ltd

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www.agilent.com

Instrument Manufacturing

Manufactured by Agilent Technologies

Bayan Lepas Free Industrial Zone,

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Warranty

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document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to the

maximum extent permitted by

applicable law, Agilent disclaims all

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with regard to this manual and any

information contained herein, including

but not limited to the implied

warranties of merchantability and

fitness for a particular purpose. Agilent

shall not be liable for errors or for

incidental or consequential damages in

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Safety Notices

A CAUTION notice denotes a hazard. It

calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a hazard. It

calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in personal injury or death.

Do not proceed beyond a WARNING

notice until the indicated conditions are

fully understood and met.

WARNING

CAUTION

Contents

Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide 3

Contents

1General Information and Safety Practices and Hazards 5

User Documentation 5

Conventions 6

Notes and Tips 6

Verifying Safe State 6

Lamp Module 7

Modules, Covers and Panels 7

Compressed gas cylinders 7

Other Precautions 8

Warning and Other Symbols 8

CE Compliance 10

Electromagnetic Compatibility 10

EN55011/CISPR11 10

ICES/NMB-001 11

2Specifications 13

Site Preparation Checklist 13

Measurement category 13

Pollution degree 13

Environmental conditions 14

Weights and dimensions 14

Electrical specifications 15

Mains Supply 15

Computer requirements 16

Contents

4 Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide

Gas requirements 16

3Installation 17

4Introduction 19

Modular concept 19

Modules 19

Cary Multicell Ambient and Peltier 20

Compact Ambient and Peltier 20

Configurations 21

Temperature probes 21

Instrument overview 21

Front and right side of the module and engine 22

Back of the engine 22

Front of the engine 22

Back of the module 23

Indicator LED 23

Using the software 23

Compressed gas purging 24

Purge kit 24

Drain outlet 25

5Troubleshooting, Maintenance and Spare Parts 27

Fuses 27

Spills 28

Spare Parts 28

General Information and Safety Practices and Hazards

Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide 5

1General Information and Safety Practices

and Hazards

User Documentation 5

Verifying Safe State 6

Lamp Module 7

Modules, Covers and Panels 7

Compressed gas cylinders 7

Other Precautions 8

Warning and Other Symbols 8

CE Compliance 10

Electromagnetic Compatibility 10

Your Agilent instrument and accessories have been carefully designed so that

when used properly you have an accurate, fast, flexible and safe analytical system.

Information about safety practices appears throughout the documentation (both

hard copy and online) provided with your instrument and accessories to help you

safely operate the instrument and accessories. Before using the instrument or

accessories, you must thoroughly read these safety practices. ALWAYS operate

the instrument and accessories in accordance with these safety practices.

User Documentation

You have been provided with the following additional documentation to help you

set up and operate your Agilent Cary 3500 UV-Vis spectrophotometer:

Cary UV software installation instruction sheet found in the software box

Cary 3500 UV-Vis module instruction sheet found in the module box

Cary 3500 UV-Vis engine instruction sheet found in the engine box

General Information and Safety Practices and Hazards

6 Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide

This manual, with safety practices and hazards information, instructions for

installing and maintaining the components of the Cary 3500 UV-Vis and

troubleshooting information.

The Cary UV Workstation Help and Learning Center provided with the Cary UV

Workstation software which provide step-by-step instructions for installing

selected accessories and programming applications, step-by-step instructions

for frequently performed analyses and instructions for using any accessories

you ordered.

Conventions

The following conventions have been used throughout the documentation:

Menus, menu items, buttons and check boxes have been typed in bold. For

example, ‘click OK’ and ‘From the Edit menu, choose Copy’.

ALL CAPITALS indicate keyboard commands. For example, ‘Press ENTER’ and

‘Press SHIFT+F3’.

Notes and Tips

A Note is used to give advice or information.

A Tip is used to give practical hints to help you achieve the best possible

performance from your instrument.

Verifying Safe State

The following general safety precautions must be observed during all phases of

operation, maintenance and service of this instrument.

To ensure continued safety of the instrument after maintenance or service

procedures verify the instrument is returned to a safe state for the user. This

includes running performance checks to verify the instruments safety systems are

functioning correctly. Check the general condition of the instrument during

operation for wear or signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings elsewhere in

this manual violates safety standards of design, manufacture, and intended use of

the instrument. Agilent Technologies assumes no liability for the customer’s

failure to comply with these requirements.

General Information and Safety Practices and Hazards

Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide 7

Lamp Module

The lamp is enclosed in a self-contained module. This module contains

components operating at high voltages. To avoid electric shock, NEVER

disassemble the module.

Modules, Covers and Panels

The only routinely accessed panel is the Cary UV spectrophotometer sample

compartment to introduce samples.

The only other cover and panel that is customer accessible is the lamp module

and is to be removed ONLY when changing the lamp module. Consult the Cary UV

Help and Learning Center for instructions and safety information.

Any other panels or covers that are retained by screws on the spectrophotometer

and accessories may be opened ONLY by Agilent service engineers.

Compressed gas cylinders

Compressed gas cylinders contain highly pressurized gas. If storage conditions

are outside of the recommended supplier’s safety codes, the cylinders can explode

or rapidly release gas into the environment. This may result in injury or death.

Store and handle compressed gases carefully and in strict adherence to safety

codes.

Secure cylinders to an immovable structure or wall.

Store and move cylinders in an upright, vertical position. Before transport,

remove regulators and install cylinder cap.

Store cylinders in a well-ventilated area away from heat, direct sunshine,

freezing temperatures, and ignition sources.

Clearly mark cylinders so there is no doubt as to their contents.

Use only approved regulators and connections.

Use only connector tubing that is chromatographically clean and has a

pressure rating significantly greater than the highest outlet pressure from the

regulator.

General Information and Safety Practices and Hazards

8 Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide

Other Precautions

Use of the Cary UV-Vis system and accessories may involve materials, solvents

and solutions that are flammable, corrosive, toxic or otherwise hazardous.

Careless, improper, or unskilled use of such materials, solvents and solutions can

create explosion hazards, fire hazards, toxicity and other hazards which can result

in death, serious personal injury, and damage to equipment and property.

ALWAYS ensure that laboratory safety practices governing the use, handling and

disposal of such materials are strictly observed. These safety practices should

include the wearing of appropriate safety clothing and safety glasses.

Warning and Other Symbols

The following is a list of symbols that appear in conjunction with warnings on the

spectrophotometer. The hazard they describe is also shown.

A triangular symbol indicates a warning. The meanings of the symbols that may

appear alongside warnings in the documentation or on the instrument itself are as

follows.

Disconnect power

Electrical shock

Heavy weight

(danger to feet)

Heavy weight

(danger to hands)

Hot surface

General Information and Safety Practices and Hazards

Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide 9

The following symbol may be used on warning labels attached to the instrument.

When you see this symbol, refer to the relevant operation or service manual for the

correct procedure referred to by that warning label.

The following symbols appear on the instrument or accessories:

Mains power on

Mains power off

Fuse

Single phase alternating current

Protective earth ground terminal

Earth ground terminal

Frame or chassis ground terminal

Nitrogen purge input at the specified flow rate

Caution, disconnect all supplies, risk of electric shock

General Information and Safety Practices and Hazards

10 Agilent Cary 3500 UV-Vis Spectrophotometer User’s Guide

CE Compliance

Your Agilent Cary UV spectrophotometer has been designed to comply with the

requirements of the Electromagnetic Compatibility (EMC) Directive and the Low

Voltage (electrical safety) Directive (commonly referred to as the LVD) of the

European Union. Agilent has confirmed that each product complies with the

relevant Directives by testing a prototype against the prescribed EN (European

Norm) standards.

Proof that a product complies with these directives is indicated by:

the CE Marking appearing on the rear of the product, and

the documentation package that accompanies the product containing a copy

of the Declaration of Conformity. The Declaration of Conformity is the legal

declaration by Agilent that the product complies with the directives listed

above, and shows the EN standards to which the product was tested to

demonstrate compliance.

Electromagnetic Compatibility

EN55011/CISPR11

Group 1 ISM equipment: group 1 contains all Industrial, Scientific and Medical

(ISM) equipment in which there is intentionally generated and/or used

conductively coupled radio- frequency energy which is necessary for the internal

functioning of the equipment itself.

Class A equipment is equipment suitable for use in all establishments other than

domestic and those directly connected to a low voltage power supply network

which supplies buildings used for domestic purposes.

This device complies with the requirements of CISPR11, Group 1, Class A as

radiation professional equipment. Therefore, there may be potential difficulties in

ensuring electromagnetic compatibility in other environments, due to conducted

as well as radiated disturbances.

Operation is subject to the following two conditions:

1This device may not cause harmful interference.

2This device must accept any interference received, including interference that

may cause undesired operation.

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