Agilent Technologies 1220 Infinity II LC Series Manual de usuario

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

User Manual

SIM Sample Cooler

for Agilent 1220 Infinity II LC System

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

2 User Manual SIM Sample Cooler_06/2018

Document History

Edition 06/2018

The information contained in this document is subject to change without notice.

SIM GmbH makes no warranty of any kind with regard to this material, including, but not

limited to, the implied warranties of merchantability and fitness for a particular purpose.

SIM GmbH shall not be liable for errors contained herein or for incidental or consequential

damages in connection with the furnishing, performance or use of this material.

Reproduction, adaptation, or translation without prior written permission is prohibited, except

as allowed under the copyright laws.

NOTE

Read this instruction carefully prior to installation and/or use. Pay attention particularly to all

advises and safety instructions to prevent injuries. SIM GmbH shall not be liable for

misusing the product or unreliable function due to unauthorized modifications.

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

User Manual SIM Sample Cooler_06/2018 3

CONTENT

1. SAFETY INSTRUCTIONS 4

1.1. Warnings 4

1.2. Meaning of the signal words 5

1.3. General Safety Instructions/ Informations générales de sécurité 5

2. SCOPE OF DELIVERY 8

2.1. LC 1220 90 40/ LC 1220 90 60/ LC 1220 94 60 8

2.2. OPT021 Driver for OpenLAB CDS ChemStation 8

2.3. OPT022 Driver for OpenLAB CDS EZChrom 8

2.4. OPT023 Standalone-Software 8

2.5. OPT024 Driver for OpenLAB CDS 2.x 9

3. SITE REQUIREMENTS 9

4. MODE OF OPERATION 10

5. INITIAL OPERATION 11

5.1. Connections 11

5.2. Software Installation 12

5.3. Set-Up and configuration for OpenLAB ChemStation/ EZChrom (OPT021/022/024) 12

5.3.1. Software settings for OPT021/022/024 (OpenLAB CDS ChemStation/EZChrom/2.x) 19

5.3.2. Installation of the Standalone Software (OPT023) 20

5.3.3. Software settings for OPT023 (Standalone Software) 22

6. START OF THE SYSTEM 24

6.1. Start of the cooling module 24

6.2. Installation of the Sample Tray 24

6.3. Water level check 24

6.4. Setting of Parameters for the Sample Tray Cooling 24

7. MAINTENANCE 25

7.1. Cleaning the module 26

7.2. Water level 26

8. TROUBLESHOOTING 28

9. TECHNICAL DATA 29

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

4 User Manual SIM Sample Cooler_06/2018

1. SAFETY INSTRUCTIONS

NOTE

The cooling module for the Agilent 1220 Infinity II LC system has to be mounted, started-up

and serviced by fully trained and qualified personnel only, taking into consideration the

generally recognized standard rules of technology.

It has to be ensured that employees or third persons are not exposed to any danger.

All safety instructions and warnings in this manual, particularly those concerning installation,

start-up, and maintenance must be strictly observed.

(1) Unpack the module and ensure that all parts and materials listed on the attached packing

list have been delivered. In case of transport damage please inform the transport

company immediately.

(2) Check all relevant safety regulations and technical indications for the specific installation

place with reference to the “User Manual of the Agilent 1220 Infinity II LC System”

(G4280-90016).

(3) Prevent errors and protect persons against injuries and the device against damage.

(4) Make sure that the ventilation slots of the module are not covered and sufficient

ventilation is provided (additional 10 cm (3.9 in) space to the side and in the rear).

(5) Periodically remove dust from the ventilation slots to prevent overheating of the system.

1.1. Warnings

The warnings in this manual are highlighted with pictograms and signal words:

Les avertissements de ce manual sont mis en evidence par des pictogrammes et des mots

de signalisation:

The pictogram and the signal word indicate the level of danger.

Le pictogramme et le mot de signalisation indiquent le niveau de danger.

The warnings that precede each action are depicted as follows:

Les avertissements qui précèdent chaque action sont représentés comme suit:

DANGER/WARNING

DANGER/ AVERTISSEMENT

Type and source of danger

Type et source de danger

Explanation of the type and source of danger

Explication du type et de la source du danger.

Measures to avert the danger

Mesures pour éviter le danger

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

User Manual SIM Sample Cooler_06/2018 5

1.2. Meaning of the signal words

Signal word/ Mot

de signalisation

Meaning/ Signification

DANGER/

DANGER

Direct danger to life or risk of severe physical injury if this danger

is not avoided.

Danger direct pour la vie ou risque de blessures corporelles

graves si ce danger n’est pas évité.

WARNING/

AVERTISSEMENT

Possible risk of severe physical injury if this danger is not avoided.

Risque possible de blessures corporelles graves si ce danger

n’est pas évité.

CAUTION/

ATTENTION

Possible risk of minor physical injury if this danger is not avoided.

Risque possible de blessures corporelles mineures si ce danger

n’est pas évité.

NOTE/

CONSEILS

Damage to property if this danger is not avoided.

Dommages matériels si ce danger n’est pas évité.

1.3. General Safety Instructions/ Informations générales de sécurité

The following safety instructions are essential and have to be observed in all operating

modes including maintenance and repair work of the module.

Failure to observe the precautions and warnings in the manual result in the violation of

development production and intended use. SIM GmbH shall not be liable for misusing the

product or unreliable function due to unauthorized modifications.

Les consignes générales de sécurité suivantes doivent être respectées lors de toutes les

phases de fonctionnement, d'entretien et de réparation de cet instrument.

Le non-respect de ces consignes ou des avertissements spécifiques énoncés ailleurs dans

ce manuel, est en violation des normes de sécurité applicable à la conception, à la

fabrication et à l'usage prévu de l'instrument. SIM GmbH ne peut être tenu responsable du

non-respect de ces exigences par le client.

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

6 User Manual SIM Sample Cooler_06/2018

DANGER/ DANGER

Dangerous Voltage! Tension électrique dangereuse!

If the covers are attached correctly, no contact with dangerous tension

is possible. Never remove the cover!

Lorsque les capots sont fixés correctement, n’y a pas de contact avec

tension dangereuse est possible.N'ouvrez jamais le capot de

l’instrument!

It is not allowed to insert objects into the housing.

Ne jamais introduire d'objets non prévus à cet effet dans les

ouvertures du boîtier

Module is partially energized when switched off, as long as power cord

is plugged in.

L'alimentation continue à utiliser un peu d'électricité, même si

l'interrupteur du panneau avant est en position d'arrêt (OFF).



Repair work at the module can lead to personal injuries, e.g. shock

hazard, when the module cover is opened and the instrument is

connected to power.

Les travaux de réparation sur le module peuvent entraîner des

blessures, par ex. des électrocutions, lorsque le capot du module est

ouvert et que l'instrument est branché au secteur.



Provide sufficient space next to the power socket of the instrument

to allow the cable to be unplugged.

Prévoyez un espace suffisamment important à proximité de la prise

d'alimentation pour que le câble puisse être débranché.



Unplug the power cord before opening the module.

Débranchez le câble d’alimentation de l’instrument avant d’ouvrir le

capot de l’instrument.

WARNING/ AVERTISSEMENT

Sharp Metal Edges! Arêtes métalliques tranchantes!

Sharp-edged parts of the equipment may cause injuries.

Les composants de l'instrument dotées d'arêtes tranchantes peuvent

occasionner des blessures.



In order to prevent personal injury, be careful when getting in

contact with sharp metal areas.

Afin d'éviter de vous blesser, prenez garde aux arêtes métalliques

tranchantes.

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

User Manual SIM Sample Cooler_06/2018 7

CAUTION/ ATTENTION

Personal Injury! Blessures corporelles!

To prevent personal injury, do not grip into the needle area of the

autosampler.

Pour éviter tout risque de blessure, n'approchez pas vos doigts de

l'aiguille pendant le fonctionnement de l'échantillonneur.



Do not try to put in or remove a sample vial into the gripper when

the gripper is underneath the needle!

Ne pas essayer d’introduire ou de retirer un flacon d’échantillon dans

la pince lorsque la pince se trouve sous l’aiguille!

CAUTION/ ATTENTION

Liquids at/ in the module!/ Liquides dans ce module!

Liquids at/in the module will damage the system electronics.

Les liquids présents dans le module endommageront l’électronique du

système.



Make sure that no liquid enters the module because this can result

in electrical shock and the destruction of the device.

La présence d'un liquide dans le module peut provoquer des

décharges électriques et endommager l'échantillonneur automatique.



In case of emergency, immediately disconnect the power plug of

the module and have it inspected by a specialist before you use it

again.

En cas d'urgence débranchez immédiatement le cordon secteur et

faites contrôler l'appareil par un technicien qualifié avant de l'utiliser à

nouveau.

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

8 User Manual SIM Sample Cooler_06/2018

2. SCOPE OF DELIVERY

2.1. LC 1220 90 40/ LC 1220 90 60/ LC 1220 94 60

cooling module (1) mounted at an 1220 Infinity II LC side wall, with power cable (not

shown)

modified tray-support with preassembled cooling plate and cooling hoses as well as

electrical connections (2)

edge protection and fixing screw (3)

syringe with threaded connection (4) for refilling the coolant

manual (not shown)

2.2. OPT021 Driver for OpenLABCDS ChemStation

software (LC 1220 10 21)

2 LAN cables (0.2 and 2m , LC 1220 10 75)

2.3. OPT022 Driver for OpenLAB CDS EZChrom

software (LC 1220 10 22)

2 LAN cables (0.2 and 2m , LC 1220 10 75)

2.4. OPT023 Standalone-Software

software (LC 1220 10 23)

2 LAN cables (0.2 and 2m, LC 1220 10 75)

1 APG remote cable

Fig. 1 Scope of delivery

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

User Manual SIM Sample Cooler_06/2018 9

2.5. OPT024 Driver for OpenLAB CDS 2.x

Software (LC 1220 10 24)

2 LAN cables (0.25 m and 2.0 m, LC 1220 10 75)

3. SITE REQUIREMENTS

DANGER/ DANGER

Absence of ground connection or use of unspecified power cord!

Absence de raccordement à la terre et utilisation d'un câble d'alimentation

non adapté!

The absence of ground connection or the use of an unspecified power cord

can lead to electric shock or short circuit.

L'absence de mise à la terre ou l'utilisation d'un câble d'alimentation non

recommandé peuvent entraîner des chocs électriques ou des courts-

circuits.

Never connect the device to a voltage source without ground

connection.

N'utilisez jamais votre instrument avec une prise de courant sans mise à la

terre.

Never use cables other than the ones supplied by SIM and Agilent

Technologies to ensure proper functionality and compliance with safety or

EMS regulations.

N'utilisez jamais de câble d'alimentation autre que le modèle SIM et Agilent

Technologies destiné à votre pays.

NOTE

In case of emergency it must be possible to disconnect the instrument from the power line

any time.

Make sure that there is easy access to the power cable of the instrument so that the

instrument can quickly and easily be disconnected from the line voltage.

Power considerations

Power supply:

The power supply has wide ranging capabilities so that there is no voltage selector at the

instrument. The fuse (T 3.15 A / 250 VAC) is accessible from the outside.

Power cord:

Different power cords are offered as options with the system. The female ends of all power

cords are identical. The female end plugs into the power-input socket at the rear of the

cooling module. The male end of each power cord is different and designed to match the wall

socket of a particular country or region.

Scientific Instruments Manufacturer GmbH

D-Oberhausen ●+49(0)208/ 94 10 78-0 ●www.sim-gmbh.de

10 User Manual SIM Sample Cooler_06/2018

Bench space

If using the cooling module together with the Agilent 1220 Infinity II LC System, the LC

system needs an additional 15 cm of space on the left side (view from the front).

Moreover, the module needs approximately 10 cm (3.9 in) at the rear and the left side for air

circulation.

Environment

NOTE

Condensation within the module can damage the system electronics in case of improper

use or storage!

Of the cooling module was shipped in cold weather, leave it in its box and allow it to warm

slowly to room temperature to avoid condensation.

The cooling module will work within specifications at ambient temperatures and relative

humidity as described in chapter 9 (see Tab. 4)

4. MODE OF OPERATION

The cooling module for the sample tray of the Agilent 1220 Infinity II LC System is firmly

mounted on the LC. It is designed to temper the sample tray from 5 ⁰C to 40 ⁰C.

The module is controlled by the delivered SIM software (possible options: driver for

OpenLAB CDS ChemStation/EZChrom/2.x or a standalone version).

The original sample tray is modified by a metal plate beneath the sample tray. This plate is

cooled with a Peltier element. Heat is drawn outside the system using a heat exchanger with

circulating cooling water.

The metal plate beneath the sample tray (for 100 x 1.8 ml vials) transmits the temperature to

the sample vials. During cooling, condensation will appear in the system. The condensed

water is safely guided out of the module.

The cooling module contains its own power supply and is switched on separately.

Communication of the cooling module with the stand-alone software or the OpenLAB driver

takes place via the local network.

If the standalone version is used, the APG Remote interface will transmit the system status.

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