Agilent Technologies 1200 series Manual de usuario

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Agilent 1200 Series

Manual Injector

Reference Manual

2 1200 Series MI Reference Manual

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

intoaforeign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1328-90010

Edition

02/06

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn, Germany

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

thisdocumentarefurnishedunder alicense

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

Software and technical data rights granted

to federal government customers include

only those rights customarily provided to

end user Customers of Software. Agilent

providesthiscustomarycommercial license

in Software and technical data pursuant to

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(ComputerSoftware)and,forDepartmentof

Defense purchases, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commercial

Computer Software or Computer Software

Documentation). Ifafederalgovernmentor

otherpublic sector Customerhas a need for

rights not conveyed under these terms, it

must negotiate with Agilent to establish

acceptable terms in a written agreement

executed by all relevant parties.

Safety Notices

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTIONnoticeuntiltheindicated

conditionsarefullyunderstoodand

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adheredto, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

1200 Series MI Reference Manual 3

In This Guide…

1 Installing the Manual Injector

Site requirements and installation of the manual injector

2 Repairing the Manual Injector

Instructions on simple, routine repair procedures

3 Parts and Materials

Detailed illustrations and lists for identification of parts and

materials

4 Theory of Operation

Operation and mechanical hardware

4 1200 Series MI Reference Manual

1200 Series MI Reference Manual 5

Contents

1 Installing the Manual Injector

Unpacking the Manual Injector 8

Installing the Manual Injector 10

Flow Connections 14

Leak Drainage 16

Choice of Injection Seal 17

Needles 17

2 Repairing the Manual Injector

Overview of Repair Procedures 20

Flushing the Manual Injector 21

Cleaning the Manual Injector 21

Stator Face 22

Injection-Valve Seal 24

Position-Sensing Switch 26

3 Parts and Materials

Manual Injector 30

Injection-Valve Assembly 32

4 Theory of Operation

Description 36

Injecting Sample 37

6 1200 Series MI Reference Manual

A Safety Information

Solvent Information 40

Agilent Technologies on Internet 41

Index

Agilent 1200 Series Manual Injector

Reference Manual

Agilent Technologies

Installing the Manual Injector

Unpacking the Manual Injector 8

Installing the Manual Injector 10

Flow Connections 14

Leak Drainage 16

Choice of Injection Seal 17

Needles 17

8 1200 Series MI Reference Manual

1 Installing the Manual Injector

Unpacking the Manual Injector

Damaged Packaging

Upon receipt of your manual injector, inspect the shipping containers for any

signs of damage. If the containers or cushioning material are damaged, save

them until the contents have been checked for completeness and the manual

injector has been mechanically checked. If the shipping container or

cushioning material is damaged, notify the carrier and save the shipping

material for the carriers inspection.

Delivery Checklist

Ensure all parts and materials have been delivered with the manual injector.

The delivery checklist is shown in Table 1. To aid in parts identification,

please see “Parts and Materials” on page 29. Please report missing or damaged

parts to your local Agilent Technologies sales and service office.

CAUTION Ifthere are signs ofdamageto themanualinjector,please donotattempt toinstallthe

manual injector.

Table 1 Manual Injector Checklist

Description Quantity Part Number

Manual injection valve with start cable,including:

operating instructions, needle port cleaner, vent tubes

(×2) and fittings, 5/64 and 9/64-inch hex keys

1 5063-6502

Mounting pole 1 5001-3738

Connection capillary, 0.17 mm id, 500 mm 1 G1328-87600

Base plate 1 G1328-44111

Organizer plate 1 5042-8553

Catch tube cap 1 5042-8576

1200 Series MI Reference Manual 9

Installing the Manual Injector 1

Valve syringe, fixed needle 50 µl 1 5182-9619

Reference Manual 1 G1328-90010

Table 1 Manual Injector Checklist (continued)

Description Quantity Part Number

10 1200 Series MI Reference Manual

1 Installing the Manual Injector

Installing the Manual Injector

1Place the baseplate on the bench.

2Connect the two organizer plates to the base plate.

3Screw the mounting pole into one of the two holes in the organizer plate.

NOTE The manual injector can be installed at the left- or right-hand side of the instrument stack.

Figure 1 Connecting the Organizer Plates

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