Agilent Technologies 5975 MSD Manual de usuario

Agilent Technologies

Agilent 5975/5977 MSD

for OpenLAB CDS

Operation Manual

2 5975/5977 Series MSD Operation Manual

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G7077-90014

Edition

First edition, August 2015

Printed in USA, August 2015

Agilent Technologies, Inc.

5301 Stevens Creek Boulevard

Santa Clara, CA 95051

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in damage to the product or

loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are

fully understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in personal injury or death.

Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

5975/5977 Series MSD Operation Manual 3

About This Manual

This manual contains information for operating and

maintaining the Agilent 5975 through 5977 series of MSD with

OpenLAB CDS software. Agilent OpenLAB CDS is a new

operating system for Agilent instruments.

The Agilent 5977B Series Mass Selective Detector (MSD) is the

base instrument described in this manual. Agilent instruments

manufactured prior to the 5977B share many features and

hardware with this new instrument. Where older Agilent

models differ from the 5977B, that difference is usually noted.

Please refer to the operating and maintenance documentation

that was delivered with your instrument if other hardware

differences are found.

1 “Introduction”

Chapter 1 describes general information about the 5977B Series

MSDs, including a hardware description, general safety

warnings, and hydrogen safety information.

2 “Installing GC Columns”

Chapter 2 shows you how to prepare a capillary column for use

with the MSD, install it in the GC oven, and connect it to the

MSD using the GC/MSD interface.

3 “Operating in Electron Ionization (EI) Mode”

Chapter 3 describes basic tasks such as setting temperatures,

monitoring pressures, tuning, venting, and pumpdown. Much of

the information in this chapter also applies to CI operation.

4 “General Maintenance”

Chapter 4 describes maintenance procedures common to both

EI and CI instruments.

4 5975/5977 Series MSD Operation Manual

Hardware User Information

5977B MSD

Accompanying your hardware and software, is a comprehensive

collection of manuals, videos, user applications, and method

development tools. These are located on the Agilent GC and

GC/MS User Manuals and Tools DVD set.

See the Agilent 5977B MSD System Quick Start document

(G7077-90103) for more details on how to install this

information on your computer.

5975/5977 Series MSD prior to the 5977B MSD

Users of Agilent MSD instruments manufactured prior to the

5977B should refer to the documentation delivered to them

when their MSD was purchased. The information in this manual

is intended to supplement that documentation. Information

included here will help you more effectively use the OpenLAB

CDS operating system with your instruments.

Additionally, there is extensive online Help and Learning

material provided with OpenLAB.

5975/5977 Series MSD Operation Manual 5

Contents

About This Manual 3

Hardware User Information 4

5977B MSD 4

5975/5977 Series MSD prior to the 5977B MSD 4

1 Introduction

5977B Series MSD Version 10

Abbreviations Used 11

The 5977B Series MSD 13

MSD Hardware Description 15

Important Safety Warnings 16

Hydrogen Safety 18

GC precautions 18

Precautions 20

Safety and Regulatory Certifications (5977B) 23

Cleaning/Recycling the Product 26

Liquid Spillage 26

Moving or Storing the MSD 26

To Replace the Primary Fuses 27

2 Installing GC Columns

Columns 30

To Install a Capillary Column in a Split/Splitless Inlet 33

To Condition a Capillary Column 36

To Install a Capillary Column in the GC/MS Interface Using the

Self-Tightening Column Nut 37

GCMS transfer line tip seals 41

6 5975/5977 Series MSD Operation Manual

To Install a Capillary Column in the GC/MS Interface Using a

Standard Column Nut 42

3 Operating in Electron Ionization (EI) Mode

Operating the MSD from the Data System 46

Operating the MSD from the GC control panel 47

Configuring the MSD through the Web User Interface (WUI) 51

To change the network settings of the MSD 51

Operating the 5975/5977 MSD from the local control panel

(LCP) 54

Modes of operation 54

To view system status during startup 57

eModule mini display readout 61

Front Panel Instrument Status LED 61

The GC/MSD Interface 62

Before You Turn On the MSD 64

Pumping Down 65

Controlling Temperatures 65

Controlling Column Flow 65

Venting the MSD 66

Set MS Analyzer Temperatures 67

Enable the GC/MS Interface and Oven 69

View MSD Temperatures and Vacuum 70

To Calibrate Column Flow Linear Velocity 72

To Run an Autotune 74

To Open the MSD Covers 76

Vent the MSD 77

5975/5977 Series MSD Operation Manual 7

To Pump Down the MS 79

To Move or Store the MSD 82

4 General Maintenance

Before Starting 86

Maintaining the Vacuum System 91

Maintaining the Analyzer 92

To Open the Analyzer Chamber 94

To Remove the EI Ion Source 96

To Disassemble the Standard or Inert EI Ion Source 99

To Disassemble the Extractor EI Ion Source 102

To Clean the EI Ion Source 105

To Assemble a Standard or Inert EI Ion Source 110

To Assemble the Extractor EI Ion Source 113

To Replace a Filament in an EI Ion Source 116

To Install the EI Ion Source 118

To Attach Wiring from the Ion Source to the feedthrough

board 119

To Replace the Electron Multiplier Horn 122

To Close the Analyzer Chamber 125

8 5975/5977 Series MSD Operation Manual

Agilent 5977B Series Agilent 5975/5977 MSD for OpenLAB CDS

Operation Manual

Agilent Technologies

Introduction

5977B Series MSD Version 10

Abbreviations Used 11

The 5977B Series MSD 13

MSD Hardware Description 15

Important Safety Warnings 16

Hydrogen Safety 18

Safety and Regulatory Certifications (5977B) 23

Cleaning/Recycling the Product 26

Liquid Spillage 26

Moving or Storing the MSD 26

To Replace the Primary Fuses 27

This chapter describes general information about the MSD, including a

hardware description, general safety warnings, and hydrogen safety

information.

10 5975/5977 Series MSD Operation Manual

1Introduction

5977B Series MSD Version

The 5977B Series MSDs are equipped with a turbomolecular (turbo) pump and

a choice of four foreline pumps or a diffusion pump paired with a Pfeiffer DUO

2.5 foreline pump. There are two types of EI sources, a standard stainless steel

EI source and an extraction EI source available on the Inert Plus MSD model.

A CI ion source includes a reagent flow control system, a CI calibration

system, and other required hardware features. The serial number label

displays a product number (Table 1) that indicates what type of MSD you have.

Table 1 Available high vacuum pumps

Model name Product number Description Ionization mode/Type

5977B MSD Diff Pump G7080B Diffusion pump Electron ionization

(EI)/Stainless Steel

5977B MSD Turbo Pump G7081B Turbo pump Electron ionization

(EI)/Stainless Steel

5977B Inert+ MSD

EI Turbo

G7077B Turbo pump MSD Electron ionization

(EI)/Extractor

5977B EI/CI MSD*G7078B Turbo pump MSD Electron ionization

(EI)/Extractor

Chemical ionization /PCI, NCI

* Operation in CI mode is not supported on the initial version of OpenLAB CDS

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