Agilent Technologies 1290 Infinity II Manual de usuario

Agilent Technologies

Agilent InfinityLab LC Series

1290 Infinity II

Preparative Open-Bed

Fraction Collector

User Manual

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7159-90000 Rev. C

Edition

02/2017

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

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contract, Software is delivered and licensed

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or as a “commercial item” as defined in

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software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 3

In This Guide

This manual contains technical reference information about the Agilent 1290

Infinity II Preparative Open-Bed Fraction Collector (G7159B).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Using the Fraction Collector

This chapter explains the essential operational parameters of the module.

4 Preparing the Fraction Collector

This chapter explains the operational parameters of the module.

5 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features and the different user interfaces.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Maintenance

This chapter describes the maintenance of the module.

8 Parts for Maintenance and Repair

This chapter provides information on parts for maintenance and repair.

4 1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

In This Guide

9 Identifying Cables

This chapter provides information on cables used with the module.

10 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

11 Appendix

This chapter provides additional information on safety, legal, and web.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 5

Contents

1Introduction 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

2 Site Requirements and Specifications 15

Site Requirements 16

Physical Specifications 19

Performance Specifications 20

3 Using the Fraction Collector 23

Solvent Information 24

Turn on/off 26

Status Indicators 27

Drawer Status Indicator 28

Exchange Drawers 29

Exchange Containers 31

Replace Inlet/Waste Tubings 32

4 Preparing the Fraction Collector 37

Best Practices 38

Solvent Information 39

Capillary Color Coding Guide 45

Installing Capillaries 46

Setting up the Fraction Collector with the Instrument Control Interface 49

Method Parameter Settings 55

Pooling 63

6 1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Contents

5 Troubleshooting and Diagnostics 65

User Interfaces 66

Agilent Lab Advisor Software 67

6 Error Information 69

What Are Error Messages 70

General Error Messages 71

7 Maintenance 79

Introduction to Maintenance 80

Warnings and Cautions 81

Cleaning the Module 83

Overview of Maintenance 84

Install and Remove the Top Fume Hood 85

Clean the Leak Pan 87

Prepare the Module for Transportation 88

Replace the Module Firmware 90

8 Parts for Maintenance and Repair 91

Supported Containers 92

List of Recommended Fraction Tubes 93

Fraction Collector Accessory Kit 94

Tubing Kits 95

Top Fume Hood Kit 97

9 Identifying Cables 99

Cable Overview 100

Analog Cables 102

Remote Cables 104

CAN/LAN Cables 108

RS-232 Cables 109

USB 110

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 7

Contents

10 Hardware Information 111

Firmware Description 112

Electrical Connections 115

Interfaces 118

Setting the 6-bit Configuration Switch 126

Early Maintenance Feedback 130

Instrument Layout 131

11 Appendix 133

General Safety Information 134

Waste Electrical and Electronic Equipment Directive 140

Radio Interference 141

Sound Emission 142

Agilent Technologies on Internet 143

8 1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Contents

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Agilent Technologies

Introduction

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

This chapter gives an introduction to the module and an instrument overview.

10 1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Introduction

Product Description

The Agilent 1290 Infinity II Preparative Open-Bed Fraction Collector is the

ideal solution that automatically manages high-capacity fraction collection of

purified peaks for semi-preparative and preparative scale purification. Collect

milligrams to multi-gram quantities of sample intuitive with ease. The Agilent

1290 Infinity II Preparative Open-Bed Fraction Collector features handling a

wide variety of collection vessels with ease and capacity of up to 5.9 L by using

150 x 25 mm (L x OD). The containers use identification tags to automatically

detect the vessel dimensions. With a novel robotic technology, Y-, Z-, theta-axis

probe functionality minimizes sample carryover between the fractions during

movements between the vessels. The Agilent 1290 Infinity II Preparative

Open-Bed Fraction Collector is optimized for flow rates up to 200 mL/min,

and can be easily integrated with any Agilent solvent delivery module,

autosampler, or detector.

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