Agilent Technologies Varian MERCURY Series Manual técnico

Installation

Planning

ERCURY

VxWorks Powered

ERCURY

-Series NMR Spectrometer Systems

Pub. No. 01-999021-00, Rev. A0100

NOTICE: This document contains references to Varian.

Please note that Varian, Inc. is now part of Agilent

Technologies. For more information, go to

www.agilent.com/chem.

Installation Planning: M

ERCURY

VxWorks Powered

ERCURY

Series NMR

Spectrometer Systems

Pub. No. 01-999021-00, Rev. A0100

Applicability of manual:

ERCURY

VxWorks-Powered

NMR spectrometer systems

(shortened to

ERCURY

throughout this manual)

Technical contributors: FritsVosman, Mark Stevenson

Technical writer: Dan Steele

Technical editor: James Welch

Revision history:

A0398 – Initial release as Pub. No. 01-999021-00 (was 87-192324-00)

A0698 – Updated telephone numbers

A0399 – Corrected magnetic ﬁeld plots in room layout diagrams

A0100 – Updated phone list

1996−

2000 by Varian, Inc.

3120 Hansen Way, Palo Alto, California 94304

http://www.varianinc.com

The information in this document has been carefully checked and is believed to be

entirely reliable. However, no responsibility is assumed for inaccuracies. Statements in

this document are not intended to create any warranty, expressed or implied.

Speciﬁcations and performance characteristics of the software described in this manual

may be changed at any time without notice.Varian reserves the right to make changes in

any products herein to improve reliability, function, or design. Varian does not assume

any liability arising out of the application or use of any product or circuit described

herein; neither does it convey any license under its patent rights nor the rights of others.

Inclusion in this document does not imply that any particular feature is standard on the

instrument.

UNITY

INOVA

ERCURY

,Gemini,

GEMINI 2000

,UNITY

plu

s,UNITY,VXR,XL,VNMR,

VnmrS, VnmrX, VnmrI, VnmrV, VnmrSGI, MAGICAL II, AutoLock, AutoShim,

AutoPhase, limNET,ASM, and SMS are registered trademarks or trademarks ofVarian,

Inc. Sun, Solaris, CDE, Suninstall, Ultra, SPARC, SPARCstation, SunCD, and NFS are

registered trademarks or trademarks of Sun Microsystems, Inc. and SPARC

International. Oxford is a registered trademark of Oxford Instruments LTD. Ethernet is

a registered trademark of Xerox Corporation.VxWORKS and VxWORKS POWERED

are registered trademarks of WindRiver Inc. Other product names in this document are

registered trademarks or trademarks of their respective holders.

01-999021-00 A0100 Installation Planning Guide

Table of Contents

Introduction ........................................................................................................ 7

Chapter 1. System Delivery.............................................................................. 9

1.1 Preparing for System Delivery ........................................................................... 10

1.2 Moving the SystemAfter Delivery ..................................................................... 10

1.3 Selecting a Local Shipping Company ................................................................ 11

1.4 Postdelivery Procedure ....................................................................................... 12

Chapter 2. Site Requirements ........................................................................ 13

2.1 Site Size .............................................................................................................. 14

2.2 Ceiling Height .................................................................................................... 15

2.3 Accessibility ....................................................................................................... 15

2.4 Maximum Altitude .............................................................................................. 15

2.5 Structural Strength of Floor ................................................................................ 15

2.6 Antivibration Bolt-Down Requirement .............................................................. 17

2.7 Floor Vibration Requirements ............................................................................ 17

2.8 Magnetic Environment ....................................................................................... 18

2.9 Radio-Frequency Environment ........................................................................... 19

2.10 Electrostatic Discharges ................................................................................... 20

2.11 Ambient Temperature and Humidity ................................................................ 20

2.12 Ventilation ......................................................................................................... 21

2.13 Helium and Nitrogen Reﬁll Volumes and Intervals .......................................... 21

Chapter 3. Site Preparation ............................................................................ 23

3.1 Line Voltage Variation ........................................................................................ 23

3.2 Uninterrupted Power Supply (UPS) ................................................................... 24

3.3 Electrical Outlets ................................................................................................ 24

3.4 Compressed Air Supply ...................................................................................... 25

3.5 Compressed Nitrogen Gas .................................................................................. 26

3.6 Telephone and Internet Access ........................................................................... 26

3.7 Air Conditioning ................................................................................................. 26

3.8 Computer Preparation ......................................................................................... 27

Chapter 4. Installation Supplies..................................................................... 31

4.1 Required Installation Supplies and Equipment .................................................. 31

4.2 Recommended Installation Supplies and Equipment ......................................... 34

Installation Planning Guide 01-999021-00 A0100

Chapter 5. Stray Magnetic Fields................................................................... 35

5.1 Safety Hazards of Strong Magnetic Fields .......................................................... 35

5.2 Stray Field Plots .................................................................................................. 36

5.3 Posting Requirements for Magnetic Field Warning Signs .................................. 39

Chapter 6. NMR Room Layouts...................................................................... 41

6.1 RF Cable Harness ................................................................................................ 41

6.2 Magnetic Field Considerations ........................................................................... 41

6.3 Typical Room Layouts ........................................................................................ 41

Index.................................................................................................................. 51

01-999021-00 A0100 Installation Planning Guide

List of Figures

Figure 1.

MERCURY

-Series Cabinet, Open Front and Back ............................................ 9

Figure 2.

Plan Views of Floor Contact Points of Magnet Stands ................................... 16

Figure 3.

Platform Antivibration System Leg Placements and Sizes ............................. 16

Figure 4.

Magnet LegAntivibration System Leg Placement and Sizes ......................... 17

Figure 5.

Stray Field Plots for 200-MHz Magnets ......................................................... 37

Figure 6.

Stray Field Plots for 300-MHz Magnets ......................................................... 37

Figure 7.

Stray Field Plots for 400-MHz Magnets ......................................................... 38

Figure 8.

10-Gauss Warning Sign ................................................................................... 40

Figure 9.

5-Gauss Warning Sign ..................................................................................... 40

Figure 10.

Magnet Area Danger Sign ............................................................................. 40

Installation Planning Guide 01-999021-00 A0100

List ofTables

Table 1.

Magnet Dimensions and Weights as Shipped with Crate and Pallet* ............................. 11

Table 2.

MERCURY-VX

Cabinet and Optional Components as Shipped with Carton and Pallet* 11

Table 3.

Magnet Dimensions and Weights with Stand and Legs Attached* ................................. 14

Table 4.

MERCURY-VX

Cabinet and Optional Components Dimensions and Weights* ............. 14

Table 5.

Ceiling Height Minimum ................................................................................................ 15

Table 6.

Interaction Between Common Objects and a Magnetic Field ......................................... 18

Table 7.

Spectrometer and Nuclei Operating Frequencies ............................................................ 19

Table 8.

Ambient Temperature and Relative Humidity ................................................................. 20

Table 9.

Liquid Helium Displacement for Room Ventilation Considerations .............................. 21

Table 10.

Helium and Nitrogen Reﬁll Intervals and Volumes ....................................................... 21

Table 11.

Electrical Outlet Requirements ..................................................................................... 24

Table 12.

Compressed Air Supply Source ..................................................................................... 25

Table 13.

Air Conditioning Requirements .................................................................................... 26

Table 14.

Solaris Preinstallation Worksheet .................................................................................. 29

Table 15.

Initial On-Site and Short-Notice Liquid Helium Supplies ............................................ 32

Table 16.

Initial On-Site Liquid Nitrogen Supply ......................................................................... 32

Table 17.

Helium Gas Supply ....................................................................................................... 33

Table 18.

Stray Field Data for Oxford Magnets ............................................................................ 36

Table 19.

Stray Field Data for NMR Magnet Systems ................................................................. 36

01-999021-00 A0100 Installation Planning Guide

Introduction

The

Installation Planning

guide assists the customer in selecting and preparing a site to

install a Varian

MERCURY

Vx Works-Powered NMR spectrometer system (shortened to

MERCURY-VX

throughout this manual), including preparing the computer system. Using

the predelivery and postdelivery checklists provided and following the information

presented in this guide should bring about a smooth transition from delivery to installation.

This guide contains the following chapters:

•

Chapter 1, ”System Delivery,” describes how to prepare for system delivery and

provides shipping dimensions and weights for NMR system components.

•

Chapter 2, “Site Requirements,” lists the factors to consider when selecting the

installation site.

•

Chapter 3, “Site Preparation,” describes the many factors to consider—electrical,

cooling, safety, supplies, and so forth—when preparing the installation site.

•

Chapter 4, “Installation Supplies,” discusses the required and recommended supplies

for the system installation.

•

Chapter 5, “Stray Magnetic Fields,” provides magnetic ﬁeld safety data and shows

stray ﬁeld plots for each magnet system.

•

Chapter 6, “NMR Room Layouts,” provides help in laying out the system room.

Safety Precautions

Throughout this guide are important warnings and cautions that you should read and follow

carefully. These safety precautions have the following format and meaning:

WARNING:

Warnings

are used when failureto observeinstructions orprecautions

could result in injury or death to humans or animals,

or signiﬁcant

property damage.

CAUTION:

Cautions

are used when failure to observe instructions could result in

permanent damage to equipment or loss of data.

Importance of Communication

In planning the system installation, good communications are essential between the

customer, the facility planner or architect, and Varian on a frequent basis. Any questions or

problems must be addressed immediately to avoid delays and additional costs.

One person from the customer’s institution should be appointed to coordinate site planning

and preparation. This person should represent all users of the system in dealing withVarian

and the facility planner or architect.

We at Varian will make every effort to ensure that the ownership of your new NMR

spectrometer is a lasting and pleasurable experience.

Introduction

Installation Planning Guide 01-999021-00 A0100

ContactingVarian

Varian’s staff of thoroughly trained service specialists throughout the world is your

assurance of always receiving prompt attention.

For product sales and service information, contact one of the Varian sales ofﬁces:

•

Argentina, BuenosAires, (114) 783-5306

•

Australia, Mulgrave, Victoria, (3) 9566-1138

•

Austria, Vösendorf, (1) 699 96 69

•

Belgium, Brussels, (2) 721 48 50

•

Brazil, Sao Paulo, (11) 829-5444

•

Canada, Ottawa, Ontario, (613) 260-0331

•

China, Beijing, (10) 6846-3640

•

Denmark, Herlev, (42) 84 6166

•

France, Orsay, (1) 69 86 38 38

•

Germany, Darmstadt, (6151) 70 30

•

Italy, Milan, (2) 921351

•

Japan, Tokyo, (3) 5232 1211

•

Korea, Seoul, (2) 3452-2452

•

Mexico, Mexico City, (5) 523-9465

•

Netherlands, Houten, (30) 635 0909

•

Norway, Oslo, (9) 86 74 70

•

Russian Federation, Moscow, (95) 241-7014

•

Spain, Madrid, (91) 472-7612

•

Sweden, Solna, (8) 445 1601

•

Switzerland, Zug, (41) 749 88 44

•

Taiwan, Taipei, (2) 2698-9555

•

United Kingdom, Walton-on-Thames, England (1932) 898 000

•United States, PaloAlto, California,

Varian, Inc., NMR Systems

Customer Sales Support, (650) 424-5145

Service Support, PaloAlto, California, 1 (800) 356-4437

E- mail: customer.support@nmr.varian.com

North American Service Manager

6440 Dobbin Rd, Ste D, Columbia, MD 21045

(410) 964-3065

•Venezuela, Valencia (41) 257608

01-999021-00 A0100 Installation Planning Guide 9

Chapter 1. System Delivery

Sections in this chapter:

•1.1 “Preparing for System Delivery” page 10

•1.2 “Moving the SystemAfter Delivery” page 10

•1.3 “Selecting a Local Shipping Company” page 11

•1.4 “Postdelivery Procedure” page 12

Varian’s delivery responsibility ends atVarian’s factory shipping dock or at the customer’s

receiving dock, depending upon the type of insurance obtained by the customer. In either

case, the customer must provide a moving crew to move the shipping crates holding the

system from the delivery truck (or storage location) to the installation site.

The method of shipping and the current conditions at the destination determine the extent

of the receiving preparations. The Varian Order Acknowledgment form indicates the

shipping method for the order. The following service is usually provided:

•Air Freight. System is delivered to unloading dock or other easily accessible outside

unloading point. Factory to destination transit time is about two days (not including

time to clear customs).

•Motor or Moving Van. System is delivered to an easily accessible interior location or

any interior location to which freight can be easily transported by movable dolly.

Excluded is transport in elevators that cannot support the weight of the shipment or up

stairways. Factory to destination within the United States is about eight days.

Figure 1 illustrates the open front and back of a MERCURY-series cabinet.

Front Back

SHM / DAC

DRIVER

CAUTION

DISABLE POWER

BEFORE

REMOVING / INSTALLING

BOARDS

ACQ CPU

ETHERNET

SERIAL PORT

STM / OUTPUT

ADC

DIAGNOSTICS

JUNCTION BD

HOMO DCPLR

HI / LOW BND

4 NUCLEI

REF GEN

LOW BND TX

OBS RX

HI BND TX

HET DCPLR

LOCK TX

LOCK RX

Figure 1. MERCURY-Series Cabinet, Open Front and Back

Digital and

rf card cages

Power supply

and amplifiers

controller

Reset

switch

PFG

amplifier

(optional)

boot up

(optional)

Chapter 1. System Delivery

10 Installation Planning Guide 01-999021-00 A0100

1.1 Preparing for System Delivery

The following steps will help you prepare for delivery of the system. Refer to the relevant

sections in this manual for additional instructions and safety precautions. Consult

knowledgeable individuals, such as plant facilities personnel, for assistance in

implementing these instructions.

1. Check the “SHIP BY” date on the Varian Order Acknowledgment form. Use this

date as a target for completing installation preparations.

If you anticipate any delays in site readiness and need to delay shipment, notify the

factory at least 90 days in advance.

2. Select the site for installing and operating the system. The site must meet the

requirements described in Chapter 2, “Site Requirements,” on page 13.

3. Prepare the installation site, including electrical outlets, compressed air supply, air

conditioning, and host computer setup form. Site preparation details are discussed in

Chapter 3, “Site Preparation,” on page 23.

Chapter 6, “NMR Room Layouts,” on page 41 provides some sample NMR room

layouts. When setting up the NMR room, remember to consider the stray magnetic

ﬁelds, as discussed in Chapter 5, “Stray Magnetic Fields,” on page 35.

4. Order the supplies and equipment needed for installation and startup operation.

These supplies are described in Chapter 4, “Installation Supplies,” on page 31.

5. Make arrangements for workers and equipment to move the system upon delivery to

the installation site. Refer to 1.2 “Moving the SystemAfter Delivery” page 10 for

details on moving the system. Refer to 1.3 “Selecting a Local Shipping Company”

page 11 for details on selecting a local shipping company.

1.2 Moving the System After Delivery

To avoid unnecessary expense, be sure moving personnel and equipment are ready for the

shipment on the delivery day. If possible, move the crates in an upright position, with a

forklift or hydraulic pallet mover, directly to the installation site.

CAUTION: Move the crates in an upright position.Do not drop or mishandle.The

crates are packed with G-force and“tip-and-tell”indicators that record

mishandling. Be especially careful about moving the magnet crate. If

one or more crates cannot be moved into the installation site because

of doorway clearance, leave the affected crates in a clean, safe, dry

location.Do not open any crate except with direct instructions from an

authorized service representative.

The installation site must be accessible from the delivery location with adequate clearance

for system crates and moving equipment throughout the access route. Table 1 and Table 2

contain system dimensions and weights for calculating vertical, horizontal, and turning

clearances, as well as evaluating the structural strength of passageways. Moving the larger

crates of the system requires a forklift or hydraulic pallet mover, which must be considered

when calculating accessibility.

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