Agilent Technologies SIPS 10 Manual de usuario

Agilent Sample

Introduction Pump

System SIPS 10/20

User’s Guide

2 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

Notices

1997, 2003–2004, 2010, 2012, 2016,

2017

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Manual Part Number

8510132800

Edition

Tenth edition, July 2017

Agilent Technologies, Inc.

679 Springvale Road Mulgrave,

Victoria, 3170, Australia

www.agilent.com

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the

implied warranties of merchantability

and fitness for a particular purpose.

Agilent shall not be liable for errors

or for incidental or consequential

damages in connection with the

furnishing, use, or performance of

this document or of any information

contained herein. Should Agilent and

the user have a separate written

agreement with warranty terms

covering the material in this

document that conflict with these

terms, the warranty terms in the

separate agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance

with the terms of such license.

Restricted Rights Legend

If software is for use in the

performance of a U.S. Government

prime contract or subcontract,

Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

defined in FAR 2.101(a) or as

“Restricted computer software” as

defined in FAR 52.227-19 (June 1987)

or any equivalent agency regulation or

contract clause. Use, duplication or

disclosure of Software is subject to

Agilent Technologies’ standard

commercial license terms, and non-

DOD Departments and Agencies of the

U.S. Government will receive no

greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 3

Contents

1. Safety Practices and Hazards 9

General 9

Verifying Safe State 10

Hazard Warnings 10

Electrical Hazards 10

Moving Parts Hazard 11

Chemical Hazards 11

Other Precautions 11

Notes and Tips 11

Warning Symbols 12

Information Symbols 13

Color Coding 13

CE Compliance 13

Electromagnetic compatibility 14

EN55011/CISPR11 14

ICES/NMB-001 15

2. Introduction 17

About this Manual 20

3. Specifications 21

Environmental 21

Power 22

Contents

4 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

External Connections 22

Weights and Dimensions 23

Weight 23

Dimensions (W × D × H) 23

Performance 23

4. Installation 25

Installation Checklist 26

Unpacking 26

Power 27

Checking the Fuses 27

Installing the Pump Unit and Electronic Control Module 28

Cabling 30

Connecting to the Agilent AA/Computer 30

Connecting to the SIPS Unit 30

Installing the Pump Bands 32

Installing the Diluent Tubing 33

Connecting the SIPS to the Nebulizer 33

Installing the SIPS Pump Tubing 33

Extending the Pump Tubing 35

Calibrating the SIPS Pressure Arm Force 35

Computer-controlled Instruments 35

Standalone Agilent 50/55 AA Instruments 37

Conditioning the SIPS Pump Tubing 38

Fitting the Dust Cover 38

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 5

Connection to an Autosampler 38

Rinse Solution 39

Replacing the Pump Tubing 39

5. Operation 41

Operational Tips 42

Nebulizer Setup 43

Automatic Calibration from a Single Standard 44

SIPS 10 44

SIPS 20 45

Automatic Calibration and Dilution of Overrange Samples 46

SIPS 10 46

SIPS 20 47

Autorun with QC Spikes (SIPS 20) 48

Online Addition of Chemical Modifier or Internal Standard

(SIPS 20) 50

Using the Autosamplers and the SIPS 10 51

Single Pump SIPS 20 Operation 52

Standard Additions Calibration 53

SIPS 20 53

SIPS 10 54

6. Command Reference 57

Method Window 58

Type/Mode Page 58

Measurement Page 58

Contents

6 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

SIPS Page 58

Standards Page 62

QC Tests Page 63

Sequence Parameters Window 64

Options Page 64

Analysis Window 64

Calibrate Pumps 64

Determine SIPS LRR 65

Flame Facilities Dialog 65

Load 65

Unload 65

Purge RH Pump 66

Purge LH Pump 66

Stop Pumps 66

Flame Optimization 66

Start Pump 66

Stop Pump 66

7. Maintenance 67

Daily 67

Weekly 70

Monthly 70

8. Troubleshooting 73

Two Pumps Not Connected 74

SIPS 10 74

SIPS 20 74

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 7

Pump Calibration Failed! Switch to Single Pump Operation 74

Dual Pump SIPS or Diluter Required to Prepare Standard Additions75

Unable to Achieve Blank Reading 75

No Flame Detected – SIPS Operation Cannot Continue 76

Dilution Factor > 50 76

Dilution factor > 200 76

LRR Calibration Failed – Default LRR Value Used 77

SIPS Offline or Pump Not Connected 77

The SIPS Doesn't Pump 77

The Absorption Signal Drifts Over Time 78

Poor Sensitivity 78

Poor Precision 79

There are Spikes in the Absorbance Signal 79

The Accuracy of the Result is Poor 79

Contents

8 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

This page is intentionally left blank.

Safety Practices and Hazards

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 9

1. Safety Practices and Hazards

General 9

Verifying Safe State 10

Hazard Warnings 10

Electrical Hazards 10

Moving Parts Hazard 11

Chemical Hazards 11

Other Precautions 11

Notes and Tips 11

Warning Symbols 12

Information Symbols 13

Color Coding 13

CE Compliance 13

Electromagnetic compatibility 14

General

Operation of the Sample Introduction Pump System (SIPS) accessory

involves the use of high voltage and moving parts. Careless, improper

or unskilled use of this accessory can cause death or serious injury to

personnel, or severe damage to equipment and property.

Appropriate safety practices have been included in this operation

manual and your spectrometer operation manual to help you operate

the equipment safely. Read all safety practices thoroughly before

attempting to operate your system.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be

impaired.

Safety Practices and Hazards

10 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

Verifying Safe State

The following general safety precautions must be observed during all

phases of operation, maintenance and service of this instrument.

To ensure continued safety of the instrument after maintenance or

service procedures, verify the instrument is returned to a safe state

for the user. This includes running performance checks to verify the

instruments safety systems are functioning correctly. Check the

general condition of the instrument during operation for wear or

signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings

elsewhere in this manual violates safety standards of design,

manufacture, and intended use of the instrument. Agilent

Technologies assumes no liability for the customer’s failure to

comply with these requirements.

Hazard Warnings

In addition to the hazard warnings specified in your spectrometer

operation manual, specific hazard warnings have been included in

this operation manual. These warnings state the hazard, describe

how to avoid it and specify the possible consequences of not

following the instructions. Read all warnings carefully and observe

them at all times.

Electrical Hazards

The SIPS electronic control module contains electrical circuits,

devices and components operating at dangerous voltages. Contact

with these circuits, devices and components can cause death, serious

injury or painful electric shock. Panels or covers retained by screws

on the SIPS may be opened only by an Agilent field service engineer.

A blown fuse should be replaced only with one of the size and rating

specified in the text adjacent to the fuse holder. Always ensure that

the accessory is turned off and disconnected from the mains supply

before attempting any replacement.

Este manual sirve para los siguientes modelos

Tabla de contenidos

Otros manuales de Equipo de laboratorio de Agilent Technologies

Agilent Technologies

Agilent Technologies Bravo Platform Manual de usuario

Agilent Technologies

Agilent Technologies G1888 Manual de operación

Agilent Technologies

Agilent Technologies 4100 Instrucciones de funcionamiento

Agilent Technologies

Agilent Technologies Enhancer Cell Manual de usuario

Agilent Technologies

Agilent Technologies 85091C Manual de usuario

Agilent Technologies

Agilent Technologies G1960-60470 Manual de usuario

Agilent Technologies

Agilent Technologies 11970 Series Manual de usuario

Agilent Technologies

Agilent Technologies 6890 Series Manual de usuario

Agilent Technologies

Agilent Technologies TS-8989 PXI Manual de usuario

Agilent Technologies

Agilent Technologies G1701EA Manual de usuario

Agilent Technologies

Agilent Technologies 1290 Infinity II Manual de usuario

Agilent Technologies

Agilent Technologies U1840A Medalist sj5000 Manual de usuario

Agilent Technologies

Agilent Technologies Truevolt Series Manual de servicio

Agilent Technologies

Agilent Technologies G3199 Series Manual de usuario

Agilent Technologies

Agilent Technologies ESG series Instrucciones de funcionamiento

Agilent Technologies

Agilent Technologies InfinityLab LC Series Manual de usuario

Agilent Technologies

Agilent Technologies 4107 Manual de usuario

Agilent Technologies

Agilent Technologies agilent 7683B Instrucciones de instalación y funcionamiento

Agilent Technologies

Agilent Technologies G1367A Manual de usuario

Agilent Technologies

Agilent Technologies PlateLoc Manual de usuario

Agilent Technologies

Agilent Technologies 1290 infinity Manual de usuario

Agilent Technologies

Agilent Technologies 1260 Infinity Manual de usuario

Agilent Technologies

Agilent Technologies Intuvo 900 Guía del usuario

Agilent Technologies

Agilent Technologies 1100 Series Manual de usuario

Manuales populares de Equipo de laboratorio de otras marcas

Qiagen

Qiagen DML 3000 Manual de usuario

Queensgate

Queensgate NANOSCAN OP400 Manual de programación

Conviron

Conviron GEN1000-GE Manual de usuario

Parr Instrument

Parr Instrument 4560 Manual de instrucciones

IKA

IKA IC control Manual de usuario

Integra

Integra DOSE IT Manual de usuario

Endress+Hauser

Endress+Hauser Cleanfit CPA875 Manual de usuario

NI PXI-5422 Manual

Collomix

Collomix Aqix Manual de usuario

SPEX SamplePrep

SPEX SamplePrep 6875 Freezer/Mill Series Manual de usuario

Ocean Insight

Ocean Insight FLAME-NIR+ Manual de usuario

Parker

Parker ALIGN-MG-NA Manual de usuario

BD 644787 Manual de usuario

DENTAURUM

DENTAURUM Compact Megaplus Manual de usuario

Biuged Laboratory Instruments

Biuged Laboratory Instruments BGD 626 Manual de usuario

VWR

VWR SAS Super IAQ Manual de usuario

illumina

illumina MiSeqDx Manual de usuario

Yamato

Yamato BM510 Manual de usuario