Agilent Technologies SIPS 10 Manual de usuario

Agilent Sample

Introduction Pump

System SIPS 10/20

User’s Guide

2 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

Notices

1997, 2003–2004, 2010, 2012, 2016,

2017

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by United States and international

Manual Part Number

8510132800

Edition

Tenth edition, July 2017

Agilent Technologies, Inc.

679 Springvale Road Mulgrave,

Victoria, 3170, Australia

www.agilent.com

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described in this document are

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Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 3

Contents

1. Safety Practices and Hazards 9

General 9

Verifying Safe State 10

Hazard Warnings 10

Electrical Hazards 10

Moving Parts Hazard 11

Chemical Hazards 11

Other Precautions 11

Notes and Tips 11

Warning Symbols 12

Information Symbols 13

Color Coding 13

CE Compliance 13

Electromagnetic compatibility 14

EN55011/CISPR11 14

ICES/NMB-001 15

2. Introduction 17

About this Manual 20

3. Specifications 21

Environmental 21

Power 22

Contents

4 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

External Connections 22

Weights and Dimensions 23

Weight 23

Dimensions (W × D × H) 23

Performance 23

4. Installation 25

Installation Checklist 26

Unpacking 26

Power 27

Checking the Fuses 27

Installing the Pump Unit and Electronic Control Module 28

Cabling 30

Connecting to the Agilent AA/Computer 30

Connecting to the SIPS Unit 30

Installing the Pump Bands 32

Installing the Diluent Tubing 33

Connecting the SIPS to the Nebulizer 33

Installing the SIPS Pump Tubing 33

Extending the Pump Tubing 35

Calibrating the SIPS Pressure Arm Force 35

Computer-controlled Instruments 35

Standalone Agilent 50/55 AA Instruments 37

Conditioning the SIPS Pump Tubing 38

Fitting the Dust Cover 38

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 5

Connection to an Autosampler 38

Rinse Solution 39

Replacing the Pump Tubing 39

5. Operation 41

Operational Tips 42

Nebulizer Setup 43

Automatic Calibration from a Single Standard 44

SIPS 10 44

SIPS 20 45

Automatic Calibration and Dilution of Overrange Samples 46

SIPS 10 46

SIPS 20 47

Autorun with QC Spikes (SIPS 20) 48

Online Addition of Chemical Modifier or Internal Standard

(SIPS 20) 50

Using the Autosamplers and the SIPS 10 51

Single Pump SIPS 20 Operation 52

Standard Additions Calibration 53

SIPS 20 53

SIPS 10 54

6. Command Reference 57

Method Window 58

Type/Mode Page 58

Measurement Page 58

Contents

6 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

SIPS Page 58

Standards Page 62

QC Tests Page 63

Sequence Parameters Window 64

Options Page 64

Analysis Window 64

Calibrate Pumps 64

Determine SIPS LRR 65

Flame Facilities Dialog 65

Load 65

Unload 65

Purge RH Pump 66

Purge LH Pump 66

Stop Pumps 66

Flame Optimization 66

Start Pump 66

Stop Pump 66

7. Maintenance 67

Daily 67

Weekly 70

Monthly 70

8. Troubleshooting 73

Two Pumps Not Connected 74

SIPS 10 74

SIPS 20 74

Contents

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 7

Pump Calibration Failed! Switch to Single Pump Operation 74

Dual Pump SIPS or Diluter Required to Prepare Standard Additions75

Unable to Achieve Blank Reading 75

No Flame Detected – SIPS Operation Cannot Continue 76

Dilution Factor > 50 76

Dilution factor > 200 76

LRR Calibration Failed – Default LRR Value Used 77

SIPS Offline or Pump Not Connected 77

The SIPS Doesn't Pump 77

The Absorption Signal Drifts Over Time 78

Poor Sensitivity 78

Poor Precision 79

There are Spikes in the Absorbance Signal 79

The Accuracy of the Result is Poor 79

Contents

8 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

This page is intentionally left blank.

Safety Practices and Hazards

Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide 9

1. Safety Practices and Hazards

General 9

Verifying Safe State 10

Hazard Warnings 10

Electrical Hazards 10

Moving Parts Hazard 11

Chemical Hazards 11

Other Precautions 11

Notes and Tips 11

Warning Symbols 12

Information Symbols 13

Color Coding 13

CE Compliance 13

Electromagnetic compatibility 14

General

Operation of the Sample Introduction Pump System (SIPS) accessory

involves the use of high voltage and moving parts. Careless, improper

or unskilled use of this accessory can cause death or serious injury to

personnel, or severe damage to equipment and property.

Appropriate safety practices have been included in this operation

manual and your spectrometer operation manual to help you operate

the equipment safely. Read all safety practices thoroughly before

attempting to operate your system.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be

impaired.

Safety Practices and Hazards

10 Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide

Verifying Safe State

The following general safety precautions must be observed during all

phases of operation, maintenance and service of this instrument.

To ensure continued safety of the instrument after maintenance or

service procedures, verify the instrument is returned to a safe state

for the user. This includes running performance checks to verify the

instruments safety systems are functioning correctly. Check the

general condition of the instrument during operation for wear or

signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings

elsewhere in this manual violates safety standards of design,

manufacture, and intended use of the instrument. Agilent

Technologies assumes no liability for the customer’s failure to

comply with these requirements.

Hazard Warnings

In addition to the hazard warnings specified in your spectrometer

operation manual, specific hazard warnings have been included in

this operation manual. These warnings state the hazard, describe

how to avoid it and specify the possible consequences of not

following the instructions. Read all warnings carefully and observe

them at all times.

Electrical Hazards

The SIPS electronic control module contains electrical circuits,

devices and components operating at dangerous voltages. Contact

with these circuits, devices and components can cause death, serious

injury or painful electric shock. Panels or covers retained by screws

on the SIPS may be opened only by an Agilent field service engineer.

A blown fuse should be replaced only with one of the size and rating

specified in the text adjacent to the fuse holder. Always ensure that

the accessory is turned off and disconnected from the mains supply

before attempting any replacement.

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