Agilent Technologies InfinityLab LC Series Manual de usuario

Agilent Instant Pilot G4208

Agilent InfinityLab LC Series

User’s Guide

G4208A User’s Guide

Notices

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Document No: SD-29000124 Rev. B

Part No: G4208-90010 Rev. B

EDITION 04/2020

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G4208A User’s Guide 3

In This Guide...

This book describes how to operate the Agilent 1100/1200/1260/1290 Series

modules and systems for HPLC using the handheld control module Agilent Instant

Pilot G4208A.

The Instant Pilot provides complete local control and monitoring of a single

module or an entire Agilent 1100/1200/1260 and 1290 Series HPLC system. There

is no data evaluation in the Instant Pilot. The Instant Pilot allows you to do a variety

of HPLC tasks including automated sample preparation and injection, isocratic,

gradient and multiple method analyses and basic diagnostics and maintenance.

1Start-upInformation

This chapter provides general information around the Agilent Instant Pilot.

2 Working with the Instant Pilot

This chapter describes the operation of the Instant Pilot.

3 Running an Isocratic Analysis

This chapter describes how to analyze the Agilent Technologies isocratic standard

sample using a single injection analysis.

4 Running Multiple-Vial Analyses

This chapter describes how to setup multiple vial analyses using the same method

and different methods.

5 Maintenance and Repair

This chapter describes how to perform firmware updates, troubleshooting and

replacements.

6Appendix

This chapter provides safety and other general information.

NOTE

If additional details are required on a specific topic/function/parameter not

mentioned in this document, please use the Instant Pilot’s Online Information

System (i), see “The i (info) key - Online Information System” on page 23.

G4208A User’s Guide 4

Contents

1Start-upInformation7

Instant Pilot Features 8

Features and Benefits 10

Requirements for the Instant Pilot 11

Physical Specifications 13

Cleaning 14

Holder Versions for the Instant Pilot 15

Adding the Instant Pilot to an Agilent HPLC Module 16

Removing the Instant Pilot 20

Instant Pilot Display and Keyboard Layout 21

The i (info) key - Online Information System 23

Basic Operational Concept of the Instant Pilot 26

Getting Started 27

System Information 33

Method Information 34

Sequence Information 36

Status Information 38

Logbook Information 43

Configuration 45

Maintenance Information 46

Diagnosis Information 50

Turning Modules ON/OFF/Standby 51

Start Analysis Screen 52

Switching from G1323A/B Control Module to Instant Pilot 53

Information on Firmware 55

G4208A User’s Guide 5

2 Working with the Instant Pilot 56

Using a USB Flash Drive 57

Printing To USB Flash Drive 59

Working with Methods 64

Sequence - Automating Analyses 84

Displaying Data Graphically 95

DAD/MWD/VWD/FLD Spectrum 98

Connecting External Devices 101

Simultaneous Execution with Software 104

Special Functions 107

3 Running an Isocratic Analysis 108

What You Will Need 109

Preparing the LC System 110

Entering Settings 111

Saving Settings in a Method 112

Creating a Sequence 113

Selecting a Signal 114

Observing the Chromatogram 115

4 Running Multiple-Vial Analyses 116

Analyzing Multiple Vials Using the Same Method 117

Analyzing Multiple Vials Using Different Methods 118

Single-Level Calibration Sequences 120

Multiple-Level Calibration Sequences 123

Re-calibrating With Multiple Groups of Standards 126

Synchronizing Analyses with External Devices 129

G4208A User’s Guide 6

In This Guide...

5 Maintenance and Repair 135

Firmware Updates 136

Troubleshooting 150

Repairing the Instant Pilot 152

Exchanging the CAN Cable 153

6Appendix157

Safety Information 158

Waste Electrical and Electronic Equipment (WEEE) Directive 160

Radio Interference 161

Agilent Technologies on Internet 162

G4208A User’s Guide 7

1Start-upInformation

Instant Pilot Features 8

Features and Benefits 10

Requirements for the Instant Pilot 11

Physical Specifications 13

Cleaning 14

Holder Versions for the Instant Pilot 15

Adding the Instant Pilot to an Agilent HPLC Module 16

Adding the Instant Pilot to an Agilent HPLC Module (1100/1200/1200 Infinity Series) 17

Adding the Instant Pilot to an Agilent HPLC Module (1200 Infinity II Series) 18

Removing the Instant Pilot 20

Instant Pilot Display and Keyboard Layout 21

The i (info) key - Online Information System 23

Basic Operational Concept of the Instant Pilot 26

Getting Started 27

System Information 33

Method Information 34

Sequence Information 36

Status Information 38

Setup of a Status Information Screen 40

Logbook Information 43

Configuration 45

Maintenance Information 46

Early Maintenance Feedback (EMF) 48

Product Number and Serial Number Change 49

Diagnosis Information 50

Turning Modules ON/OFF/Standby 51

Start Analysis Screen 52

Switching from G1323A/B Control Module to Instant Pilot 53

Information on Firmware 55

This chapter provides general information around the Agilent Instant Pilot.

G4208A User’s Guide 8

1 Start-up Information

Instant Pilot Features

Figure 1 The Agilent Instant Pilot

The Agilent Instant Pilot (IP) provides complete local control and monitoring of a

single module or an entire Agilent 1100/1200/1260/1290 Series HPLC system.

You have easy access to every supported function, you can easily control all

parameters and settings and you can configure various communication channels

with other devices, in order to comfortably analyze the generated data.

•Color display, size 13.1 x 9.9 cm (5.0 x 3.8 inch), 640 x 480 dots

•Install any desired configuration of Agilent 1100/1200/1260/1290 Series

HPLC modules. The Instant Pilot software will reflect which modules are

present in the LC system and adjust the screens accordingly.

•Enter parameter settings for every module, perform on/off functions as well

as calibration and configuration settings in a self- explanatory and intuitive

way.

•Define automated analyses including methods, timetables, method

sequences and automated calibration settings using the Instant Pilot.

•Use the configurable status screen to monitor various activities on a single

screen.

•Easy configuration of the system and/or modules.

G4208A User’s Guide 9

1 Start-up Information

Instant Pilot Features

•Protect your method from any inadvertent keyboard changes by setting

method file protection.

•Use USB Flash Drive to store and transfer methods and sequences between

Agilent systems.

•Monitor all operations and error events using the self- updating logbooks.

•Use the context- sensitive online information system to get further

information on all topics.

•To help comply with Good Laboratory Practice (GLP) regulations, select a

variety of module tests that will check the performance of the LC system.

•Use the early maintenance feedback (EMF) limits for scheduling maintenance

work.

•Display data graphically using the Plot screen, where as many as four

different signals can be monitored at the same time.

•Printing to an USB Flash Drive.

•Version A.05.15 is compatible with 1100/1200 modules that run on firmware

A.05.11/13 and A.05.09/10 (introduced November 2006).

NOTE

Firmware revision A.05.13/14 does not run on Instant Pilot modules with serial

numbers starting with MY due to new flash ROM type that does not allow

downgrades to B.02.07 and below. This was fixed with firmware A.05.15 and

B.02.15.

G4208A User’s Guide 10

1 Start-up Information

Features and Benefits

Table 1 Features and Benefits

Feature Benefit

•Large size, color display with background light, high reso-

lution and contrast

Better readability and usability.

•USB port / USB Flash Drive Faster and more flexible method and sequence transfer to

other Agilent systems. Handling for unsupported formats /

formatting

•State of the art electronic Faster application, large number of Agilent modules connect-

able, all detector signals available in plot.

•System visualization with status display in start screen Fast overview of configuration and state of system

•Flat dialog structure; easy to understand icons Much faster confidence and usability, less training required

•Automatic, context sensitive help in status line ('Tool Tip') Easier parameter input through given ranges

•Diagnosis with passed/failed No user interpretation necessary, clear result

•Setup wizards Easier system configuration and sequence setup

•Dynamic adjustment to changed system configuration No restart necessary when system configuration changes,

e.g. different detector

•Method on- and offline editable Methods can be changed during runs

•New sequence: wizard, table view, priority sample, insert

method, parameter, ...

Simpler and more flexible, better overall view

•Printing to USB Flash Drive The files can be opened using Microsoft Internet Explorer and

printed from there.

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