Metrohm 930 Compact IC Flex Manual de usuario

930 Compact IC Flex

930 Compact IC Flex Deg

Manual

8.930.8002EN / 2017-07-31

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

930 Compact IC Flex

930 Compact IC Flex Deg

2.930.1160

Manual

8.930.8002EN / 2017-07-31 zst

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

930 Compact IC Flex Deg (2.930.1160) ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Instrument description ......................................................... 1

1.2 Intended use ......................................................................... 3

1.3 Safety instructions ................................................................ 3

1.3.1 General notes on safety ........................................................... 3

1.3.2 Electrical safety ........................................................................ 3

1.3.3 Tubing and capillary connections ............................................. 4

1.3.4 Flammable solvents and chemicals ........................................... 5

1.3.5 Recycling and disposal ............................................................. 5

1.4 Symbols and conventions .................................................... 5

2 Overview of the instrument 7

2.1 Front ...................................................................................... 7

2.2 Rear ........................................................................................ 8

2.3 Feed-throughs for capillaries and cables .......................... 10

3 Installation 13

3.1 Setting up the instrument .................................................. 13

3.1.1 Packaging .............................................................................. 13

3.1.2 Checks .................................................................................. 13

3.1.3 Location ................................................................................ 13

3.2 Capillary connections in the IC system ............................. 13

3.3 Removing transport locking screws .................................. 16

3.4 Connecting the drainage tubing and leak sensor ............ 17

3.4.1 Installing the drainage tubing ................................................ 17

3.4.2 Connecting the leak sensor .................................................... 19

3.5 Connecting the eluent bottle ............................................. 19

3.6 Connecting the eluent degasser ........................................ 23

3.7 Installing the high-pressure pump .................................... 23

3.8 Installing an inline filter ..................................................... 24

3.9 Installing the pulsation absorber ...................................... 25

3.10 Injection valve ..................................................................... 26

3.11 Installing the conductivity detector .................................. 28

3.12 Installing the amperometric detector ............................... 29

3.13 Connecting the sample degasser (optional) ..................... 29

3.14 Connecting the instrument to a computer ....................... 31

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Deg (2.930.1160)

3.15 Connecting the instrument to the power grid ................. 32

3.16 Initial start-up ..................................................................... 33

3.17 Connecting and rinsing the guard column ....................... 35

3.18 Connecting the separation column ................................... 37

3.19 Conditioning ........................................................................ 40

4 Operation 42

5 Operation and maintenance 43

5.1 IC system ............................................................................. 43

5.1.1 Operation .............................................................................. 43

5.1.2 Care ...................................................................................... 43

5.1.3 Maintenance by Metrohm Service .......................................... 43

5.1.4 Shutting down and recommissioning ..................................... 44

5.2 Capillary connections ......................................................... 45

5.3 Servicing the door .............................................................. 45

5.4 Handling the eluent ............................................................ 45

5.4.1 Manufacturing eluent ............................................................ 46

5.4.2 Changing the eluent .............................................................. 46

5.5 Servicing the eluent degasser ........................................... 47

5.6 Notes on operating the high-pressure pump ................... 47

5.7 Servicing the high-pressure pump .................................... 48

5.8 Servicing the inline filter .................................................... 61

5.9 Servicing the pulsation absorber ...................................... 64

5.10 Injection valve ..................................................................... 64

5.11 Servicing the detector ........................................................ 64

5.12 Rinsing the sample path .................................................... 64

5.13 Separation column ............................................................. 66

5.13.1 Separating efficiency .............................................................. 66

5.13.2 Protecting the separation column .......................................... 66

5.13.3 Storing the separation column ............................................... 66

5.13.4 Regenerating the separation column ...................................... 66

5.14 Quality management and qualification with Metrohm ... 67

6 Troubleshooting 68

6.1 ............................................................................................. 68

7 Technical specifications 72

7.1 Reference conditions .......................................................... 72

7.2 Instrument ........................................................................... 72

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

930 Compact IC Flex Deg (2.930.1160) ￭￭￭￭￭￭￭￭ V

7.3 Ambient conditions ............................................................ 72

7.4 Housing ............................................................................... 73

7.5 Weight ................................................................................. 73

7.6 Leak sensor ......................................................................... 73

7.7 Eluent degasser .................................................................. 73

7.8 High-pressure pump ........................................................... 74

7.9 Injection valve ..................................................................... 75

7.10 Detector ............................................................................... 75

7.11 Sample degasser ................................................................. 75

7.12 Power connection ............................................................... 75

7.13 Interfaces ............................................................................. 76

8 Accessories 77

Index 78

Table of figures ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

VI ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Deg (2.930.1160)

Table of figures

Figure 1 Front ................................................................................................. 7

Figure 2 Rear .................................................................................................. 8

Figure 3 Feed-throughs on the door .............................................................. 10

Figure 4 Openings for capillaries and cables .................................................. 11

Figure 5 Ducts for capillaries ......................................................................... 12

Figure 6 Removing the transport locking screws ............................................ 16

Figure 7 Installing the eluent bottle cap ........................................................ 20

Figure 8 Installing tubing weighting and aspiration filter ................................ 21

Figure 9 High-pressure pump with purge valve .............................................. 24

Figure 10 Inline filter ....................................................................................... 25

Figure 11 Pulsation absorber ........................................................................... 25

Figure 12 Exchanging the sample loop ............................................................ 27

Figure 13 High-pressure pump – Parts ............................................................. 48

Figure 14 High-pressure pump – Cross-section ................................................ 55

Figure 15 Tool for piston seal (6.2617.010) ..................................................... 56

Figure 16 Removing the piston cartridge from the pump head ........................ 56

Figure 17 Inserting the piston seal into the tool ............................................... 57

Figure 18 Parts of the piston cartridge ............................................................ 58

Figure 19 Inline filter – Removing the filter ...................................................... 62

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

930 Compact IC Flex Deg (2.930.1160) ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Instrument description

The 930 Compact IC Flex is a robust ion chromatograph. It is distinguished

by:

￭Its intelligence: All of the functions are monitored, optimized and docu-

mented in an FDA-compatible manner. Intelligent components, such as

iColumns, save important data onto a chip.

￭Its compact design: It has a small footprint.

￭Its transparency: All components are easily accessible and located for

simple visibility and can be monitored during operation through a large

window.

￭Its safety: The wet end and the electronics are physically separated,

thereby preventing fluids from coming into contact with the electronics

to a large extent. A leak sensor is integrated into the wet end.

￭Its environmental compatibility.

￭Its low noise emission.

￭The intelligent MagIC Net software.

The 930 Compact IC Flex is operated using the MagIC Net software. A

USB cable is used to connect the instrument to a computer with

MagIC Net installed. The intelligent software detects the instrument auto-

matically and checks its functionality. The software controls and monitors

the instrument, evaluates the measured data and manages it in a data-

base.

The 930 Compact IC Flex Deg consists of the following modules:

Housing

The sturdy housing contains the instrument's electronic components,

including their interfaces and one connector for a separation column. In

addition, the housing provides space for a conductivity detector or an

amperometric detector. Capillaries and cables can be fed into and out of

the instrument through several openings.

Leak sensor

The leak sensor detects leaking liquid that collects in the instrument's base

tray. Liquid that leaks in the instrument is routed to the base tray using

drainage tubing and detected there.

Eluent degasser

The eluent degasser removes gas bubbles and dissolved gases from the

eluent.

1.1 Instrument description ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 930 Compact IC Flex Deg (2.930.1160)

High-pressure pump

The intelligent and low-pulsation high-pressure pump pumps the eluent

through the IC system. It is equipped with a chip where its technical speci-

fications and "life history" (operating hours, service data, etc.) are stored.

Inline filter

Inline filters protect the separation column reliably from potential contami-

nation from the eluent. The filter pads with 2 µm pore size can be

replaced quickly and easily. They remove particles from the solutions, such

as bacteria and algae.

Pulsation absorber

The pulsation absorber protects the separation column from damage

caused by pressure fluctuations, e.g. when the injection valve is switched,

and reduces interfering pulsations during highly sensitive measurements.

Injection valve

The injection valve connects the eluent path to the sample path. By a

quick and precise switching of the valve, a quantity of sample solution

defined by the size of the sample loop is injected and flushed to the sepa-

ration column with the eluent.

Detector

Metrohm offers a series of different detectors for various analysis tasks. A

suitable detector type must be ordered as a separate device.

Sample degasser

The sample degasser removes gas bubbles and dissolved gases from the

sample.

Separation column

The intelligent separation column separates different components accord-

ing to their interactions with the column. Metrohm separation columns

are equipped with a chip where their technical specifications and history

(start-up, operating hours, injections etc) are stored.

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