Metrohm 930 Compact IC Flex SeS Manual de usuario

930 Compact IC Flex

930 Compact IC Flex SeS

Manual – Short Instructions

8.930.8107EN / v3 / 2023-03-31

Metrohm AG

CH-9100 Herisau

Switzerland

+41 71 353 85 85

[email protected]

www.metrohm.com

930 Compact IC Flex

930 Compact IC Flex SeS

2.930.1400

Manual – Short Instructions

8.930.8107EN / v3 / 2023-03-31

Technical Communication

Metrohm AG

CH-9100 Herisau

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

Disclaimer

Deficiencies arising from circumstances that are not the responsibility of

Metrohm, such as improper storage or improper use, etc., are expressly

excluded from the warranty. Unauthorized modifications to the product

(e.g. conversions or attachments) exclude any liability on the part of the

manufacturer for resulting damage and its consequences. Instructions and

notes in the Metrohm product documentation must be strictly followed.

Otherwise, Metrohm's liability is excluded.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

930 Compact IC Flex SeS (2.930.1400) ￭￭￭￭￭￭￭￭ III

Table of contents

1 About this quick start guide 1

2 Introduction 2

2.1 Instrument description ......................................................... 2

2.2 Accessories and additional information ............................. 4

2.3 Symbols and conventions .................................................... 4

3 Safety 6

3.1 Intended use ......................................................................... 6

3.2 Responsibility of the operator ............................................. 6

3.3 Requirements for operating personnel ............................... 7

3.4 Safety instructions ................................................................ 7

3.4.1 General notes on safety ........................................................... 7

3.4.2 Electrical safety ........................................................................ 7

3.4.3 Tubing and capillary connections ............................................. 8

3.4.4 Flammable solvents and chemicals ........................................... 9

3.4.5 Recycling and disposal ............................................................. 9

4 Overview of the device 10

4.1 Front .................................................................................... 10

4.2 Rear ...................................................................................... 11

5 Installation 13

5.1 Setting up the instrument .................................................. 13

5.1.1 Packaging .............................................................................. 13

5.1.2 Checks .................................................................................. 13

5.1.3 Location ................................................................................ 13

5.2 Capillary connections in the IC system ............................. 13

5.3 Removing transport locking screws .................................. 14

5.4 Connecting the drainage tubing and leak sensor ............ 16

5.4.1 Installing the drainage tubing ................................................ 16

5.4.2 Connecting the leak sensor .................................................... 17

5.5 Connecting the eluent bottle ............................................. 18

5.6 Installing the high-pressure pump .................................... 20

5.7 Installing an inline filter ..................................................... 21

5.8 Installing the pulsation absorber ...................................... 21

5.9 Injection valve ..................................................................... 21

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 930 Compact IC Flex SeS (2.930.1400)

5.10 Metrohm Suppressor Module (MSM) ............................... 21

5.10.1 Inserting the rotors ................................................................ 22

5.10.2 Connecting the Metrohm Suppressor Module (MSM) ............. 23

5.11 Metrohm CO2 Suppressor (MCS) ....................................... 26

5.11.1 Connecting the MCS ............................................................. 26

5.11.2 Installing the adsorber cartridge ............................................. 26

5.12 Installing the conductivity detector .................................. 28

5.13 Installing the amperometric detector ............................... 29

5.14 Connecting the instrument to a computer ....................... 29

5.15 Connecting the instrument to the power grid ................. 30

5.16 Initial start-up ..................................................................... 31

5.17 Connecting and rinsing the guard column ....................... 33

5.18 Connecting and rinsing the separation column ............... 34

5.19 Conditioning ........................................................................ 36

6 Operation 38

Index 39

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

930 Compact IC Flex SeS (2.930.1400) ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front ............................................................................................... 10

Figure 2 Rear ................................................................................................ 11

Figure 3 Removing the transport locking screws ............................................ 15

Figure 4 Installing the tubing weighting and aspiration filter .......................... 20

Figure 5 Metrohm Suppressor Module (MSM) – Connection capillaries .......... 24

Figure 6 Connecting the MCS ....................................................................... 26

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 About this quick start guide

930 Compact IC Flex SeS (2.930.1400) ￭￭￭￭￭￭￭￭ 1

1 About this quick start guide

This short instruction manual contains important chapters from the com-

prehensive manual. In addition to an introduction, safety instructions and

an overview of the instrument, you will also find information about instal-

ling and operating the 930 Compact IC Flex SeS as well as information

regarding the warranty. The comprehensive manual can be downloaded

as a PDF file from the Internet.

Downloading the manual

You can find the detailed manual on the Internet under

http://www.metrohm.com/:

1. Enter the order number for your instrument as the search term (e.g.

2.930.1400).

2. Click on Documents.

All available documents for the instrument will be displayed.

3. Click on the PDF link to download the desired manual.

2.1 Instrument description ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 930 Compact IC Flex SeS (2.930.1400)

2 Introduction

2.1 Instrument description

The 930 Compact IC Flex is a robust ion chromatograph. It is distinguished

by:

￭Its intelligence: All of the functions are monitored, optimized and docu-

mented in an FDA-compatible manner. Intelligent components, such as

iColumns, save important data onto a chip.

￭Its compact design: It has a small footprint.

￭Its transparency: All components are easily accessible and located for

simple visibility and can be monitored during operation through a large

window.

￭Its safety: The wet end and the electronics are physically separated.

This prevents fluids from coming into contact with the electronics to a

large extent. A leak sensor is integrated into the wet end.

￭Its environmental compatibility.

￭Its low noise emission.

￭The intelligent MagIC Net software.

The 930 Compact IC Flex is operated using the MagIC Net software. A

USB cable is used to connect the device to a computer with MagIC Net

installed. The intelligent software detects the device automatically and

checks its functionality. The software controls and monitors the device,

evaluates the measured data and manages it in a database.

The 930 Compact IC Flex SeS consists of the following modules:

Housing

The sturdy housing contains the instrument's electronic components,

including their interfaces and one connector for a separation column. In

addition, the housing provides space for a conductivity detector or an

amperometric detector. Capillaries and cables can be fed into and out of

the instrument through several openings.

Leak sensor

The leak sensor detects leaking liquid that collects in the instrument's base

tray. Liquid that leaks in the instrument is routed to the base tray using

drainage tubing and detected there.

High-pressure pump

The intelligent and low-pulsation high-pressure pump pumps the eluent

through the IC system. It is equipped with a chip where its technical speci-

fications and "life history" (operating hours, service data, etc.) are stored.

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