Metrohm 889 IC Sample Center Basic Manual de usuario

889 IC Sample Center Basic

Manual

8.889.8004EN / v1 / 2023-01-10

Metrohm AG

CH-9100 Herisau

Switzerland

+41 71 353 85 85

[email protected]

www.metrohm.com

889 IC Sample Center Basic

Manual

8.889.8004EN / v1 / 2023-01-10

Technical Communication

Metrohm AG

CH-9100 Herisau

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

Disclaimer

Deficiencies arising from circumstances that are not the responsibility of

Metrohm, such as improper storage or improper use, etc., are expressly

excluded from the warranty. Unauthorized modifications to the product

(e.g. conversions or attachments) exclude any liability on the part of the

manufacturer for resulting damage and its consequences. Instructions and

notes in the Metrohm product documentation must be strictly followed.

Otherwise, Metrohm's liability is excluded.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

889 IC Sample Center Basic ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Device description ................................................................ 1

1.1.1 Model versions ........................................................................ 1

1.1.2 Device components ................................................................. 1

1.1.3 Accessories and additional information .................................... 2

1.2 About the documentation ................................................... 2

1.2.1 Symbols and conventions ........................................................ 2

2 Safety 4

2.1 Intended use ......................................................................... 4

2.2 Responsibility of the operator ............................................. 4

2.3 Requirements for operating personnel ............................... 5

2.4 Safety instructions ................................................................ 5

2.4.1 General notes on safety ........................................................... 5

2.4.2 Electrical safety ........................................................................ 5

2.4.3 Tubing and capillary connections ............................................. 7

2.4.4 Personnel safety ....................................................................... 7

2.4.5 Flammable solvents and chemicals ........................................... 8

2.4.6 Recycling and disposal ............................................................. 8

3 Overview of the device 9

3.1 Front and rear ....................................................................... 9

3.2 Opening the device ............................................................. 10

3.3 Interior view ........................................................................ 12

3.4 Interior ................................................................................. 13

3.5 Cooling option .................................................................... 14

4 Installation 15

4.1 Setting up the instrument .................................................. 15

4.1.1 Packaging .............................................................................. 15

4.1.2 Checks .................................................................................. 15

4.1.3 Location ................................................................................ 15

4.1.4 Removing the device from the packaging .............................. 15

4.2 Connecting the instrument to the power grid ................. 16

4.3 Connecting a computer ...................................................... 17

4.4 Tubing setup ....................................................................... 18

4.5 Drainage tubing .................................................................. 19

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 889 IC Sample Center Basic

5 Operation and maintenance 21

5.1 General ................................................................................ 21

5.2 Care ...................................................................................... 21

5.2.1 Cleaning in general ................................................................ 22

5.3 Maintenance and service ................................................... 22

5.3.1 Replacing the sample needle ................................................. 22

5.3.2 Replacing the air needle ........................................................ 24

5.3.3 Replacing the fuses ................................................................ 25

6 Troubleshooting 26

6.1 Error list ............................................................................... 26

6.1.1 General ................................................................................. 26

6.1.2 Rack unit ............................................................................... 26

6.1.3 Needle unit ............................................................................ 27

6.1.4 Cooling unit .......................................................................... 29

6.1.5 Electronics ............................................................................. 29

6.2 Analytical problems ............................................................ 30

6.2.1 Autosampler .......................................................................... 30

7 Appendix 32

7.1 Samples and sample vials .................................................. 32

7.2 I/O interface ........................................................................ 32

7.2.1 Properties of the I/O interface ................................................ 33

7.2.2 Pin assignment of the remote interface .................................. 33

8 Technical specifications 34

8.1 General ................................................................................ 34

8.2 Sampling .............................................................................. 34

8.3 Interfaces ............................................................................. 35

8.4 Options (pre-installed) ........................................................ 35

8.5 Power connection ............................................................... 35

8.6 Ambient conditions ............................................................ 35

8.7 Dimensions .......................................................................... 36

Index 37

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

889 IC Sample Center Basic ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 889 IC Sample Center Basic - front .................................................... 9

Figure 2 889 IC Sample Center Basic - rear .................................................... 10

Figure 3 Interior view without covering ......................................................... 12

Figure 4 Interior with sampling equipment .................................................... 13

Figure 5 Interior view with installed cooling option ....................................... 14

Figure 6 Unpacking the 889 IC Sample Center Basic ...................................... 15

Figure 7 Mounting the outlet tubing ............................................................. 19

Figure 8 Mounting the leakage tubing .......................................................... 19

Figure 9 Connecting the outlet tubing .......................................................... 20

Figure 10 Replacing the sample needle ........................................................... 22

Figure 11 Pin assignment of I/O socket and plug ............................................. 33

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

889 IC Sample Center Basic ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Device description

The 889 IC Sample Center Basic is a robust Autosampler for high sample

throughput, optimized for the challenges of the modern analytics labora-

tory. Its greatest advantages are small sample volumes and the cooling

option (8.889.0040).

Special features:

￭The control per PC software makes operation readily comprehensible.

A context-sensitive online help function is available for every window

and every dialog.

￭As a means of enhancing safety, no needle movements are carried out

when the door is open.

￭The optional sample cooling guarantees consistent results.

Standard microtiter plates (high or low form) or sample racks can be used.

Different plates or racks can be present in the left-hand and right-hand

loading drawers.

1.1.1 Model versions

2.889.0030 889 IC Sample Center Basic

With:

￭Needle with capillary, 79 µL (6.2816.220)

2.889.0040 889 IC Sample Center Basic – cool

With:

￭Needle with capillary, 79 µL (6.2816.220)

￭Accessories for cooling the samples

1.1.2 Device components

The 889 IC Sample Center Basic has the following components:

￭2 sample racks

Each for 48 vials.

￭Needle arm

With air needle and drives for horizontal and vertical positioning.

￭Cooling module (optional)

For cooling the samples.

￭USB connector

For the connection to a PC.

1.2 About the documentation ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 889 IC Sample Center Basic

￭I/O interface

For output of an inject marker signal.

1.1.3 Accessories and additional information

Additional information is available on the Metrohm website (https://

www.metrohm.com):

￭Product family

￭Product versions

￭Accessories

￭Documents about the product

Downloading the accessories list

NOTICE

The accessories list is a part of the product documentation. Download

the accessories list and store it as a reference.

1. Use the search function to search for the product.

2. Open the desired product version.

3. Download the accessories list.

1.2 About the documentation

CAUTION

Read through this documentation carefully before putting the device

into operation. The documentation contains information and warnings

which the user must follow in order to ensure safe operation of the

device.

1.2.1 Symbols and conventions

The following symbols and styles are used in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the

second to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

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