Agilent Technologies 8355 Sulfur Manual de usuario

Agilent Technologies

Agilent 8355 Sulfur and

8255 Nitrogen

Chemiluminescence

Detectors

User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or

translation into a foreign language)

without prior agreement and written

consent from Agilent Technologies, Inc. as

governed by United States and

international copyright laws.

Manual Part Number

G3488-90010

Edition

Fourth edition, February 2016

Third edition, December 2015

Second edition, October 2015

First edition, September 2015

Printed in USA or China

Agilent Technologies, Inc.

2850 Centerville Road

Wilmington, DE 19808-1610 USA

安捷伦科技（上海）有限公司

上海市浦东新区外高桥保税区

英伦路 412 号

联系电话：（800）820 3278

Warranty

The material contained in this document

is provided “as is,” and is subject to

being changed, without notice, in future

editions. Further, to the maximum extent

permitted by applicable law, Agilent

disclaims all warranties, either express

or implied, with regard to this manual and

any information contained herein,

including but not limited to the implied

warranties of merchantability and fitness

for a particular purpose. Agilent shall not

be liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or performance

of this document or of any information

contained herein. Should Agilent and the

user have a separate written agreement

with warranty terms covering the

material in this document that conflict

with these terms, the warranty terms in

the separate agreement shall control.

Safety Notices

CAUTION

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered

to, could result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indicated

conditions are fully understood and

met.

SCD and NCD User Manual 3

Contents

1 Getting Started

Manuals, Information, Tools and Where to Find Them 8

GC Manuals, Tools, and Online Help 8

User Apps 14

Education Opportunities 17

Overview of the 8355 SCD and 8255 NCD 18

Overview of Installation and First Startup 22

2 Safety and Regulatory Information

Introduction 24

Important Safety Information 25

Many internal parts of the detector carry dangerous voltages 25

Electrostatic discharge is a threat to GC electronics 26

Many parts are dangerously hot 26

Hydrogen safety 26

Ozone 28

Oxygen environments 28

Symbols 29

Fuses 30

Safety and Regulatory Information 31

Sound Emission Certification for Federal Republic of Germany 32

Schalldruckpegel 32

Electromagnetic compatibility 32

Intended Use 34

Cleaning 34

Recycling the Product 34

Technical Assistance 34

4SCD and NCD User Manual

3SystemDescription

Specifications 36

8355 SCD 36

8255 NCD 36

Theory of Operation 37

SCD 37

NCD 37

Description of Major Components 39

Burner assembly 39

Ozone generator 41

Reaction cell and photomultiplier tube (PMT) 42

EPC modules 42

Vacuum pump 42

Ozone destruction trap 42

Oil coalescing filter 42

FID adapter (optional) 42

NCD chiller 43

4Operation

Introduction 46

Integrated version 46

Setting Parameters 47

Parameters and ranges 47

Software control 48

GC keyboard control 50

Identifying the detector 50

Detector Stability and Response 51

Typical Operating Conditions 52

Adjusting the Operating Conditions 53

Start-up 54

Resource Conservation 55

Shutdown 56

Configure Auto Flow Zero on the GC 57

Configure the Detector 58

SCD and NCD User Manual 5

5 Maintenance

Maintenance Log and Early Maintenance Feedback (EMF) 62

Maintenance Schedule 63

Tracking Detector Sensitivity 64

Consumables and Replacement Parts 65

Exploded Parts View of the SCD 67

Exploded Parts View of the NCD 68

Detector Maintenance Method 69

Attach a Column to the Detector 70

Replace the Inner Ceramic Tube (SCD) 73

Replace the Quartz Tube (NCD) 76

Check the Vacuum Pump Oil 80

Add Vacuum Pump Oil 81

Replace the Vacuum Pump Oil 83

Replace the Ozone Trap 85

Change the Oil Mist Filter 87

Clean the Detector Exterior 88

Calibrate the Flow and Pressure Sensors 89

Updating Firmware 90

6 Troubleshooting

Solving Detector Problems 92

Troubleshooting Table 93

Status Indicator LED 96

Detector Messages 97

Leaks 98

Ozone leaks 98

Hydrogen leaks 98

Oxidizer leaks 98

Checking for hydrogen and oxidizer leaks 99

Power Problems 100

No power 100

Ozone Generation Problems 101

6SCD and NCD User Manual

Coking 102

Hydrogen Poisoning 103

Contaminated Gases 104

7 Performance Verification

About Chromatographic Checkout 106

Prepare for Chromatographic Checkout 107

Prepare sample vials 108

Check SCD Performance 109

Check NCD Performance 114

Agilent 8355 SCD and 8255 NCD

User Manual

Agilent Technologies

Getting Started

Manuals, Information, Tools and Where to Find Them 8

Overview of the 8355 SCD and 8255 NCD 18

Overview of Installation and First Startup 22

This chapter introduces the Agilent 8355 Sulfur

Chemiluminescence Detector (SCD) and the Agilent 8255

Nitrogen Chemiluminescence Detector (NCD), and provides

details about where to find helpful information and tools, such

as GC manuals, flow calculators, and so forth.

8SCD and NCD User Manual

1Getting Started

Manuals, Information, Tools and Where to Find Them

This manual describes how to operate the Agilent 8355 Sulfur

Chemiluminescence Detector (SCD) and the Agilent 8255

Nitrogen Chemiluminescence Detector (NCD) as installed on an

Agilent 7890B Gas Chromatograph (GC). This manual also

provides operating recommendations, maintenance procedures,

and troubleshooting. For installation instructions, see the

Agilent 8355 SCD and 8255 NCD Installation and First Startup

Guide. To prepare the installation site for a new SCD or NCD,

see the Agilent 8355 SCD and 8255 NCD Site Preparation

Guide.

In addition, Agilent provides other manuals, familiarization

information, and help systems for self-paced learning about the

7890B GC. You will need to reference this general GC

information for installation and operation of the detector. The

sections below describe this information and where to find it.

GC Manuals, Tools, and Online Help

Agilent provides several learning products that explain how to

install, operate, maintain, and troubleshoot the 7890B GC

system. These manuals can be found on the Agilent GC and

GC/MS User Manuals & Tools DVDs that are included with your

GC shipment.

Installing your manuals provides for a much richer user

experience by providing the ability to install the manuals you

want, in the language you want. Install HTML and PDF versions.

Getting Started 1

SCD and NCD User Manual 9

Allrights reserved.

Madein USA

Agilent Technologies

GC/GCMS Hardware User Manuals and Videos

S1N

Disk 2/3

Toinstall:

1.Insert disk into DVD drive

2.Follow the instructions on the screen.

3.If autoplay is not enabled, double-click

"index_xx.html"on the DVD

where xx is:

enfor English

chfor 中文

jp for 日本語

Version B.01.05

January,2013

Allrights reserved.

Madein USA

Agilent Technologies

GC/GCMS Hardware User Manuals and Videos

S1N

Disk 2/3

Toinstall:

1.Insert disk into DVD drive

2.Follow the instructions on the screen.

3.If autoplay is not enabled, double-click

"index_xx.html"on the DVD

where xx is:

enfor English

chfor 中文

jp for 日本語

Version B.01.05

January,2013

Select the Instrument Manuals icon

from the GC and GC/MS User Manuals

& Tools DVD and install the suite of

manuals for your system.

10 SCD and NCD User Manual

1Getting Started

Available manuals

Table 1 7890B GC Learning Products

Learning product Contents When to use this documentation

Getting Started Overview of the manuals. Where to

find information. How to install the

manuals. Overview of the GC.

Safety Manual Lists safety and regulatory

information. Precautions for using

hydrogen carrier (or fuel) gas.

Precautions for performing

maintenance tasks.

•Before installation, to prepare for a

safe installation process.

•Before maintenance.

GC, GC/MS, and ALS Site Prep Guide Requirements for: space and weight

for the lab bench, power, heat

dissipation, exhaust venting,

laboratory conditions (expected local

environment), gas and reagent gas

purity, gas supplies, gas plumbing

(including filters, regulator types, and

tubing needs), and cryogenic cooling

supplies (if used).

Recommended supplies to purchase

before installation.

•Before installation, to prepare the

laboratory site.

•Before installation, to find what

supplies are needed for successful

installation (such as gases,

installation kits, gas purifiers,

regulators, tubing, fittings,

consumable parts, and so on).

•At any time, to refer to expected

requirements for gas supplies,

regulators, cryogenic cooling

supplies, supply pressures, and so

on.

Installation and First Startup How to install the GC on the

laboratory bench. Cabling pinouts.

•During installation.

Operation Manual Common keyboard functions. Using

the keyboard to start runs and

sequences. Using the keyboard when

connected to an Agilent data system.

Methods and sequences overview.

Startup and shutdown. How to check

GC performance after installation.

Energy conservation (sleep/wake).

Early Maintenance Feedback.

Configuration.

•To learn common operating tasks

(making a run, loading a method,

running a series of samples).

•To learn how to use the GC keyboard

when under data system control.

•Before a short-term or long-term

shutdown.

•When starting up the GC after a

period of inactivity.

•Whenever you need to verify

performance of the instrument

against factory standards, for

example, after certain maintenance

procedures.

•To learn how to properly configure GC

components, especially when newly

installed.

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