Agilent Technologies InfinityLab LC Series Manual de usuario

Diode Array Detectors

Agilent InfinityLab LC Series

User Manual

Agilent InfinityLab LC Series Diode Array Detectors User Manual

Notices

Document Information

Document No: SD-29000132 Rev. B

EDITION 09/2020

No part of this manual may be repro-

duced in any form or by any means

(including electronic storage and retrieval

or translation into a foreign language)

without prior agreement and written con-

sent from Agilent Technologies, Inc. as

governed by United States and interna-

tional copyright laws.

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future edi-

tions. Further, to the maximum extent

permitted by applicable law, Agilent dis-

claims all warranties, either express or

implied, with regard to this manual and

any information contained herein, includ-

ing but not limited to the implied warran-

ties of merchantability and fitness for a

particular purpose. Agilent shall not be lia-

ble for errors or for incidental or conse-

quential damages in connection with the

furnishing, use, or performance of this

document or of any information con-

tained herein. Should Agilent and the user

have a separate written agreement with

warranty terms covering the material in

this document that conflict with these

terms, the warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such

license.

Restricted Rights Legend

U.S. Government Restricted Rights. Soft-

ware and technical data rights granted to

the federal government include only

those rights customarily provided to end

user customers. Agilent provides this

customary commercial license in Soft-

ware and technical data pursuant to FAR

12.211 (Technical Data) and 12.212

(Computer Software) and, for the Depart-

ment of Defense, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commer-

cial Computer Software or Computer

Software Documentation).

Safety Notices

CAUTI ON

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in personal injury or death.

Do not proceed beyond a WARN-

ING notice until the indicated

conditions are fully understood

and met.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 3

In This Book

This manual covers the Agilent 1290 Infinity II Diode Array Detectors

•G7117A - 1290 Infinity II Diode Array Detector FS (with fixed slit)

•G7117B - 1290 Infinity II Diode Array Detector (with variable slit)

•G7117C - 1260 Infinity II Diode Array Detector HS (with fixed slit)

Find information on other Agilent Diode Array Detectors in separate manuals.

1 Introduction

This chapter gives an introduction to the detector and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3 Using the Module

This chapter explains the essential operational parameters of the module.

4 Preparing the Module

This chapter provides information on how to set up the module for an analysis and

explains the basic settings.

5 Optimizing the Detector

This chapter provides information on how to optimize the detector.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 4

8 Test Functions and Calibration

This chapter describes the tests for the module.

9 Maintenance

This chapter describes the maintenance of the module.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter provides information on cables used with the Agilent 1200 Infinity

Series modules.

12 Hardware Information

This chapter describes the detector in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 5

Contents

1 Introduction 9

Overview of the Module 10

Product Description 11

Optical System 14

Leak and Waste Handling 19

Operating Principle 24

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3 Using the Module 37

Magnets 38

Turn on/off 39

Status Indicators 41

Instrument Configuration 42

Set up the Detector with Agilent Open Lab ChemStation 44

The Detector User Interface 45

Detector Control Settings 47

Method Parameter Settings 48

4 Preparing the Module 52

Leak and Waste Handling 53

Setting up an Analysis 55

Solvent Information 62

Capillary Coding Guide 68

Installing Capillaries 71

Agilent InfinityLab LC Series Diode Array Detectors User Manual 6

5 Optimizing the Detector 75

Introduction 76

Optimization Overview 77

Optimizing for Sensitivity, Selectivity, Linearity and Dispersion 83

Optimizing Selectivity 94

Optimizing the Detector Regarding to the System 96

Warm up of the Detector 102

6 Troubleshooting and Diagnostics 104

Available Tests vs User Interfaces 105

Agilent Lab Advisor Software 107

7 Error Information 108

What Are Error Messages 109

General Error Messages 110

Detector Error Messages 116

8 Test Functions and Calibration 121

Introduction 122

Use of Max-Light Cartridge Test Cell 126

Conditions of Detector 127

Failing a Test 127

Self-Test 128

Intensity Test 130

Cell Test 132

Quick Noise Test 134

ASTM Drift and Noise Test 137

Slit Test 140

Wavelength Verification Test 143

Wavelength Calibration 145

D/A Converter (DAC) Test 148

Dark Current Test 150

Other Lab Advisor Functions 152

Agilent InfinityLab LC Series Diode Array Detectors User Manual 7

9 Maintenance 153

Introduction to Maintenance 154

Warnings and Cautions 154

Overview of Maintenance 156

Cleaning the Module 157

Remove and Install Doors 157

Replace the Deuterium Lamp 159

Replace the Max-Light Cartridge Cell 162

Clean the Max-Light Cartridge Cell 165

Storage of Max-Light Cartridge Cell 166

Correcting Leaks 167

Replace Leak Handling System Parts 168

Replace the Module Firmware 170

Information from Module’s Assemblies 171

10 Parts and Materials for Maintenance 172

Overview of Maintenance Parts 173

Accessory Kit 174

11 Identifying Cables 175

Cable Overview 176

Analog Cables 178

Remote Cables 180

CAN/LAN Cables 183

RS-232 Cables 184

USB Cables 184

12 Hardware Information 185

Firmware Description 186

Electrical Connections 189

Interfaces 192

Setting the 6-bit Configuration Switch 199

Instrument Layout 202

Early Maintenance Feedback 203

Agilent InfinityLab LC Series Diode Array Detectors User Manual 8

13 LAN Configuration 205

What You Have to Do First 206

TCP/IP parameter configuration 207

Configuration Switches 208

Initialization Mode Selection 209

Dynamic Host Configuration Protocol (DHCP) 211

Manual Configuration 214

14 Appendix 219

General Safety Information 220

Waste Electrical and Electronic Equipment (WEEE) Directive 226

Radio Interference 227

Sound Emission 227

Solvent Information 228

Agilent Technologies on Internet 229

Agilent InfinityLab LC Series Diode Array Detectors User Manual 9

1 Introduction

Overview of the Module 10

Product Description 11

Product Description G7117A 11

Product Description G7117B 12

Product Description G7117C 13

Optical System 14

Lamp 15

Max-Light Cartridge Flow Cell 15

Slit Assembly 16

Grating and Diode Array 18

Leak and Waste Handling 19

Waste Concept 23

Operating Principle 24

This chapter gives an introduction to the detector and an instrument overview.

Agilent InfinityLab LC Series Diode Array Detectors User Manual 10

1 Introduction

Overview of the Module

The detector is designed for highest optical performance, GLP compliance and

easy maintenance. It includes the following features:

•Maximum of 120 Hz (G7117A/G7117C) or 240 Hz (G7117B) data acquisition

rate.

•Higher sensitivity for conventional LC as well as ultra fast applications by

using next generation optical design.

•Increased sensitivity with 60 mm Max-Light cartridge flow cell.

•Optimized cell geometry for less peak dispersion for narrow bore applications.

•Max-Light cartridge flow cells for standard applications are available, see

“Max-Light Cartridge Flow Cell” on page 15.

•More reliable and robust peak integration process (automated) due to less

baseline noise/drift/refractive index and thermal effects especially under ultra

fast gradient conditions.

•RFID tracking technology is used for the UV-lamp and the Max-Light cartridge

flow cells.

•Multiple wavelength and full spectral detection at 120 Hz

(G7117A/G7117C)/240 Hz (G7117B) sampling rate, keeping up with the

analysis speed of ultra-fast LC.

•Programmable 1 – 8 nm slit (G7117B) or fixed 4 nm slit (G7117A/C) for rapid

optimization of sensitivity, linearity and spectral resolution provides optimum

incident light conditions.

•Improved Electronic temperature control (ETC) provides maximum baseline

stability and practical sensitivity under fluctuating ambient temperature and

humidity conditions.

•Additional diagnostic signals for temperature and lamp voltage monitoring.

•Easy exchange of flow cell by cartridge design.

Otros manuales para InfinityLab LC Series

Este manual sirve para los siguientes modelos

Tabla de contenidos

Otros manuales de Sensor de seguridad de Agilent Technologies

Agilent Technologies

Agilent Technologies 1260 Infinity Manual de usuario

Agilent Technologies

Agilent Technologies VS C15 Series Guía

Agilent Technologies

Agilent Technologies CrossLab CS Manual de usuario

Agilent Technologies

Agilent Technologies InfinityLab 1290 Infinity II Manual de usuario

Agilent Technologies

Agilent Technologies 8355 Sulfur Manual de usuario

Agilent Technologies

Agilent Technologies 1100 Series Manual de usuario

Agilent Technologies

Agilent Technologies G3388B Manual de instalación

Agilent Technologies

Agilent Technologies G8610 Series Manual de usuario

Agilent Technologies

Agilent Technologies InfinityLab LC Series Manual de usuario

Agilent Technologies

Agilent Technologies PHD-4 Manual de usuario

Agilent Technologies

Agilent Technologies 1260 Infinity Manual de usuario

Agilent Technologies

Agilent Technologies 1260 Infinity Manual de usuario

Agilent Technologies

Agilent Technologies Helium Manual de usuario

Agilent Technologies

Agilent Technologies G3485A Manual de usuario

Agilent Technologies

Agilent Technologies 1100 Series Manual de usuario

Agilent Technologies

Agilent Technologies 355 SCD Manual de usuario

Agilent Technologies

Agilent Technologies 7250 Manual de usuario

Agilent Technologies

Agilent Technologies 8480 Series Manual de servicio

Agilent Technologies

Agilent Technologies VS Series Manual de usuario

Agilent Technologies

Agilent Technologies G1315B Manual de usuario

Agilent Technologies

Agilent Technologies G2334A Manual de usuario

Agilent Technologies

Agilent Technologies G3440-68011 Manual de usuario

Agilent Technologies

Agilent Technologies 6820 GC Manual de usuario

Agilent Technologies

Agilent Technologies 1100 Series Manual de usuario

Manuales populares de Sensor de seguridad de otras marcas

THORLABS

THORLABS PDA10JT Manual de usuario

Waeco

Waeco UV-DETECT Manual de usuario

Intermatic

Intermatic IOS-DSIMF Manual de usuario

urmet domus

urmet domus 1083 Manual de usuario

Siemens

Siemens AZL66 Series Manual de usuario

BTI

BTI Profiline Multi Finder Manual de usuario

Challenger

Challenger SL01 Manual de usuario

DMP Electronics

DMP Electronics 1122INT Manual de usuario

Rielta

Rielta Ladoga MK-RK Manual de usuario

Mirion Technologies

Mirion Technologies ACCURAD PRD Manual de usuario

Bosch

Bosch DS835 Manual de usuario

DBI SALA

DBI SALA EZ Stop Manual del operador

Lamptime

Lamptime ST05C Manual de usuario

Ubiquiti

Ubiquiti MFI-MSC Manual de usuario

Subsite

Subsite 910R Instrucciones de instalación

Satel

Satel OPAL Pro Manual de usuario

Aleph

Aleph XC-1XTEU Manual de usuario

Pima

Pima LARIS QUAD Manual de usuario