Agilent Technologies 5977B Series Manual de usuario

Agilent Technologies

Agilent 5977B Series 

MSD

Operating Manual

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G7077-90026

Edition

First edition, September 2016

Printed in USA

Agilent Technologies, Inc.

5301 Stevens Creek Boulevard

Santa Clara, CA 95051

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in damage to the product or

loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are

fully understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in personal injury or death.

Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

5977B Series MSD Operating Manual 3

About This Manual

This manual contains information for operating and

maintaining the Agilent 5977B Series Mass Selective Detector

(MSD).

1 “Introduction”

Chapter 1 describes general information about the 5977B Series

MSDs, including a hardware description, general safety

warnings, and hydrogen safety information.

2 “Installing 7890 GC Columns”

Chapter 2 shows you how to prepare a capillary column for use

with the MSD, install it in the GC oven, and connect it to the

MSD using the GC/MSD interface.

3 “Intuvo 9000 GC Column Maintenance”

Chapter 3 shows you how to install an Agilent Intuvo column,

connect a flow path from the column through the MS transfer

line and into the ion source, and maintain the column guard

chip.

4 “Operating in EI Mode”

Chapter 3 describes basic tasks such as setting temperatures,

monitoring pressures, tuning, venting, and pumpdown. Much of

the information in this chapter also applies to CI operation.

5 “Operating in CI Mode”

Chapter 4 describes additional tasks necessary to operate in CI

mode.

6 “General Maintenance”

Chapter 5 describes maintenance procedures common to both

EI and CI instruments.

4 5977B Series MSD Operating Manual

7 “CI Maintenance”

Chapter 6 describes maintenance procedures unique to CI

MSDs.

5977B Series MSD Operating Manual 5

6 5977B Series MSD Operating Manual

Hardware User Information

Accompanying your hardware and software is a comprehensive

collection of manuals, videos, user applications, and method

development tools. These are located on the:

•Agilent GC and GC/MS User Manuals and Tools DVD set

•Agilent GC/MS Software Information and Manuals memory

stick

See the Agilent 5977B MSD with MassHunter Quick Start

document for information on finding and installing the

documentation located on this USB and DVDs.

5977B Series MSD Operating Manual 7

Contents

1 Introduction

5977B Series MSD Version 14

Abbreviations Used 15

The 5977B Series MSD 17

MSD Hardware Description 19

Important Safety Warnings 21

Hydrogen Safety 23

GC precautions 24

Precautions 26

Safety and Regulatory Certifications 28

Intended Use 31

Cleaning/Recycling the Product 31

Accidental Liquid Spillage 31

Moving or Storing the MSD 31

To Replace the Primary Fuses 32

2 Installing 7890 GC Columns

Columns 36

To Install a Capillary Column in a Split/Splitless Inlet 38

To Condition a Capillary Column 41

To Install a Capillary Column in the GC/MS Interface Using the

Self-Tightening Column Nut 42

To Install a Capillary Column in the GC/MS Interface Using a

Standard Column Nut 47

To Install the Interface Tip Seal 50

8 5977B Series MSD Operating Manual

To Calibrate Column Flow Linear Velocity 52

The GC/MSD Interface for a 7890B Series GC 55

3 Intuvo 9000 GC Column Maintenance

Columns 58

Conditioning columns 59

Tips and hints 59

To Replace an Intuvo GC Column 61

To Replace an Intuvo 9000 GC Gasket 65

To Install a Column Guard or Jumper Chip 66

To Replace the 9000 GC/MS Tail 70

To Condition an Intuvo Capillary Column 74

To Install the Interface Tip Seal 76

The GC/MS Interface for a 9000 Series GC 77

4 Operating in EI Mode

Operating the MSD from the DS 80

Operating the MSD from the GC control panel 81

Configuring the MSD through the Web User Interface (WUI) 85

To change the network settings of the MSD 85

eModule Mini Display Readout 88

Front Panel Instrument Status LED 88

Before You Turn On the MSD 89

Pumping Down 90

Controlling Temperatures 90

Controlling Column Flow 90

Controlling JetClean Hydrogen Flow 91

5977B Series MSD Operating Manual 9

Venting the MSD 91

To View MSD Temperature and Vacuum in Manual Tune 93

To Set Monitors for MSD Temperature and Vacuum Status 95

To Set Analyzer Temperatures from the Instrument Control

To Set the MassHunter 7890 GC/MSD Interface Temperature

100

To Monitor High Vacuum Pressure 101

To Tune the MSD in EI Mode 104

To Set the Operation Mode for the Optional JetClean System 106

To Set the JetClean Parameters for the Clean Only Mode 107

To Verify EI System Performance 108

To Perform High-Mass Testing 109

To Open the MSD Covers 112

To Vent the MSD 113

To Pumpdown the MSD 116

5 Operating in CI Mode

General Guidelines 120

CI Autotune 121

To Operate the CI MSD 123

To Pumpdown the MSD in CI Mode 124

To Set Up the Software for CI Operation 125

To Operate the Reagent Gas Flow Control Module 127

To Set Up Methane Reagent Gas Flow 130

To Use Other Reagent Gases 132

10 5977B Series MSD Operating Manual

To Perform a PCI Autotune (Methane Only) 135

To Perform an NCI Autotune (Methane Reagent Gas) 137

To Verify PCI Performance 139

To Verify NCI Performance 140

To Monitor CI Mode High Vacuum Pressure 141

6 General Maintenance

Before Starting 144

Maintaining the Vacuum System 149

Maintaining the Analyzer 150

To Open the Analyzer Chamber 152

To Remove the EI HES 154

To Connect/Disconnect Wiring to the EI HES 156

To Disassemble the EI HES 157

To Clean the EI HES 160

To Assemble the EI HES 163

To Remove the EI HES filaments 168

To Install the EI HES Filament 170

To Install the EI HES 171

To Remove the EI XTR, SS, or Inert Source 172

To Connect/Disconnect Wiring from the EI XTR, SS, and Inert

Sources 173

To Disassemble the EI SS or EI Inert Source 174

To Disassemble the EI XTR Source 177

To Clean an EI XTR, SS, or Inert Source 180

To Assemble an EI SS or Inert Source 185

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