PerkinElmer Lambda 365 Manual de usuario

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PerkinElmer, 710 Bridgeport Avenue,

Shelton, CT06484-4794, U.S.A

Produced in the USA.

Lambda 365 Changer 8-Cell for Dissolution Installation

Instructions

This instruction sheet describes the installation of this accessory which is used with the Lambda 365

Spectrophotometer.

NOTE:

Read these instructions before you install this accessory.

Contacting PerkinElmer

Supplies, replacement parts, and accessories can be ordered directly from PerkinElmer, using the part

numbers.

See our website:

http://perkinelmer.com

PerkinElmer's catalog service offers a full selection of high-quality supplies.

To place an order for supplies and many replacement parts, request a free catalog, or ask for information:

If you are located within the U.S., call toll free 1-800-762-4002, 8 a.m. to 8 p.m. EST. Your order will be

shipped promptly, usually within 24 hours.

If you are located outside of the U.S., call your local PerkinElmer sales or service office.

Features

•Suitable size for the standard cells

•Excellent durability

Figure 1 Lambda 365 Changer 8-Cell for Dissolution [P/N: N4104018]

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Dimensions and Specifications

Dimensions

Physical Characteristic Specification Comment

Outline

Height (mm) 140.5

Width (mm) 134.5

Depth (mm) 356.5

Inner

Height (mm) 35

Suitable for the Standard

Cell

Width (mm) 14

Depth (mm) 12.5

Weight (kg) 2.5

Specifications

Physical Characteristic Specification Comment

Space between cells (mm) 10.4

Moving distance of one cell (mm) 11.5

Moving distance of eight cells (mm) 80.5

Moving time of one cell (sec) 1.3

Moving time of eight cells (sec) 8.5

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Configuration of Changer 8-Cell for Dissolution

Figure 2 Changer 8-Cell for Dissolution Configuration

- Used to fix a cell holder, a base plate or a front plate for Lambda 365.

- Spare screws (2 each) are included with the accessory.

Figure 3 Round headscrew with washer (M4 *12L)

Figure 4. Manifold Figure 5. Plate for Calibration

Figure 6. Lid

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Figure 7. Tubings for cell compartment inside (P/N B2000049) and outside

(P/N B2000515)

Figure 8. Flow Cell (N4101052)

NOTE

: Tubings for cell compartment inside (B2000049) and outside (P/N B2000515) and Flow cell

(P/N N4101052) must be purchased separately.

Manifold and tubing connection

1. Prepare a manifold

2. Connect a red connector of the inside tube (P/N B2000049) to the In port of the manifold and

other white connector of the inside tube (short connector) to the flow cell with the arrow mark

(Inlet).

Figure 9. Connecting the inlet tube

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3. Connect a red connector of the inside tube (P/N B2000049) to the Out port of the manifold and

other white connector of the inside tube (long connector) to the flow cell’s outlet port.

Figure 10. Connecting the outlet tube

4. Connect a red connector of the outside tube (P/N B2000515) to the port of the manifold.

Figure 11. Connecting the outside tube

5. Connect all the connectors in the same way.

Figure 12. Manifold and tubing connection

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Installation

1. Prepare the Lambda 365 Spectrophotometer to install this accessory.

2. Connect the power cord and the communication cable. DO NOT turn on the power of the

instrument!

3. Remove the two round head screws with washer (M4*12L) to remove the existing cell holder and

base plate.

Figure 13. Location of the round head screws with washer

4. Pull out the cell holder and base plate by hand.

Figure 14. Pulling out the cell holder and base plate

CAUTION

ATTENTION

Make sure the instrument is turned off while installing this accessory.

Assurez-vous que l’instrument est é

teint lors de l’installation de cet

accessoire.

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5. Insert the Changer 8-Cell for Dissolution in the sample compartment.

Figure 15. Inserting the Changer 8-Cell for Dissolution into the sample compartment

6. Gently press the Changer 8-Cell for Dissolution to connect the communication port (male) under

the bottom of the Changer 8-Cell for Dissolution to the port (female) in the sample compartment.

Figure 16. Connecting the communication ports

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7. Tighten the Changer 8-Cell for Dissolution in the sample compartment with the screws. (The red

circles indicate the location of the screws in the figure).

Figure 17. Tighten the Changer 8-Cell for Dissolution

8. Attach the plate for calibration on the front plate and tighten the 4 bolts.

Figure 18. Tighten the 4 bolts

9. Close the sample compartment cover and turn on the power switch of the instruments.

CAUTION

ATTENTION

Do not start the UV Express software before finishing the initialization of grating.

Ne démarrez pas

le logiciel UV Express avant de terminer l'initialisation du

réseau.

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Measurement

NOTE:

Start the System Self Test after warming up the system for at least 20 minutes.

1. Double-click on the UV Express Software folder and select one of the mode for starting.

2. The following message box will be shown. Empty the cell holder and close the lid firmly. Click OK.

3. System Self Test stars. Click OK after finishing the System Self Test.

4. Select New to open a new window. Select Experiment Type and select OK.

5. Open Method in the main menu.

6. Perform multi-cell calibration according to the ‘Calibration of Multi-Cell Position’ chapter. (p 15)

NOTE:

Calibrate the beam position of the Changer 8-Cell for Dissolution whenever it is installed or beam position

is incorrect.

7. After completing the multi-cell calibration, remove the Plate for Calibration.

Figure 19. Removing the Plate for Calibration

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8. Prepare the manifold with all the tubing connected in Chap. ‘Manifold and tubing connection’ (p4).

Figure 20. Manifold with all the tubing connected

9. Insert the tubes and cells through the front cover first and hold the manifold in place.

Figure 21. Inserting the tubes and cells

10. Tighten the 4 bolts.

Figure 22. Tighten the 4 bolts

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