Metrohm 900 Touch Control Instrucciones de operación

900 Touch Control

Tutorial

8.900.8010EN

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

900 Touch Control

Tutorial

8.900.8010EN 01.2019

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

900 Touch Control ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Structure of the tutorial ....................................................... 1

1.2 Symbols and conventions .................................................... 1

2 Setup and configuration 3

2.1 Setting up the instruments .................................................. 3

2.2 Configuring ............................................................................ 5

2.2.1 Switching the instrument on and off ........................................ 5

2.2.2 Switching off the instrument .................................................... 6

2.2.3 Display elements and controls .................................................. 6

2.2.4 Setting the dialog language ..................................................... 8

2.2.5 Configuring a new titrant ........................................................ 9

2.2.6 Defining the report output ..................................................... 12

3 Carrying out simple titrations 14

3.1 Creating a titration method ............................................... 14

3.2 Entering user name and sample data ............................... 23

3.3 Carrying out the determination ........................................ 25

3.3.1 Preparing the titration ............................................................ 25

3.3.2 Carrying out the titration ....................................................... 26

3.3.3 Displaying the results ............................................................. 27

3.3.4 Recalculating the determination ............................................. 28

3.3.5 Printing a report manually ...................................................... 30

4 Carrying out an extended titration 31

4.1 Statistics function ............................................................... 31

4.2 Saving the determination and the PC/LIMS report ......... 32

4.3 Modifying the titration parameters .................................. 34

4.4 Saving a method ................................................................. 37

4.5 Creating a sample table ..................................................... 37

4.6 Carrying out titrations ........................................................ 40

4.7 Displaying statistics data ................................................... 41

5 Setting up the user administration 42

5.1 Creating a user list .............................................................. 42

5.2 Automatic login with USB flash drive ............................... 44

5.3 Login with password .......................................................... 46

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

900 Touch Control ￭￭￭￭￭￭￭￭ 1

1 Introduction

The present tutorial helps you to get acquainted with the operation of the

900 Touch Control. You will be guided step by step through the most

important dialog pages by using a simple pH titration as an example.

Thereby you will learn how to efficiently operate and use the 900 Touch

Control.

1.1 Structure of the tutorial

￭Setup

Preparing the titration system.

￭Basics – simple acid-base titration

Loading and carrying out methods, displaying results.

￭Additional functions – creating methods, statistics etc.

Optimizing titration parameters, calculating statistics, efficiently using

the sample table.

￭User administration

User list, login with USB flash drive or password.

Detailed information on the functioning and operation of the Titrando sys-

tem can be found in the online help and the corresponding manuals:

￭Manual for the Titrando

￭Manual for the 900 Touch Control

￭Manual for the exchange unit

￭Manual for the 800 Dosino or the dosing unit

1.2 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-

ond to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

Method Dialog text, parameter in the software

File ▶ New Menu or menu item

[Next] Button or key

1.2 Symbols and conventions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 900 Touch Control

WARNING

This symbol draws attention to a possible life-threat-

ening hazard or risk of injury.

WARNING

This symbol draws attention to a possible hazard due

to electrical current.

WARNING

This symbol draws attention to a possible hazard due

to heat or hot instrument parts.

WARNING

This symbol draws attention to a possible biological

hazard.

CAUTION

This symbol draws attention to possible damage to

instruments or instrument parts.

NOTE

This symbol highlights additional information and

tips.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Setup and configuration

900 Touch Control ￭￭￭￭￭￭￭￭ 3

2 Setup and configuration

2.1 Setting up the instruments

What you will need:

￭A 900 Touch Control

￭A Titrando with internal dosing drive and an 806 Exchange Unit

A Titrando without internal dosing drive, with an 800 Dosino and an

807 Dosing Unit

￭A magnetic stirrer (801 Stirrer), an 803 Ti Stand or an 804 Ti Stand with

propeller stirrer (802 Stirrer)

￭Some sample vessels

￭A pH electrode with connection cable

￭Possibly an additional 805 Dosimat with an exchange unit (e.g. 20 mL)

Possibly an additional 800 Dosino (dosing drive) with a dosing unit (e.g.

20 mL)

￭A bottle with titrant (e.g. caustic soda c(NaOH)=0.1 mol/L)

￭Possibly a printer with connecting cable

￭Possibly a balance with connecting cable

￭Deionized water (carbonate-free)

The manual for the Titrando describes in detail how to install the accesso-

ries. A few notes about this:

Titrant

During this tutorial you will carry out simple titrations. Select an acid or

base as titrant.

Sensor

Use a pH glass electrode for the acid-base titration. Do not forget to plug

the electrode cable into the connector Ind. on the rear of the instrument.

Stirrer

Connect the magnetic stirrer (801 Stirrer) on the rear of the instrument

to the connector MSB 1.

Printer

Select a printer with a USB connector. Use a commercially available USB

cable to connect the printer.

2.1 Setting up the instruments ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

4￭￭￭￭￭￭￭￭ 900 Touch Control

Balance

If you connect a balance to the 900 Touch Control, you can transfer the

sample size per push-button from the balance to the titrator.

800 Dosino

In case you would like to automatically add an auxiliary solution to the

sample before the titration, you will also need a Dosino. Connect it to the

connector MSB 2 on the Titrando.

Samples and sample vessels

You can use sample beakers of any size. Use an acid or base as sample,

which can be titrated with the selected titrant.

Please note that the stirrer has to be connected to the connector MSB 1

of the Titrando for the following example methods. If you use a Titrando

without internal dosing drive, then you must connect the external dosing

device (here: Dosino) to the MSB connector of the stirrer. This way it will

be controlled like an internal dosing drive of the Titrando, i.e. as dosing

device 1.

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