Metrohm 855 Manual de usuario

855 Robotic Titrosampler

Manual

8.855.8001EN / 2020-02-29

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

855 Robotic Titrosampler

Manual

8.855.8001EN / 2020-02-29

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

855 Robotic Titrosampler ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 The 855 Robotic Titrosampler in the Titrando system ...... 1

1.2 Instrument description ......................................................... 2

1.2.1 Model versions ........................................................................ 3

1.2.2 Instrument components ........................................................... 4

1.2.3 Intended use ........................................................................... 4

1.3 About the documentation ................................................... 5

1.3.1 Symbols and conventions ........................................................ 5

1.4 Safety instructions ................................................................ 6

1.4.1 General notes on safety ........................................................... 6

1.4.2 Electrical safety ........................................................................ 6

1.4.3 Tubing and capillary connections ............................................. 7

1.4.4 Personnel safety ....................................................................... 7

1.4.5 Flammable solvents and chemicals ........................................... 9

1.4.6 Recycling and disposal ............................................................. 9

2 Overview of the instrument 10

2.1 Front and rear ..................................................................... 10

2.2 Back panel ........................................................................... 12

2.3 Sensor connectors .............................................................. 12

2.4 Sample racks ....................................................................... 13

3 Installation 15

3.1 Setting up the instrument .................................................. 15

3.1.1 Packaging .............................................................................. 15

3.1.2 Checks .................................................................................. 15

3.1.3 Location ................................................................................ 15

3.2 Preparing the Sample Processor ....................................... 15

3.2.1 Connecting the instrument to the power grid ........................ 15

3.3 Connecting a computer ...................................................... 16

3.4 Connecting the Swing Head .............................................. 18

3.5 Configuring the robotic arm .............................................. 19

3.6 Mounting the robotic arm ................................................. 21

3.7 Robotic arms with beaker sensor ..................................... 23

3.8 Installing the rinsing and aspiration equipment .............. 24

3.9 Placing tubing and cables in the guide chain .................. 27

3.10 Equipping the titration head ............................................. 28

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 855 Robotic Titrosampler

3.11 Connecting the tower stirrer ............................................. 31

3.12 Connecting an external pump ........................................... 32

3.13 Connecting MSB devices .................................................... 33

3.13.1 Connecting a dosing device ................................................... 34

3.13.2 Connecting a stirrer or titration stand .................................... 35

3.13.3 Connecting a Remote Box ..................................................... 36

3.14 Connecting USB devices ..................................................... 37

3.14.1 Connecting a barcode reader ................................................. 37

3.15 Mounting the base plate ................................................... 39

3.16 Mounting the drip pan ....................................................... 40

3.17 Attaching a sample rack .................................................... 41

3.18 Mounting the safety shield ................................................ 42

4 Operation and maintenance 44

4.1 General notes ...................................................................... 44

4.2 Care ...................................................................................... 44

5 Troubleshooting 45

5.1 Sample Processor ............................................................... 45

5.2 Robotic arm ......................................................................... 45

5.3 Pump .................................................................................... 46

6 Appendix 47

6.1 Beaker sensor ..................................................................... 47

6.2 Rinsing nozzles ................................................................... 47

6.3 Remote interface ................................................................ 48

6.3.1 Pin assignment of the remote interfaces ................................ 49

6.4 Stirring rate ......................................................................... 50

6.5 Robotic arms ....................................................................... 51

6.5.1 Robotic arms for titration ....................................................... 51

6.5.2 Robotic arms for sample preparation ..................................... 53

6.5.3 Robotic arms for special applications ..................................... 54

7 Technical specifications 55

7.1 Measuring interface ........................................................... 55

7.1.1 Potentiometry ........................................................................ 55

7.1.2 Polarizer ................................................................................ 55

7.1.3 Temperature .......................................................................... 56

7.2 Lift and turntable ............................................................... 56

7.3 Membrane pump(s) with valve .......................................... 57

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

855 Robotic Titrosampler ￭￭￭￭￭￭￭￭ V

7.4 786 Swing Head ................................................................. 57

7.5 Interfaces and connectors ................................................. 57

7.6 Power connection ............................................................... 58

7.7 Ambient temperature ......................................................... 58

7.8 Reference conditions .......................................................... 58

7.9 Dimensions .......................................................................... 58

8 Accessories 59

Index 60

Table of figures ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

VI ￭￭￭￭￭￭￭￭ 855 Robotic Titrosampler

Table of figures

Figure 1 The Titrando system .......................................................................... 1

Figure 2 Front 855 Robotic Titrosampler ....................................................... 10

Figure 3 Rear 855 Robotic Titrosampler ......................................................... 11

Figure 4 Connector strip ............................................................................... 12

Figure 5 Sensor connectors ........................................................................... 13

Figure 6 Sample rack 6.2041.840 ................................................................. 13

Figure 7 Connecting the computer ................................................................ 17

Figure 8 Connecting the Swing Head ............................................................ 18

Figure 9 Robotic arms - standard model versions: .......................................... 19

Figure 10 Configuration data of the robotic arms ............................................ 20

Figure 11 Limitation screw on the robotic arm ................................................ 21

Figure 12 Mounting the robotic arm ............................................................... 22

Figure 13 Connecting a beaker sensor (for example 6.1462.150) .................... 23

Figure 14 Mounting the rinsing and aspiration tubings .................................... 24

Figure 15 Installing the rinsing tubings and the aspiration tip .......................... 29

Figure 16 Installing stirrer and electrode .......................................................... 30

Figure 17 Rod stirrer 802 Stirrer ...................................................................... 31

Figure 18 Magnetic stirrer 741 Stirrer .............................................................. 31

Figure 19 Connecting the tower stirrer ............................................................ 31

Figure 20 Connecting a pump ......................................................................... 32

Figure 21 MSB connections ............................................................................ 33

Figure 22 Connecting a dosing device ............................................................. 35

Figure 23 Connecting an MSB stirrer ............................................................... 35

Figure 24 Connecting the rod stirrer to the titration stand ............................... 36

Figure 25 Connecting the Remote Box ............................................................ 37

Figure 26 USB connectors ............................................................................... 38

Figure 27 Mounting the base plate ................................................................. 39

Figure 28 Installing the drip pan ...................................................................... 40

Figure 29 Attaching rack ................................................................................. 41

Figure 30 Mounting the safety shield .............................................................. 42

Figure 31 Beaker sensor on the tower ............................................................. 47

Figure 32 Spray nozzles - Mode of operation .................................................. 48

Figure 33 Connectors of the Remote Box ........................................................ 48

Figure 34 Pin assignment of remote socket and remote plug ........................... 49

Figure 35 Rotational speed depending on the stirring rate ............................... 50

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

855 Robotic Titrosampler ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 The 855 Robotic Titrosampler in the Titrando sys-

tem

The 855 Robotic Titrosampler is a component of the modular Titrando sys-

tem. Operation is carried out either by a Touch Control with a touch-sensi-

tive screen ("stand-alone titrator") or by a computer with a corresponding

software.

A Titrando system can contain numerous, various kinds of instruments.

The following figure provides an overview of the peripheral devices you

can connect to the 855 Robotic Titrosampler.

MSB

USB

Controller

PC Keyboard

Barcode

Reader

USB Hub

RS-232/USB Box

Balance

Touch Control

USB Sample Processor

Robotic Titrosampler

Printer

Bluetooth USB

Adapter

Personal Computer

Relay Box

Remote Box

Dosing Interface

Stirrer / Ti Stand Dosino Dosimat

Status

805

Titrando

pH Module

Conductivity Module

Figure 1 The Titrando system

1.2 Instrument description ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 855 Robotic Titrosampler

Up to three control instruments (Titrando, Dosing Interface, USB Sample

Processor, etc.) can be controlled via USB connection during operation

with the 900 Touch Control. If the tiamo software is used, then there is no

limit to the number of control instruments that can be used to extend the

system.

Updating the device software is described in the manual for the Touch

Control or in the online help for the tiamo software.

1.2 Instrument description

The 855 Robotic Titrosampler is a combined analyzer, unifying the func-

tionality of a titrator and a sample changer. It can be seamlessly incorpora-

ted as a system component and control instrument into a Metrohm

Titrando system.

The 855 Robotic Titrosampler is a versatile instrument. It has been

designed exclusively for usage in factories, as long as ambient conditions

(see chapter 7.7, page 58) are fulfilled, and laboratories and thereby cov-

ers a wide range of applications.

Thanks to the integration of high-performance USB interfaces, it can be

incorporated seamlessly into a Metrohm Titrando system. The versatile

communications options of the Titrando system (Remote Box, LIMS link,

etc.) can thus all be used. Thanks to these abilities, a 855 Robotic Titro-

sampler is predetermined for all kind of automation tasks in a modern lab-

oratory, especially for highly integrated laboratory data systems.

The user interface of the Touch Control or the tiamo software guarantees

comfortable operation and programming of the 855 Robotic Titrosampler.

The comprehensive range of commands and the various configuration

possibilities can comfortably and efficiently be used this way. The integra-

tion into the Titrando system also guarantees a 100% conformity of the

complete automation system with the FDA regulations (Food and Drug

Administration), especially with the regulation 21 CFR part 11, electronic

records and signatures.

There are exchangeable standard sample racks available for many vessel

dimensions. Freely selectable special beaker positions can be defined for

e.g. rinsing or conditioning beakers on every rack.

The equipment with a 786 Swing Head allows to process a large number

of samples in one single sample series. The robotic arms for the 786

Swing Head make it possible to move to any given point on a sample rack.

This way the number (a maximum of 999 rack positions) and sequencing

of the samples is almost unlimited.

Customer-specific special racks for individual requirements can be fabrica-

ted upon request.

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