Agilent Technologies Cary 60 Manual de usuario

Agilent Cary 60 Spectrophotometer

User’s Guide

2 Agilent Cary 60 Spectrophotometer User’s Guide

Notices

Manual Part Number

G6860-90001

Edition 5, March 2019

2014-2016, 2019

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Agilent Technologies Australia (M)

Pty Ltd

679 Springvale Road

Mulgrave, Victoria 3170 Australia

www.agilent.com

Instrument Manufacturing

Manufactured by Agilent Technologies

Bayan Lepas Free Industrial Zone,

Penang, PG, 11900, MY

Printed in USA

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to the

maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein, including

but not limited to the implied

warranties of merchantability and

fitness for a particular purpose. Agilent

shall not be liable for errors or for

incidental or consequential damages in

connection with the furnishing, use, or

performance of this document or of

any information contained herein.

Should Agilent and the user have a

separate written agreement with

warranty terms covering the material in

this document that conflict with these

terms, the warranty terms in the

separate agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance with

the terms of such license.

Restricted Rights Legend

If software is for use in the

performance of a U.S. Government

prime contract or subcontract,

Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

defined in FAR 2.101(a) or as

“Restricted computer software” as

defined in FAR 52.227-19 (June 1987)

or any equivalent agency regulation or

contract clause. Use, duplication or

disclosure of Software is subject to

Agilent Technologies’ standard

commercial license terms, and non-

DOD Departments and Agencies of the

U.S. Government will receive no

greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard. It

calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indicated

conditions are fully understood and

met.

CAUTION

WARNING

Contents

Agilent Cary 60 Spectrophotometer User’s Guide 3

Contents

1General Information 7

User Documentation 7

Conventions 8

Notes and Tips 8

Verifying Safe State 8

Lamp Module 9

Modules, Covers and Panels 9

Other Precautions 9

Warning and Other Symbols 10

CE Compliance 11

Electromagnetic Compatibility 12

ICES/NMB-001 13

South Korean Class A EMC declaration 13

2Specifications 15

Measurement Category 15

Pollution Degree 15

Environmental Conditions 15

Weights and Dimensions 16

Electrical Specifications 17

Mains Supply 17

Computer Requirements 18

3Installation 19

Installation 19

Contents

4 Agilent Cary 60 Spectrophotometer User’s Guide

Unpacking 20

Installing the Cary WinUV Software 21

Installing the Hardware 22

Registering and Validating Your Cary 60 22

Running the Tutorials 23

Cell Holder 24

Installation 24

Alignment 25

Other Sample Holders 26

Installing Accessories 26

4Introduction 27

Instrument Overview 27

Indicator Lamp 27

Connections 28

Using the Software 28

5Troubleshooting 29

Access Denied 29

Problem 29

Solution 29

No Green Light Indicating that the Cary 60 is Powered 30

Problem 30

Solution 30

Start Button Replaced with Connect Button 30

Problem 1 30

Solution 31

Problem 2 31

Contents

Agilent Cary 60 Spectrophotometer User’s Guide 5

Solution 31

Absorbance is 10 Abs and Fluctuates Wildly During a Scan 32

Problem 32

Solution 32

Instrument Performance Testing 33

Problem 33

Solution 33

Wavelength Calibration 33

Problem 33

Solution 34

Front Panel LED Troubleshooting 34

LED Won’t Light Up 34

Solid Red LED 34

Flashing Red LED 34

6Maintenance and Spare Parts 35

Maintenance 35

Spare Parts 35

Contents

6 Agilent Cary 60 Spectrophotometer User’s Guide

This page is intentionally left blank.

General Information

Agilent Cary 60 Spectrophotometer User’s Guide 7

1General Information

User Documentation 7

Lamp Module 9

Modules, Covers and Panels 9

Other Precautions 9

Warning and Other Symbols 10

CE Compliance 11

Your Agilent instrument and accessories have been carefully designed so that

when used properly you have an accurate, fast, flexible and safe analytical system.

Information about safety practices appears throughout the documentation (both

hard copy and online) provided with your instrument and accessories to help you

safely operate the instrument and accessories. Before using the instrument or

accessories, you must thoroughly read these safety practices. ALWAYS operate

the instrument and accessories in accordance with these safety practices.

User Documentation

You have been provided with the following documentation to help you set up and

operate your Agilent Cary 60 spectrophotometer:

•Cary 60 Installation Card, with information on unpacking the instrument and

setting up the system.

•This manual, with safety practices and hazards information, instructions for

installing and maintaining the components of the Cary 60, and troubleshooting

information.

•Cary Tutorials which provide step-by-step instructions for installing selected

accessories and programming applications.

•Extensive Help (in English only) provided with the Cary WinUV software

containing context-sensitive Help, step-by-step instructions for frequently

performed analyses and instructions for using any accessories you ordered.

General Information

8 Agilent Cary 60 Spectrophotometer User’s Guide

Conventions

The following conventions have been used throughout the documentation:

•Menus, menu items, buttons and check boxes have been typed in bold. For

example, ‘click OK’ and ‘From the Edit menu, choose Copy’.

•ALL CAPITALS indicate keyboard commands. For example, ‘Press ENTER’ and

‘Press SHIFT+F3’.

NOTE Throughout this manual, UV Dissolution and UV Fiber Optic Dissolution users

should replace “Cary WinUV Software” with “UV Dissolution Software” or “UV Fiber

Optic Dissolution Software” respectively.

Notes and Tips

A Note is used to give advice or information.

A Tip is used to give practical hints to help you achieve the best possible

performance from your instrument.

Verifying Safe State

The following general safety precautions must be observed during all phases of

operation, maintenance and service of this instrument.

To ensure continued safety of the instrument after maintenance or service

procedures verify the instrument is returned to a safe state for the user. This

includes running performance checks to verify the instruments safety systems are

functioning correctly. Check the general condition of the instrument during

operation for wear or signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings elsewhere in

this manual violates safety standards of design, manufacture, and intended use of

the instrument. Agilent Technologies assumes no liability for the customer’s

failure to comply with these requirements.

General Information

Agilent Cary 60 Spectrophotometer User’s Guide 9

Lamp Module

The lamp is enclosed in a self-contained module. This module contains

components operating at high voltages. To avoid electric shock, NEVER

disassemble the module.

When operating, the lamp module emits high intensity light that can cause serious

damage to eyes. To avoid eye damage, never operate the lamp outside the

instrument.

Modules Covers and Panels

The Cary 60 spectrophotometer module that operators and other personnel will

routinely access is the sample compartment module.

The only other cover and panel that is customer accessible is the main cover and

lamp module and is to be removed ONLY when changing the lamp module and

aligning it. Consult the Cary WinUV Help for instructions and safety information.

Any other panels or covers that are retained by screws on the spectrophotometer

and accessories may be opened ONLY by Agilent service engineers.

Other Precautions

Do not block any ventilation grills present on the computer. Consult the manuals

supplied with your PC, monitor and printer/plotter for their specific ventilation

requirements.

Allow at least 50 mm (2 in.) of space on the sides, and 150 mm (6 in) at the rear of

the system to permit free air circulation.

Use of the Cary 60 system and accessories may involve materials, solvents and

solutions that are flammable, corrosive, toxic or otherwise hazardous.

Careless, improper, or unskilled use of such materials, solvents and solutions can

create explosion hazards, fire hazards, toxicity and other hazards which can result

in death, serious personal injury, and damage to equipment and property.

General Information

10 Agilent Cary 60 Spectrophotometer User’s Guide

ALWAYS ensure that laboratory safety practices governing the use, handling and

disposal of such materials are strictly observed. These safety practices should

include the wearing of appropriate safety clothing and safety glasses.

Warning and Other Symbols

The following is a list of symbols that appear in conjunction with warnings on the

spectrophotometer. The hazard they describe is also shown.

A triangular symbol indicates a warning. The meanings of the symbols that may

appear alongside warnings in the documentation or on the instrument itself are as

follows.

Electrical shock

Eye hazard

Heavy weight

(danger to feet)

Heavy weight

(danger to hands)

The following symbol may be used on warning labels attached to the instrument.

When you see this symbol, refer to the relevant operation or service manual for the

correct procedure referred to by that warning label.

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