Agilent Technologies Intuvo 9000 Hoja de instrucciones

Agilent Technologies

Agilent Intuvo 9000

Gas Chromatograph

Installation and First Startup

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or

translation into a foreign language)

without prior agreement and written

consent from Agilent Technologies, Inc. as

governed by United States and

international copyright laws.

Manual Part Number

G4580-90008

Edition

Fifth edition, July 2019

Fourth edition, February 2018

Third edition, September 2017

Second edition, February 2017

First edition, September 2016

Printed in USA

Agilent Technologies, Inc.

2850 Centerville Road

Wilmington, DE 19808-1610 USA

安捷伦科技（上海）有限公司

上海市浦东新区外高桥保税区

英伦路 412 号

联系电话：（800）820 3278

Warranty

The material contained in this document is

provided “as is,” and is subject to being

changed, without notice, in future editions.

Further, to the maximum extent permitted

by applicable law, Agilent disclaims all

warranties, either express or implied, with

regard to this manual and any information

contained herein, including but not limited

to the implied warranties of

merchantability and fitness for a particular

purpose. Agilent shall not be liable for

errors or for incidental or consequential

damages in connection with the

furnishing, use, or performance of this

document or of any information contained

herein. Should Agilent and the user have a

separate written agreement with warranty

terms covering the material in this

document that conflict with these terms,

the warranty terms in the separate

agreement shall control.

Safety Notices

CAUTION

A CAUTION notice denotes a hazard. It

calls attention to an operating proce-

dure, practice, or the like that, if not

correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not pro-

ceed beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a hazard.

It calls attention to an operating pro-

cedure, practice, or the like that, if

not correctly performed or adhered

to, could result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indicated

conditions are fully understood and

met.

Agilent Intuvo 9000 GC Installation 3

Contents

1 Installing the GC

Overview of Installation 8

Purpose of this procedure 8

Customer responsibilities 8

About Agilent’s installation service 8

Tools and additional parts required 9

Performing checkout 9

System installation 10

Ship kit contents 10

The Intuvo 9000 GC 11

Unpacking 12

Place the GC on the bench. 13

Verify line voltage and power cord. 15

Power consumption 15

Power cords available 15

Grounding 18

If purchased, install the ALS tray support brackets. 19

Intuvo 9000 7693A Tray Support Assembly kit contents 19

Install the pivot block and stop bracket 19

Connect the power cord and LAN cable. 26

Turn on the GC. 27

View the feature tour. 28

View the System Setup wizard. 30

Set the system time zone, date, time, and pressure units. 31

Configure the GC IP address. 32

Configure the 5977B MS 34

Configure another MS type 35

Prepare the GC. 36

Configure gases and detector-specific settings. 40

Connect to the GC and view the complete installation guide. 41

Prepare gas supplies. 42

Install the gas regulators 42

Connect tubing to gas supplies and purge. 45

Connect the tubing to the gas source 45

4Agilent Intuvo 9000 GC Installation

Install filters and traps, then purge. 46

Install traps 46

Connect gases to the GC. 47

Plumb to EPC flow modules 47

Leak test all connections and set source pressures. 49

Vent hazardous gases to a fume hood. 51

Install FID vent chimney 51

Connect cryogenic cooling (if present). 53

Connecting liquid carbon dioxide 53

Connecting liquid nitrogen 54

Connecting air to the multimode inlet 56

Connect valve actuator air (if present). 58

Connect the external cables. 59

Back panel connectors 59

Connecting cables 61

Labeling BCD and EVENT cables 61

GC / MS / Agilent data system / ALS 62

Additional cabling configurations 62

Install ALS, if available. 63

Install tray bracket onto the tray (7693A only) 63

Install the tray on the GC (7693A only) 65

Install the injector 66

Configure the ALS 67

Calibrate the tray, if installed 68

Prepare the ALS for checkout 69

Install the Intuvo chips and column. 70

Remove the packing materials 71

Install the Intuvo inlet chip and Guard chip 73

Install a new column gasket 78

Install the checkout column 80

Condition the column and bake out the detector. 85

Transfer the checkout sample to a screw-top sample vial. 86

Enter the checkout method. 87

Run one injection. 88

Evaluate Results. 89

Prepare for the next analysis. 90

If appropriate, update firmware. 91

GC firmware 91

Agilent Intuvo 9000 GC Installation 5

A Making Swagelok Connections

Making Swagelok Connections 94

Using a Swagelok Tee 97

B Cabling Diagrams and Remote Start/Stop

Using the Remote Start/Stop Cable 100

Connecting Agilent products 100

Connecting non-Agilent products 100

Multi-instrument Cabling Examples 103

GC / ALS / Non-Agilent Data System 103

Using a Y-Cable in a setup (GC/MSD/Data System/Headspace

Sampler) 104

GC / External Events (unspecified, non-Agilent instrument) 104

Cable Diagrams 106

Analog signal cable, general use, G1530-60560 106

Agilent analog signal cable, G1530-60570 106

Remote start/stop cable, general use, 35900-60670 107

Agilent APG remote start/stop cable, 03396-61010 108

Agilent APG remote start/stop cable, G1530-60930 108

Agilent remote start/stop Y-cable, G1530-61200 109

BCD cable, G1530-60590 109

BCD cable, G1530-61100 110

External event cable, G1530-60590 112

External valve cable, G1580-60710 113

6Agilent Intuvo 9000 GC Installation

Agilent Intuvo 9000 Gas Chromatograph

Installation and First Startup

Agilent Technologies

Installing the GC

This section contains installation procedures for the Agilent

Intuvo 9000 GC. Some of the steps in this procedure are

optional based on your installed components, such as plumbing

cryogenic cooling or valve actuator air.

Instructions for connecting cables from the GC to other

instruments in a typical Intuvo 9000 system are included here

and in Appendix B, “Cable Diagrams."

8Agilent Intuvo 9000 GC Installation

1Installing the GC

Overview of Installation

Before installing the GC, read the important safety information

in the Agilent Intuvo 9000 Gas Chromatograph Safety

Information manual (provided with the GC) and the Safety

manual (available from the Agilent GC and GC/MS User

Manuals & Tools DVDs).

Purpose of this procedure

This procedure ensures that instruments and systems are

installed and functioning as designed. Correct installation is the

first step in ensuring that instruments and systems operate

reliably over their lifetimes.

Customer responsibilities

1Make sure your site meets the basic requirements, including

the necessary space, electrical outlets, gases, tubing,

operating supplies, consumables and other usage-dependent

items required for a successful installation. Refer to the

Agilent Intuvo 9000 GC, GC/MS, and ALS Site Preparation

Guide.

2If Agilent is delivering installation and familiarization

services, users of the instrument should be present

throughout these services; otherwise, these users will miss

important operational, maintenance, and safety information.

Additional information is available via the GC Touchscreen,

Browser Interface help & information suite, and the Agilent GC

and GC/MS User Manuals & Tools DVDs and through the

instrument’s website.

Once the GC is turned on, open a browser and connect to the

instrument's help and information system.

If your site complies with all site preparation specifications, the

average installation time for the GC is about 2 hours. Allow

more time for any additional products (for example, an ALS),

add-ons, and software.

About Agilent’s installation service

The installation service does not include:

•Network setup with other computers or to the site or

building LAN.

Installing the GC 1

Agilent Intuvo 9000 GC Installation 9

•Customization of the system.

•Method development and testing.

•Analysis of customer standards or samples.

•Testing against the instrument performance specification.

(Operational qualification and performance verification

services, OQ/PV, can be purchased separately.)

If you need assistance beyond this installation service, please

contact your local Agilent Technologies office. Assistance with

installation and with user-specific services and applications is

available and will be contracted separately.

Tools and additional parts required

Installation requires the following tools, fittings, and hardware.

These items are not included with the instrument.

•Precleaned copper tubing, 1/8-inch or 1/4-inch od.

•Fittings.

•Tubing cutter.

•Filters for gas supplies.

•7/16-inch and 9/16-inch open-end wrenches for assembling

Swagelok fittings.

•Carrier and other gas supplies.

•Pressure regulator for each gas supply.

•A computer, tablet, or other LAN-capable device (for

accessing GC user information and for firmware updates).

•Any additional LAN components, such as cables and a switch

or hub, for connection to the site LAN (not included in

Agilent installation services).

The Agilent Intuvo 9000 GC, GC/MS, and ALS Site Preparation

Guide contains a listing of Agilent installation kits and a

description of parts included with each. These kits contain

filters, fittings, tubing, tools (wrenches, tubing cutter, drivers,

and so on), and other required parts for installing a GC.)

Performing checkout

If using an Agilent data system, you can use it to perform the

checkout procedure. Read these GC installation instructions

and the instructions for installing the data system.

10 Agilent Intuvo 9000 GC Installation

1Installing the GC

System installation

If installing an ALS, the ALS can be used for checkout. Also

refer to the ALS installation documentation.

When installed as part of a complete system including an

Agilent data system, first install the GC up to the checkout step.

Configure the new GC in the data system and open an online

instrument session. Use the data system to perform the

checkout test.

When installed as part of other complete systems, for example

in an Agilent GC/MSD or GC/MS system, see the installation

instructions for that system.

Ship kit contents

Several ship kits will arrive with the GC. Most parts needed for

installation will be found in the 9000 GC System Ship Kit. Ship

kits for the ordered inlet and detector will include the inlet- and

detector-specific parts needed for checkout and maintenance,

for example, the inlet checkout liner, inlet wrench, septa,

detector checkout sample, and typical cleaning tools (varies by

inlet and detector type).

Syringe and plunger button, for manual injection

1/8-in Nut and ferrule set, brass, 10/pk

Certified vial sample pack

LAN cable

Intuvo Torque Driver handle and extension

Torx keys, T10 and T20

Gas line ID labels

Agilent Intuvo 9000 Gas Chromatograph Safety Information manual

MSD Cover insert assembly

Intuvo inlet chip, G4581-60031

Bus front door assembly, G4581-60207

Compression bolts (2), G4581-60260

Intuvo gaskets, polyimide, 2/pk

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