Agilent Technologies G1701DA Manual de usuario

Agilent Technologies

Agilent G1701DA

MSD ChemStation

5973 MSD / ChemStation

Quick Reference

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What’s New in Revision D.01.00

• A new toolbar has been added to the Top view

and an expanded set of toolbars have been

added to Data Analysis. Moving the cursor of

the mouse over a toolbar will display tool tips

(quick descriptions) for each of the buttons.

• The sequence user interface or sample log

table has been transformed into a

spreadsheet user interface.

• During sequencing the ABORT button in the

status panel has been changed to Pause.

When this is selected, the sequence will pause

immediately. When thesequenceis started,it

will restart the sequence from where it was

paused.

• Long files names are supported. Data file and

method paths can be up to 100 characters

long. The names of individual data files and

methods can be up to 50 characters long.

• User Interfaces for selecting or saving files

and directories have been enhanced with

browse buttons.

• Support for 5973A and 6890A instruments

using GPIB has been restored.

• It is now possible to disable Method

Resolution for most changes in the 6890

configuration.

• The Manual Tune and Diagnostics / Vacuum

Control views have be merged into a single

view, Tune and Vacuum Control.

• A Tune Wizard has been provided to simplify

the modification of criteria (tune limits,

target ratios) used by the tuning algorithms.

• Loading data files in Data Analysis will now

preview the chromatogram.

• The method has been expanded to permit

printers other than the default printer to be

used for reports generated during Run

Method.

• Headers in Data Analysis reports are now

configurable for the reports generated by Run

Method.

• An improved BOOTP service has replaced the

previous BOOTP program. The new BOOTP

service will not interfere with shutting down or

logging off the computer.

• The SICL drivers have been updated to version

L.02.01 . Version M.01.01 is on the software

CD and is for GPIB support.

Use the online help to learn about these

new features as well as to learn about

instrumentcontrol,dataacquisition,data

analysis,methods,sequencing,tuning,and

how to use system commands and

variables. Troubleshooting the MSD is

included to help you diagnose problems.

Online Help

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Using Online Help

To access the online help, select Help

Topics from the Help menu in any

window, or click the Help button on any

dialog box.

Item Description

Hide / Show Lets you turn on or off the

display of the list of help

topics.

Back Goes back to the previous help

topic.

Print Lets you print the current book

or help topic.

Contents Displays the list of help topics

(shown above).

Index Lets you use keywords to

search the help index for a

particular topic.

Search Lets you type a word or phrase

and then displays a list of all

the topics in the online help

that contain those words. Indicates a book containing more help topics.

To open a book, select it then double-click.

Indicates an open book of help topics. To close

an open book, select it then double-click.

Indicates a help topic. To jump to a help topic,

select it then double-click.

Help Icons

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5973 MSD with a 6890 GC

Column oven

5973 MSD

Status display

6890 GC

Keypad

Status board

ALS tower

On/off switch

Local control

panel

ALS tray

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GC Keypad

The MSD ChemStation software provides instrument control for the 6890 GC. This allows you to use

the software, instead of the GC keypad, to program the instrument. However, there are times when you

may want to use the keypad to quickly perform one of the following tasks.

Stop a run

Display column information Prepare a run (manual injection)

Start a run (manual injection)

Display the oven

temperature

Display the GC/MSD

interface temperature

(Thermal Aux 2)

Display the front injection

port temperature

Display the rear injection

port temperature

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Instrument Control View

Acquisition Status Lets you tell at a glance the status of the current

instrument or run (if any).

Start Button Lets you start a run. When a run is not in progress, the

arrow is green. To start a run, click the green arrow, fill in the Sample

Information, and click Start Run. When a run is in progress, the arrow

is gray.

This button also shows the current data file name, sample information

(if any), and the vial number (1 if no ALS).

See the online help for more details

on the menus, buttons, or windows

used in the software.

The Instrument Control view is displayed when you start up

the MSD ChemStation. This is where you set and monitor

instrument parameters. If you are in a different view, select

View / Instrument Control when you are ready to set up the

system for data acquisition.

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Run Time Clock Shows the elapsed time since the beginning of the

run if a run is in progress. The scheduled run time is shown below

the digital clock. When a run is not in progress, the Run Time clock

shows the elapsed time since the last run.

Stop Button Lets you stop the system when it is in Pre-Run,

Run, or Post-Run mode. The stop sign is red when a run is in

progress and gray when a run is not in progress.

Logbook Button Displays a menu where you can choose to view,

open, clear, save, or print a particular logbook.

Help Button Displays a menu where you can select an online help

topic for the Instrument Control view. Choose Help Topics to go to

the online help for the entire system.

Injector Button Lets you set parameters for the injector when

you have configured your system with an ALS.

Inlets Button Lets you set parameters for the GC inlet (injection

port) that is configured on your system.

Columns Button Lets you configure columns and set up ramped

flow and pressure programs.

Oven Button Displays a menu that lets you edit GC oven

parameters or GC monitor parameters. When the GC is ready, the

small square in the upper right corner is green. When the GC is not

ready, the square is red.

Aux Button Lets you set the temperature of the GC/MSD

interface (usually Thermal Aux 2).

MS Button Displays a menu that lets you edit MS acquisition

parameters, select another tune file, or edit MS monitors.

Monitor Each monitor displays one instrument parameter. See

the online help for a description of the instrument monitors.

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Top Menus

Sequence

Run...

Load...

Save...

Edit Sample Log Table...

Load and Run Sequence...

Print Sequence...

Simulate Sequence

Position and Run...

View Sequence Log...

View Sequence Quality Log

Print Sequence Log

Import Sequence Information from CSV file...

Batch Mode...

More...

Method

Run...

Load...

Save...

Edit Entire Method...

Set New Default Paths...

Exit

Secured Control

Enable Security...

Start Secured Control...

Select Methods for Secured Control...

Set/Change Startup Method <...>

Set Change Standby Method <...>

Assign Sample Names to Method...

Use Sample-centric Secured Control...

Report Manager password...

Edit Accounts...

View

Help

Help Topics

Using Help

View Revision Readme File

Review Revision History...

About

Top

Instrument Control

Data Analysis (offline)

Select View / Top to access

these menus.

The software menus shown on the following

pages are for an MSD ChemStation in

Enhanced Mode.

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Top Toolbar

Load Sequence Loads the selected sequence.

Save Sequence Saves the specified sequence.

Run Sequence Saves the specified sequence.

Edit Sequence Lets you set up or modify the sample log

table.

Print Sequence Prints the current sequence.

Simulate Sequence Simulates the current sequence.

Load Method Loads the selected method.

Save Method Saves the specified method.

Run Method Runs the current method. The Start Run

dialog box is displayed.

Edit Method Lets you modify the method parameters

for the current method.

Print Method Prints the current method.

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Instrument Control Menus

Method

Run...

Load...

Save...

Edit Entire Method...

Additional Method Information...

Exit

Abort

View

Top

Instrument Control

Data Analysis (offline)

Tune and Vacuum Control...

Instrument

Inlet/Injection Types

GC Edit Parameters...

GC Plot...

GC Monitors...

Acquire RTLock Calibration Data...

Unlock Method...

Disable Method Resolution

Select MS Tune File...

MS SIM/Scan Parameters...

Change MSD Temperatures...

MS Monitors...

Edit MS Tune Parameters...

Perform MS Autotune...

EMF Utilities...

Select View / Instrument Control to

access these menus.

Window

Cascade

Tile Horizontal

Tile Vertical

Arrange Icons

Arrange Plots and Monitors

Qualify

Checkout Tune

Tune Evaluation

View Tunes...

Sensitivity Check

Software Validation

Installation Checklist

Familiarization Checklist

Help

Help Topics

Using Help

Review Revision History...

View Revision Readme File

About

73NQuickReference.fm Page 10 Tuesday, August 12, 2003 1:26 PM

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