Agilent Technologies 7820A Manual de usuario
Agilent Technologies
Agilent 7820A
Gas Chromatograph
Operating Guide
Notices
© Agilent Technologies, Inc. 2011
No part of this manual may be reproduced
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laws.
Manual Part Number
G4350-90012
Edition
Third edition, June 2011
Second edition, October 2009
First edition, March 2009
Printed in China
Agilent Technologies, Inc.
412 Ying Lun Road
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Safety Notices
CAUTION
A CAUTION notice denotes a hazard. It
calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION notice
until the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a hazard.
It calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in personal injury or
death. Do not proceed beyond a
WARNING notice until the indicated
conditions are fully understood and
met.
Operating Guide 3
Contents
1 Introduction
Where to Find Information 8
Online User Documentation 8
Agilent Customer Portal 9
Chromatography Using a GC 10
The Front View of the Agilent 7820A GC 11
The Back View of the Agilent 7820A GC 12
The Inlets 13
The GC Column and Oven 15
Detectors 16
The Operating Panel 17
The display 17
Indicator Lights 17
Alert Tones 18
The keypad 19
2 Operating Basics
Overview 22
Instrument Control 23
Correcting Problems 24
To Start Up the GC 25
To Shut Down the GC for Less Than a Week 26
To Shut Down the GC for More Than a Week 27
3 Software Keypad Operation
To Install the Software Keypad 30
The Software Keypad 31
To connect to a GC 31
To disconnect from a GC 32
Other program settings 32
To minimize or expand the software keypad 33
To troubleshoot a connection 33
To get help 34
The Run Keys 35
The Service Mode Key 35
4Operating Guide
The GC Component Keys 36
The Status Key 37
The Info Key 38
The General Data Entry Keys 39
The Supporting Keys 40
Method Storage and Automation Keys 41
Keypad Functionality When the GC Is Controlled by an Agilent Data
System 42
About GC Status in the Software Keypad 43
Indicators 43
Error conditions 43
Blinking setpoint 44
About Logs 45
4 Running a Method or a Sequence from the Software Keypad
Loading, Storing, and Running Methods from the Software Keypad 48
To load a method 48
To store a method 48
To manually inject a sample with a syringe and start a run 48
To run a method to process a single ALS sample 48
To abort a method 49
Loading, Storing, and Running Sequences from the Software Keypad 50
To load a sequence 50
To store a sequence 50
To start running a sequence 50
To pause a running sequence 51
To resume a paused sequence 51
To stop a running sequence 51
To resume a stopped sequence 51
Aborting a sequence 51
To resume an aborted sequence 52
5 About Methods, Sequences, and Data Analysis
What Is a Method? 54
What Is Saved in a Method? 54
What Happens When You Load a Method? 55
What Is a Sequence? 55
Automating Data Analysis, Method Development, and Sequence
Development 55
6Operating Guide
7
Agilent 7820AGas Chromatograph
Operating Guide
Agilent Technologies
1
Introduction
Where to Find Information 8
Chromatography Using a GC 10
The Front View of the Agilent 7820A GC 11
The Back View of the Agilent 7820A GC 12
The Inlets 13
The GC Column and Oven 15
Detectors 16
The Operating Panel 17
This document provides an overview of the individual
components that make up the Agilent 7820A Gas
Chromatograph (GC).
8Operating Guide
1Introduction
Where to Find Information
In addition to this document, Agilent provides several
learning products that document how to install, operate,
maintain, and troubleshoot the Agilent 7820A GC.
Before operating your GC, be sure to read the safety and
regulatory information included on the Agilent GC and
GC/MS Hardware User Information & Utilities DVD. The
most common safety hazards when working on the GC are:
•Burns caused by touching heated areas on or in the GC
•Release of pressurized gas containing hazardous chemical
compounds caused by opening inlets
•Glass cuts or puncture wounds caused by sharp capillary
column ends
•Use of hydrogen as a GC carrier gas
Online User Documentation
Now your Agilent instrument documentation is in one place,
at your fingertips.
The Agilent GC and GC/MS Hardware User Information &
Utilities DVD that ships with your instrument provides an
extensive collection of online help, videos, and books for
current Agilent gas chromatographs, mass selective detectors,
and GC samplers. Included are localized versions of the
information you need most, such as:
•Getting Familiar documentation
•Safety and Regulatory guide
•Site Preparation information
•Installation information
Introduction 1
Operating Guide 9
•Operating guides
•Maintenance information
•Troubleshooting details
Agilent Customer Portal
Agilent also provides customized information for the
products you own through a customer portal. This web
service provides many customizable services as well as
information related directly to your Agilent products and
orders. Log onto the portal at http://www.agilent.com/chem.
10 Operating Guide
1Introduction
Chromatography Using a GC
Chromatography is the separation of a mixture of
compounds into individual components.
There are three major steps involved with separating and
identifying components of a mixture using a GC. They are:
1Injecting a sample into the GC. (This takes place at the
inlet.)
2Separating the sample into individual components. (This
takes place inside the column in the oven.)
3Detecting what compounds were in the sample. (This is
done in the detector.)
During this process, status messages from the Agilent 7820A
GC are displayed, and user changes to parameter settings
can be made through the software keypad.
Each part of this process is described in brief on the
following pages of this document. Refer to the Advanced
User Guide for more details.
Inlet
Detector
Oven
Operating panel
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