Agilent Technologies 1200 series Manual de usuario

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Agilent 1200 Series

Vacuum Degasser

Reference Manual

2 1200 Series VD Reference Manual

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1322-90010

Edition

Edition 02/06

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn, Germany

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

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to federal government customers include

only those rights customarily provided to

end user Customers of Software. Agilent

provides this customary commercial license

in Software and technical data pursuant to

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(Computer Software) and, for Department of

Defense purchases, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commercial

Computer Software or Computer Software

Documentation). If a federal government or

other public sector Customer has a need for

rights not conveyed under these terms, it

must negotiate with Agilent to establish

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Safety Notices

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTION notice until the indicated

conditions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

1200 Series VD Reference Manual 3

In This Guide…

1 Installing the Vacuum Degasser

How to install the vacuum degasser

2 Optimizing Performance

How to optimize the vacuum degasser to achieve best

chromatographic results

3Troubleshooting

Errors, their probable cause, and the action required to correct

them

4 Repairing the Vacuum Degasser

Instructions on how to repair the vacuum degasser

5 Parts and Materials

Detailed illustrations and listings for parts and materials

identification

6 Theory of Operation

The vacuum degasser’s operation and electronics

7 Specifications

Performance specifications of the vacuum degasser

A Appendix

Safety Information

4 1200 Series VD Reference Manual

1200 Series VD Reference Manual 5

Contents

1 Installing the Vacuum Degasser

Site Requirements 10

Unpacking the Vacuum Degasser 13

Optimizing the Stack Configuration 15

Installing the Vacuum Degasser 17

Flow Connections to the Vacuum Degasser 19

Transporting the Vacuum Degasser 22

2 Optimizing Performance

Introduction to the Vacuum Degasser 24

When to Use a Vacuum Degasser? 25

Operation Modes of the Vacuum Degasser 26

Normal Operation Mode 1 27

Normal Operation Mode 2 (Timing Mode) 27

Continuous Mode 28

Error Mode 28

Operational Hints for the Vacuum Degasser 29

Solvent Information 31

Prevent Blocking of Solvent Filters 32

3 Troubleshooting

Status Indicators 34

Hardware Symptoms 36

All Lamps are Off and the Vacuum Degasser Appears Dead 37

6 1200 Series VD Reference Manual

If the Status Indicator is Red 39

If the Status Indicator is Yellow and the Vacuum Pump is not

Running 40

If the Status Lamp is Yellow and the Vacuum Pump Runs

Continuously 41

4 Repairing the Vacuum Degasser

Overview of the Repair Procedures 46

Using the ESD Strap 48

Removing and Refitting the Top Cover 49

Assembling the Main Cover 51

Exchanging the Status Light Pipe 52

Overview of Internal Parts 53

Exchanging Internal Parts 54

Exchanging the Vacuum Chamber 55

Exchanging the Vacuum Pump 57

Exchanging the Solenoid Valve 59

Exchanging the Degasser Control Assembly and the Sensor

Assembly 60

5 Parts and Materials

Vacuum Degasser Parts 64

Cover Parts 66

Sheet Metal Kit 67

Power and Status Light Pipes 68

Accessory Kit 69

Cable Overview 70

Remote Cables 71

Auxiliary Cable 72

1200 Series VD Reference Manual 7

6 Theory of Operation

How the Electronics Work 74

7 Specifications

Performance Specifications 80

A Safety Information

General Safety Information 82

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 85

Radio Interference 86

Sound Emission 87

Solvent Information 88

Agilent Technologies on Internet 89

Index

8 1200 Series VD Reference Manual

Agilent 1200 Series Vacuum Degasser

Reference Manual

Agilent Technologies

Installing the Vacuum Degasser

Site Requirements 10

Unpacking the Vacuum Degasser 13

Optimizing the Stack Configuration 15

Installing the Vacuum Degasser 17

Flow Connections to the Vacuum Degasser 19

Transporting the Vacuum Degasser 22

10 1200 Series VD Reference Manual

1Installing the Vacuum Degasser

Site Requirements

A suitable environment is important to ensure optimum performance of the

vacuum degasser.

Power Considerations

The vacuum degasser power supply has wide-ranging capability (see Table 1

on page 11). It accepts any line voltage in the range mentioned below.

Consequently there is no voltage selector in the rear of the vacuum degasser.

There are two externally accessible fuses, that protect the power supply.

Power Cords

Different power cords are offered as options with the vacuum degasser. The

female end of each of the power cords is identical. It plugs into the

power-input socket at the rear of the vacuum degasser. The male end of each of

the power cords is different and designed to match the wall socket of a

particular country or region.

WARNING To disconnect the instrument from line, unplug the pwer cord. The power supply still

uses some power, even if the instrument is switched off.

WARNING Shock hazard or damage of your instrumentation can result, if the devices are

connected to a line voltage higher than specified.

CAUTION Make sure to have easy access to the power cable of the instrument, in order to

disconnect the instrument from line.

WARNING Never use cables other than the ones supplied by Agilent Technologies to ensure

proper functionality and compliance with safety or EMC regulations.

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