Milwaukee MI 413 Manual de usuario

USER MANUAL

MI 413

Free & Total Chlorine

High Range Meter

Dear Customer,

Thank you for choosing a Martini product.

This manual will provide you with the

necessary information for the correct use of

the instrument.

Please read it carefully before using the

meter. This instrument is in compliance with

directives.

SPECIFICATIONS:

Range 0.00 to 10.00 mg/L Cl2

Resolution 0.01 mg/L (0.00-3.50 mg/L);

0.10 mg/L (above 3.50 mg/L)

Precision ±0.10 mg/L @ 5.00 mg/L

Light Source Tungsten lamp

Light Detector Silicon Photocell and

525 nm narrow band interference filter

Method Adaptation of the USEPA

method 330.5 and Standard Method

4500-Cl G.

Environment 0 to 50°C (32 to 122°F);

100% RH max.

Battery Type 1 x 9 volt

Auto-Shut off After 10' of non-use

Dimensions 192 x 104 x 52 mm

(7.5 x 4.1 x 2”)

Weight 380 g

MEASUREMENT PROCEDURE:

1• Turn the meter on by pressing

ON/OFF.

2• When the LCD displays “- - -”, the

meter is ready.

3• Fill the cuvet with 10

mL of sample, up to the

mark, and replace the

cap.

4• Place the cuvet into the

holder and ensure that

the notch on the cap is

positioned securely into

the groove.

5• Press ZERO and “SIP”

will blink on the display.

6• After a few seconds the

display will show “-0.0-

”. The meter is now

zeroed and ready for

measurement.

7• Empty the cuvet !

8• For free chlorine measurement:

Add 5 mL of Distiled/Deionized water

by using a syringe

9• Fill the cuvet up to the 10 mL mark

with 5 mL of unreacted sample using

a pipette.

10 • Add the content of one packet

of MI526-100 reagent.

11• Replace the cap and swirl

gently for 20 seconds

12• Reinsert the cuvet into the

holder and ensure that the

notch on the cap is

positioned securely into the groove.

13• Wait 1 minute for free chlorine

and press READ. “SIP” will blink

during measurement.

14• The instrument directly displays

concentration in mg/L of chlorine.

15• For total chlorine measurement,

Prepare new 5 mL of Distiled /

Deionized water by using a

syringe

16• Fill the cuvet up to the 10 mL mark

with 5 mL of unreacted sample

using a pipette

17• Add the content of one packet of

MI524-100 reagent

18• Replace the cap and swirl

gently for 20 seconds

19• Reinsert the cuvet into the holder

and ensure that the notch on the

cap is positioned securely into the

groove.

20• Wait for 2 minutes and 30

seconds then

press READ

and “SIP” will

blink during

measurement.

21• The instrument directly displays

concentration in mg/L of total

chlorine.

Interferences

• Bromine (positive error)

• Chlorine dioxide (positive error)

• Iodine (positive error)

• Oxidized Manganese and Chromium

(positive error)

• Ozone (positive error)

• Alkalinity above 250 mg/L CaCO3 or

acidity above 150 mg/L CaCO3 will

not reliable develop the full amount of

color or it may rapidly fade. To resolve

this, neutralize the sample with diluted

HCl or NaOH.

GUIDE TO DISPLAY CODES:

This prompt appears for 1 second each

time the instrument is turned on.

The dashes “- - -”

indicates that the

meter is in a ready

state and zeroing can

be performed.

Sampling In Progress.

Flashing “SIP” prompt

appears each time the

meter is performing a

measurement.

“-0.0-”, the meter is in

a zeroed state and

measurement can be

performed.

The blinking "BAT"

indicates that the

battery voltage is

getting low and the

battery needs to be

replaced.

“-bA-”, the battery is

dead and must be

replaced. Once this

indication is displayed,

the meter will lock up.

Change the battery

and restart the meter.

“Conf”, the meter has

lost its configuration. Contact your

dealer or the nearest Martini Customer

Service Center.

ERROR MESSAGES

On zero reading

• Blinking “-0.0-” indicates that the

zeroing procedure failed due to a low

signalto-noise ratio.

In this case

press ZERO again.

• “no L”, the

instrument can not

adjust the light

level. Please check

that the sample

does not contain

any debris.

• “L Lo”, there is

not enough light to

perform a

measurement.

Please check the

preparation of the

zero cuvet.

• “L Hi”, there is too

much light to

perform a

measurement.

Please check the preparation of the zero

cuvet.

On sample reading

• “-SA-”, there is too

much light for the

sample

measurement.

Please check if the

right sample cuvet is

inserted.

• “Inv”, the sample

and the zero cuvet

are inverted.

• “ZErO”, a zero

reading was not

taken. Follow the instruction in the

measurement procedure for zeroing the

meter.

• Under range. A blinking “0.00”

indicates that the

sample absorbs less

light than the zero

reference.

Check the procedure

and make sure you

use the same cuvet

for reference (zero)

and measurement.

• A flashing value of

the maximum

concentration

indicates an over

range condition.

The concentration of the sample is

beyond the programmed range: dilute

the sample and re-run the test.

BATTERY REPLACEMENT

Battery replacement must only take

place in a non-hazardous environment.

Simply rotate the battery cover on the

back of the meter.

Detach the

battery from

the terminals

and attach a

fresh 9V

battery while

paying

attention to

the correct

polarity.

Insert the battery and replace the cover.

ACCESSORIES:

MI513-045 Free & Total Chlorine

reagent set (45 tests)

MI0001 Glass cuvets (2 pcs)

MI0002 Caps for cuvets (2 pcs)

MI0003 Stoppers for cuvets (2 pcs)

MI0004 Tissue for wipping cuvets

(4 pcs)

MI0005 9V battery (1 pc)

WARRANTY

This instrument is warranted against defects

in materials and manufacturing for a period of

two years from the date of purchase.

If during this period the repair or replacement

of parts is required, where the damage is not

due to negligence or erroneous operation by

the user, please

return the meter to either distributor or our

office in the original packing and the repair

will be free of charge.

Damages due to accidents, misuse,

tampering or lack of prescribed maintenance

are not covered.

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