Metrohm NIRS XDS RapidContent Manual de usuario

NIRS XDS RapidContent Analyzer

Manual

8.921.8001EN / 2020-04-30

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

NIRS XDS RapidContent Analyzer

Manual

8.921.8001EN / 2020-04-30

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Instrument description ......................................................... 1

1.2 Intended use ......................................................................... 2

1.3 About the documentation ................................................... 2

1.3.1 Symbols and conventions ........................................................ 2

1.4 Safety instructions ................................................................ 3

1.4.1 General notes on safety ........................................................... 3

1.4.2 Electrical safety ........................................................................ 3

1.4.3 Flammable solvents and chemicals ........................................... 4

1.4.4 Recycling and disposal ............................................................. 4

2 Overview of the instrument 5

2.1 Monochromator .................................................................... 5

2.1.1 Connectors/rear ....................................................................... 5

2.1.2 Status display ........................................................................... 6

2.1.3 Instrument connection ............................................................. 6

3 Installation 7

3.1 Unpacking and inspecting the instrument ......................... 7

3.1.1 Packaging ................................................................................ 7

3.1.2 Checks .................................................................................... 7

3.1.3 Scope of application ................................................................ 7

3.2 Setting up the instrument .................................................... 7

3.2.1 Lifting and transporting instruments ........................................ 7

3.2.2 Ambient conditions ................................................................. 8

3.2.3 General conditions ................................................................... 8

3.2.4 Vibrations and/or shocks .......................................................... 8

3.3 Connecting monochromator to measuring module .......... 9

3.4 Connecting the power supply cable ................................. 10

3.5 Connecting the network cable .......................................... 11

3.6 Switching on the instrument ............................................. 11

3.7 Initial start-up ..................................................................... 12

3.8 Setting up accessories ........................................................ 12

4 Operation 13

5 Operation and maintenance 14

5.1 General notes ...................................................................... 14

5.1.1 Care ...................................................................................... 14

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭

5.1.2 Maintenance by Metrohm Service .......................................... 14

5.2 Maintenance ....................................................................... 14

5.2.1 Overview ............................................................................... 15

5.2.2 Replacing the fan filter ........................................................... 15

5.2.3 Replacing the lamp ................................................................ 18

5.2.4 Replacing the fuse ................................................................. 26

5.2.5 Cleaning the sampling window .............................................. 28

6 Appendix 30

6.1 Accessories for sample compartment ............................... 31

6.1.1 Sample cell ............................................................................ 31

6.1.2 Iris ......................................................................................... 32

6.2 Calibration standards ......................................................... 35

7 Technical specifications 36

7.1 LAN interface ...................................................................... 36

7.2 Power connection ............................................................... 36

7.3 Ambient conditions ............................................................ 36

7.4 Operation ............................................................................ 36

7.5 Reference conditions .......................................................... 37

7.6 Dimensions .......................................................................... 37

7.7 Housing ............................................................................... 38

8 Accessories 39

Glossary 40

Index 42

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front - measuring instrument ............................................................ 5

Figure 2 Rear - monochromator ...................................................................... 5

Figure 3 Status display .................................................................................... 6

Figure 4 Instrument connection ...................................................................... 6

Figure 5 On/off switch .................................................................................. 11

Figure 6 Mini sample cup with disposable back ............................................. 34

Figure 7 Vials ................................................................................................ 34

Figure 8 Transflection vessel with gold or stainless steel diffuse reflector ....... 34

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

￭￭￭￭￭￭￭￭ 1

1 Introduction

This manual gives you a comprehensive overview of the installation and

maintenance of the NIRS XDS RapidContent Analyzer. The NIRS XDS Rap-

idContent Analyzer is operated with the control software. You can find

information on operating the instrument in the tutorial and in the manual

for the control software.

NOTICE

You can request application descriptions in the form of

Application Notes and Application Bulletins from your

Metrohm representative or download them from

http://www.metrohm.com.

1.1 Instrument description

The NIRS XDS RapidContent Analyzer is a measuring instrument for reflec-

tion measurement in the visible to near-infrared wavelength range.

The complete NIRS XDS RapidContent Analyzer measuring instrument

consists of two modules, monochromator and measuring module.

The monochromator operates in the range from 400 to 2,500 nm.

The measuring module to the NIRS XDS RapidContent Analyzer is

equipped with the corresponding accessories for specific samples and can

be replaced with other measuring modules during ongoing operation

(hot-swappable).

The NIRS XDS RapidContent Analyzer is designed for quality monitoring in

production processes and can be applied for the following purposes:

￭Quick and non-destructive incoming goods inspection of raw materials

￭Production process monitoring

￭Final inspection of finished products

The NIRS XDS RapidContent Analyzer can be used to measure the follow-

ing sample types:

￭Powders

￭Coarse solids/granulates

￭Solids/coatings/paper

￭Tablets/capsules

￭Turbid liquids

￭Pastes/creams

1.2 Intended use ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭

￭Viscous liquids/gels

￭Clear liquids

The NIRS XDS RapidContent Analyzer is operated with the control soft-

ware via an external computer.

1.2 Intended use

The NIRS XDS RapidContent Analyzer is designed for use in production

facilities. It can be used for incoming goods inspection or for production

process monitoring.

This instrument is suitable for measuring chemicals and flammable sam-

ples. Usage of the NIRS XDS RapidContent Analyzer therefore requires the

user to have basic knowledge and experience in handling toxic and caustic

substances. Knowledge with respect to the application of the fire preven-

tion measures prescribed for laboratories is also mandatory.

1.3 About the documentation

CAUTION

Please read through this documentation carefully before putting the

instrument into operation. The documentation contains information

and warnings which the user must follow in order to ensure safe opera-

tion of the instrument.

1.3.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-

ond to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

Method Dialog text, parameter in the software

File ▶ New Menu or menu item

[Next] Button or key

WARNING

This symbol draws attention to a possible life-threat-

ening hazard or risk of injury.

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