Metrohm 930 Compact IC Flex Manual

930 Compact IC Flex

930 Compact IC Flex Oven SeS/PP/Deg

Manual – Short Instructions

8.930.8120EN / 2017-07-31

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

930 Compact IC Flex

930 Compact IC Flex Oven

SeS/PP/Deg

2.930.2560

Manual – Short Instructions

8.930.8120EN / 2017-07-31 zst

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560) ￭￭￭￭￭￭￭￭ III

Table of contents

1 About these short instructions 1

2 Introduction 2

2.1 Instrument description ......................................................... 2

2.2 Intended use ......................................................................... 4

2.3 Safety instructions ................................................................ 5

2.3.1 General notes on safety ........................................................... 5

2.3.2 Electrical safety ........................................................................ 5

2.3.3 Tubing and capillary connections ............................................. 6

2.3.4 Flammable solvents and chemicals ........................................... 6

2.3.5 Recycling and disposal ............................................................. 6

2.4 Symbols and conventions .................................................... 7

3 Overview of the instrument 8

3.1 Front ...................................................................................... 8

3.2 Rear ........................................................................................ 9

4 Installation 11

4.1 Setting up the instrument .................................................. 11

4.1.1 Packaging .............................................................................. 11

4.1.2 Checks .................................................................................. 11

4.1.3 Location ................................................................................ 11

4.2 Capillary connections in the IC system ............................. 11

4.3 Removing transport locking screws .................................. 12

4.4 Connecting the drainage tubing and leak sensor ............ 14

4.4.1 Installing the drainage tubing ................................................ 14

4.4.2 Connecting the leak sensor .................................................... 15

4.5 Column oven ....................................................................... 16

4.6 Connecting the eluent bottle ............................................. 16

4.7 Connecting the eluent degasser ........................................ 18

4.8 Installing the high-pressure pump .................................... 19

4.9 Installing an inline filter ..................................................... 19

4.10 Installing the pulsation absorber ...................................... 19

4.11 Injection valve ..................................................................... 19

4.12 Metrohm Suppressor Module (MSM) ............................... 19

4.12.1 Inserting the rotors ................................................................ 20

4.12.2 Connecting the Metrohm Suppressor Module (MSM) ............. 21

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

4.13 Peristaltic pump .................................................................. 24

4.13.1 Installing the peristaltic pump ................................................ 24

4.14 Metrohm CO2 Suppressor (MCS) ....................................... 26

4.14.1 Connecting the MCS ............................................................. 26

4.14.2 Installing adsorption cartridges .............................................. 26

4.15 Installing the conductivity detector .................................. 28

4.16 Installing the amperometric detector ............................... 29

4.17 Connecting the sample degasser (optional) ..................... 29

4.18 Connecting the instrument to a computer ....................... 30

4.19 Connecting the instrument to the power grid ................. 31

4.20 Initial start-up ..................................................................... 32

4.21 Connecting and rinsing the guard column ....................... 34

4.22 Connecting the separation column ................................... 35

4.23 Conditioning ........................................................................ 37

5 Operation 39

6 Accessories 40

Index 41

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560) ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front ................................................................................................. 8

Figure 2 Rear .................................................................................................. 9

Figure 3 Removing the transport locking screws ............................................ 13

Figure 4 Installing tubing weighting and aspiration filter ................................ 18

Figure 5 Metrohm Suppressor Module (MSM) – Connection capillaries .......... 22

Figure 6 Connecting the MCS ....................................................................... 26

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 About these short instructions

930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560) ￭￭￭￭￭￭￭￭ 1

1 About these short instructions

This short instruction manual contains important chapters from the com-

prehensive manual. In addition to an introduction, safety instructions and

an overview of the instrument, you will also find information about instal-

ling and operating the 930 Compact IC Flex Oven SeS/PP/Deg as well as

information regarding the warranty. You can download the comprehen-

sive manual as a PDF file from the Internet.

Downloading the manual

You can find the detailed manual on the Internet under

http://www.metrohm.com/:

1. Enter the order number for your instrument as the search term (e.g.

2.930.2560).

2. Click on >More information.

3. Click on Documents.

All available documents for the instrument will be displayed.

4. Click on the PDF link to download the desired manual.

2.1 Instrument description ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

2 Introduction

2.1 Instrument description

The 930 Compact IC Flex is a robust ion chromatograph. It is distinguished

by:

￭Its intelligence: All of the functions are monitored, optimized and docu-

mented in an FDA-compatible manner. Intelligent components, such as

iColumns, save important data onto a chip.

￭Its compact design: It has a small footprint.

￭Its transparency: All components are easily accessible and located for

simple visibility and can be monitored during operation through a large

window.

￭Its safety: The wet end and the electronics are physically separated,

thereby preventing fluids from coming into contact with the electronics

to a large extent. A leak sensor is integrated into the wet end.

￭Its environmental compatibility.

￭Its low noise emission.

￭The intelligent MagIC Net software.

The 930 Compact IC Flex is operated using the MagIC Net software. A

USB cable is used to connect the instrument to a computer with

MagIC Net installed. The intelligent software detects the instrument auto-

matically and checks its functionality. The software controls and monitors

the instrument, evaluates the measured data and manages it in a data-

base.

The 930 Compact IC Flex Oven SeS/PP/Deg consists of the following mod-

ules:

Housing

The sturdy housing contains the instrument's electronic components,

including their interfaces and one connector for a separation column. In

addition, the housing provides space for a conductivity detector or an

amperometric detector. Capillaries and cables can be fed into and out of

the instrument through several openings.

Leak sensor

The leak sensor detects leaking liquid that collects in the instrument's base

tray. Liquid that leaks in the instrument is routed to the base tray using

drainage tubing and detected there.

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