Metrohm 941 Manual de usuario

941 Eluent Production Module

Manual

8.941.8001EN / 2020-01-08

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

941 Eluent Production Module

Manual

8.941.8001EN / 2020-01-08

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

941 Eluent Production Module (2.941.0010) ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Instrument description ......................................................... 1

1.1.1 Intended use ........................................................................... 1

1.2 About the documentation ................................................... 2

1.2.1 Symbols and conventions ........................................................ 2

1.3 Safety instructions ................................................................ 3

1.3.1 General notes on safety ........................................................... 3

1.3.2 Electrical safety ........................................................................ 3

1.3.3 Tubing and capillary connections ............................................. 4

1.3.4 Flammable solvents and chemicals ........................................... 4

1.3.5 Recycling and disposal ............................................................. 4

2 Overview of the instrument 6

2.1 Front ...................................................................................... 6

2.2 Rear ........................................................................................ 7

3 System overview 8

4 Installation 10

4.1 Setting up the instrument .................................................. 10

4.1.1 Packaging .............................................................................. 10

4.1.2 Checks .................................................................................. 10

4.1.3 Location ................................................................................ 10

4.2 Base tray and bottle holder ............................................... 10

4.2.1 Basic information on base tray and bottle holder ................... 10

4.2.2 Mounting base tray and bottle holder (optional) .................... 11

4.3 Connecting the eluent bottle ............................................. 16

4.4 Connecting the concentrate bottle ................................... 19

4.5 Connecting the ultrapure water container ....................... 22

4.5.1 Connecting the ultrapure water canister ................................ 22

4.5.2 Connecting an ELGA PURELAB flex ........................................ 25

4.6 Installing the Dosino .......................................................... 26

4.7 Connecting the instrument ................................................ 29

4.7.1 Connecting the instrument to the ion chromatograph ........... 29

4.7.2 Connecting the instrument to the power grid ........................ 29

5 Operation 31

6 Operation and maintenance 32

6.1 Care ...................................................................................... 32

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 941 Eluent Production Module (2.941.0010)

6.2 Servicing the door .............................................................. 32

6.3 Dosino .................................................................................. 33

6.4 Dosing unit .......................................................................... 33

7 Troubleshooting 34

7.1 Dosino .................................................................................. 34

7.2 Dosing unit .......................................................................... 34

8 Technical specifications 35

8.1 Reference conditions .......................................................... 35

8.2 Ambient temperature ......................................................... 35

8.3 Level sensor ........................................................................ 35

8.4 Housing ............................................................................... 36

8.5 Weight ................................................................................. 36

8.6 Dosino .................................................................................. 36

8.7 Dosing unit .......................................................................... 36

8.8 Power connection ............................................................... 36

8.9 Interfaces ............................................................................. 37

9 Accessories 38

Index 39

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

941 Eluent Production Module (2.941.0010) ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front ................................................................................................. 6

Figure 2 Rear .................................................................................................. 7

Figure 3 Removing the base tray ................................................................... 12

Figure 4 Mounting the base tray ................................................................... 13

Figure 5 Removing the bottle holder ............................................................. 14

Figure 6 Mounting the bottle holder ............................................................. 15

Figure 7 Bottle cap for level sensor - Inserting the measuring sensor ............. 16

Figure 8 Installing the eluent bottle cap with level sensor .............................. 17

Figure 9 Installing the concentrate bottle cap without level sensor ................ 19

Figure 10 Installing the concentrate bottle cap with level sensor ..................... 20

Figure 11 Installing the ultrapure water canister cap without level sensor ........ 22

Figure 12 Installing the ultrapure water canister cap with level sensor ............. 23

Figure 13 Installing an ELGA PURELAB flex ...................................................... 25

Figure 14 Connecting the Dosino .................................................................... 27

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

941 Eluent Production Module (2.941.0010) ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Instrument description

The 941 Eluent Production Module allows you to produce eluent for

your IC system from a concentrate and ultrapure water as needed and in a

software-controlled manner.

Thanks to the built-in Level Control, the instrument is capable of monitor-

ing the liquid levels in up to 4 liquid containers, if they are equipped with

level sensors.

A level sensor for the eluent bottle is indispensable for the automated pro-

duction of eluent and is contained in the scope of delivery of the 941 Elu-

ent Production Module. However, we recommend using level sensors to

also monitor the bottle with the concentrate and the ultrapure water con-

tainer. Additional level sensors are available as optional accessories in vari-

ous versions.

The 941 Eluent Production Module is operated with the MagIC Net soft-

ware. If the 941 Eluent Production Module is connected to a 940 Profes-

sional IC Vario instrument, MagIC Net automatically detects the 941 Elu-

ent Production Module and checks its functional capability. It controls and

monitors the entire IC system including all connected instruments; it evalu-

ates the measured data and manages it in a database.

1.1.1 Intended use

The 941 Eluent Production Module is an instrument for the automated

production of eluent for ion chromatography systems. It can monitor the

levels of various liquid containers and, where necessary, perform appropri-

ate actions controlled by the software.

The present instrument is suitable for processing chemicals. Usage of the

941 Eluent Production Module therefore requires the user to have basic

knowledge and experience in handling toxic and caustic substances.

Knowledge regarding the application of fire prevention measures prescri-

bed for laboratories is also mandatory.

1.2 About the documentation ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 941 Eluent Production Module (2.941.0010)

1.2 About the documentation

CAUTION

Read through this documentation carefully before putting the instru-

ment into operation. The documentation contains information and

warnings which the user must follow in order to ensure safe operation

of the instrument.

1.2.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-

ond to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

Method Dialog text, parameter in the software

File ▶ New Menu or menu item

[Next] Button or key

WARNING

This symbol draws attention to a possible life-threat-

ening hazard or risk of injury.

WARNING

This symbol draws attention to a possible hazard due

to electrical current.

WARNING

This symbol draws attention to a possible hazard due

to heat or hot instrument parts.

WARNING

This symbol draws attention to a possible biological

hazard.

CAUTION

This symbol draws attention to possible damage to

instruments or instrument parts.

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