Metrohm Combustion-IC-System Manual de usuario

Combustion-IC-System

Manual – Short Instructions

8.920.8003EN / 2018-08-31

Metrohm AG

CH-9100 Herisau

Switzerland

+41 71 353 85 85

[email protected]

www.metrohm.com

Combustion-IC-System

Manual – Short Instructions

8.920.8003EN / 2018-08-31

Technical Communication

Metrohm AG

CH-9100 Herisau

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

Disclaimer

Deficiencies arising from circumstances that are not the responsibility of

Metrohm, such as improper storage or improper use, etc., are expressly

excluded from the warranty. Unauthorized modifications to the product

(e.g. conversions or attachments) exclude any liability on the part of the

manufacturer for resulting damage and its consequences. Instructions and

notes in the Metrohm product documentation must be strictly followed.

Otherwise, Metrohm's liability is excluded.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

Combustion-IC-System ￭￭￭￭￭￭￭￭ III

Table of contents

1 About these short instructions 1

2 Introduction 2

2.1 The Combustion IC system ................................................... 2

2.1.1 Overview ................................................................................. 2

2.1.2 System description ................................................................... 3

2.1.3 Sequence of a determination ................................................... 3

2.2 Intended use ......................................................................... 5

2.3 Safety instructions ................................................................ 5

2.3.1 General notes on safety ........................................................... 5

2.3.2 Electrical safety ........................................................................ 5

2.3.3 Tubing and capillary connections ............................................. 6

2.3.4 Flammable solvents and chemicals ........................................... 7

2.3.5 Recycling and disposal ............................................................. 7

3 Installation 8

3.1 Overview ................................................................................ 8

3.2 Dosino for ultrapure water ................................................ 11

3.2.1 Connecting the ports – Overview ........................................... 11

3.3 Dosino for the absorber solution ...................................... 12

3.3.1 Connecting the ports – Overview ........................................... 12

3.4 10-port-valve ....................................................................... 13

3.4.1 Connecting the ports ............................................................. 13

3.5 6-port valve ......................................................................... 14

3.5.1 Connecting the ports ............................................................. 14

3.6 Connecting the 920 Absorber Module to the remaining

components ........................................................................ 15

3.6.1 Connecting the Combustion Module (AJ) inlet: water infeed .. 16

3.6.2 Connecting the Combustion Module (AJ) outlet: absorber

solution ................................................................................. 18

3.6.3 Connecting the Combustion Oven (TEI) inlet .......................... 20

3.6.4 Connecting the Combustion Oven (TEI) outlet ........................ 21

3.6.5 Connecting the 930 Compact IC Flex ..................................... 21

3.7 Connecting the LPG/GSS Module ...................................... 23

4 Start-up 26

Index 29

Table of figures ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ Combustion-IC-System

Table of figures

Figure 1 Detectable elements .......................................................................... 2

Figure 2 Overview – CIC system ...................................................................... 3

Figure 3 Sequence of the determination ......................................................... 4

Figure 4 Capillaries and tubings in use – Overview .......................................... 9

Figure 5 Connect the Dosino for ultrapure water .......................................... 11

Figure 6 Connect the Dosino for the absorber solution .................................. 12

Figure 7 Connecting the 10-port valve .......................................................... 13

Figure 8 Connecting the 6-port valve ............................................................ 14

Figure 9 Combustion tube – Inlet .................................................................. 17

Figure 10 Combustion tube – Outlet ............................................................... 18

Figure 11 Combustion tube – Inlet .................................................................. 20

Figure 12 Combustion Oven (TEI) – Outlet ...................................................... 21

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 About these short instructions

Combustion-IC-System ￭￭￭￭￭￭￭￭ 1

1 About these short instructions

These Short Instructions contain important information about the Com-

bustion IC system. In addition to an introduction and safety instructions,

you can find a description of the Combustion IC system and information

on installing the 920 Absorber Module and its interfaces to the Combus-

tion-IC-System. You can download the detailed manual for the 920

Absorber Module as a PDF file from the Internet

(https://www.metrohm.com).

2.1 The Combustion IC system ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ Combustion-IC-System

2 Introduction

2.1 The Combustion IC system

2.1.1 Overview

Combustion is a sample preparation technique that uses burning to digest

a sample. Solid, liquid and gaseous samples that are flammable can be

digested using combustion. Combustion IC is particularly suited for deter-

mining the following elements:

Figure 1 Detectable elements

An additional instrument is required for the determination of gaseous

samples: the LPG/GSS Module (AJ) (2.136.0720) or the GLS Sampler CIC

(TEI) (2.0136.0630).

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Introduction

Combustion-IC-System ￭￭￭￭￭￭￭￭ 3

2.1.2 System description

Figure 2 Overview – CIC system

The sample is combusted in the Combustion Module (AJ) / Combustion

Oven (TEI).

The gases generated during combustion are dissolved into an absorber

solution in the 920 Absorber Module and are optimized for analysis using

suitable sample preparation techniques.

In the end, the absorption solution is preconcentrated in an ion chromato-

graph and analyzed.

The entire process is controlled and monitored using MagIC Net software.

The analysis data is saved in the software's database.

2.1.3 Sequence of a determination

A determination in the Combustion IC system runs according to the fol-

lowing diagram:

2.1 The Combustion IC system ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

4￭￭￭￭￭￭￭￭ Combustion-IC-System

Start determination

(CIC system)

Rinse absorber tube and

provide absorber solution

(920 Absorber Module)

Sample input

(Combustion Module)

Rinse c apillary f. combustion

gases w. absorber solution

(920 Absorber Module)

Absorption of

combustion gases

(920 Absorber Module)

optional: Water infeed

(920 Absorber Module)

Combustion

Fill loop with

absorption solution

(920 Absorber Module)

Matrix elimination

(930 Compact IC Flex)

Re-rinse absorber tube

(920 Absorber Module)

IC determination

(930 Compact IC Flex)

Combustion Module (AJ)/

Combustion Oven (TEI)

Combustion Module (AJ)/Combustion Oven (TEI)

Figure 3 Sequence of the determination

NOTICE

Do not mix these up!

￭Absorber solution: e.g. H2O2 solution for oxidizing sulfur oxides.

￭Absorption solution: Combustion gases dissolved in the absorber

solution.

The determination is controlled entirely by MagIC Net. You can find a

detailed description of the sequence in the online help for MagIC Net

under the title "Combustion sequence".

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