Metrohm Combustion-IC-System Manual de usuario
Combustion-IC-System
Manual – Short Instructions
8.920.8003EN / 2018-08-31
Metrohm AG
CH-9100 Herisau
Switzerland
+41 71 353 85 85
www.metrohm.com
Combustion-IC-System
Manual – Short Instructions
8.920.8003EN / 2018-08-31
Technical Communication
Metrohm AG
CH-9100 Herisau
This documentation is protected by copyright. All rights reserved.
This documentation has been prepared with great care. However, errors
can never be entirely ruled out. Please send comments regarding possible
errors to the address above.
Disclaimer
Deficiencies arising from circumstances that are not the responsibility of
Metrohm, such as improper storage or improper use, etc., are expressly
excluded from the warranty. Unauthorized modifications to the product
(e.g. conversions or attachments) exclude any liability on the part of the
manufacturer for resulting damage and its consequences. Instructions and
notes in the Metrohm product documentation must be strictly followed.
Otherwise, Metrohm's liability is excluded.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents
Combustion-IC-System ￭￭￭￭￭￭￭￭ III
Table of contents
1 About these short instructions 1
2 Introduction 2
2.1 The Combustion IC system ................................................... 2
2.1.1 Overview ................................................................................. 2
2.1.2 System description ................................................................... 3
2.1.3 Sequence of a determination ................................................... 3
2.2 Intended use ......................................................................... 5
2.3 Safety instructions ................................................................ 5
2.3.1 General notes on safety ........................................................... 5
2.3.2 Electrical safety ........................................................................ 5
2.3.3 Tubing and capillary connections ............................................. 6
2.3.4 Flammable solvents and chemicals ........................................... 7
2.3.5 Recycling and disposal ............................................................. 7
3 Installation 8
3.1 Overview ................................................................................ 8
3.2 Dosino for ultrapure water ................................................ 11
3.2.1 Connecting the ports – Overview ........................................... 11
3.3 Dosino for the absorber solution ...................................... 12
3.3.1 Connecting the ports – Overview ........................................... 12
3.4 10-port-valve ....................................................................... 13
3.4.1 Connecting the ports ............................................................. 13
3.5 6-port valve ......................................................................... 14
3.5.1 Connecting the ports ............................................................. 14
3.6 Connecting the 920 Absorber Module to the remaining
components ........................................................................ 15
3.6.1 Connecting the Combustion Module (AJ) inlet: water infeed .. 16
3.6.2 Connecting the Combustion Module (AJ) outlet: absorber
solution ................................................................................. 18
3.6.3 Connecting the Combustion Oven (TEI) inlet .......................... 20
3.6.4 Connecting the Combustion Oven (TEI) outlet ........................ 21
3.6.5 Connecting the 930 Compact IC Flex ..................................... 21
3.7 Connecting the LPG/GSS Module ...................................... 23
4 Start-up 26
Index 29
Table of figures ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭
IV ￭￭￭￭￭￭￭￭ Combustion-IC-System
Table of figures
Figure 1 Detectable elements .......................................................................... 2
Figure 2 Overview – CIC system ...................................................................... 3
Figure 3 Sequence of the determination ......................................................... 4
Figure 4 Capillaries and tubings in use – Overview .......................................... 9
Figure 5 Connect the Dosino for ultrapure water .......................................... 11
Figure 6 Connect the Dosino for the absorber solution .................................. 12
Figure 7 Connecting the 10-port valve .......................................................... 13
Figure 8 Connecting the 6-port valve ............................................................ 14
Figure 9 Combustion tube – Inlet .................................................................. 17
Figure 10 Combustion tube – Outlet ............................................................... 18
Figure 11 Combustion tube – Inlet .................................................................. 20
Figure 12 Combustion Oven (TEI) – Outlet ...................................................... 21
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 About these short instructions
Combustion-IC-System ￭￭￭￭￭￭￭￭ 1
1 About these short instructions
These Short Instructions contain important information about the Com-
bustion IC system. In addition to an introduction and safety instructions,
you can find a description of the Combustion IC system and information
on installing the 920 Absorber Module and its interfaces to the Combus-
tion-IC-System. You can download the detailed manual for the 920
Absorber Module as a PDF file from the Internet
(https://www.metrohm.com).
2.1 The Combustion IC system ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭
2￭￭￭￭￭￭￭￭ Combustion-IC-System
2 Introduction
2.1 The Combustion IC system
2.1.1 Overview
Combustion is a sample preparation technique that uses burning to digest
a sample. Solid, liquid and gaseous samples that are flammable can be
digested using combustion. Combustion IC is particularly suited for deter-
mining the following elements:
Figure 1 Detectable elements
An additional instrument is required for the determination of gaseous
samples: the LPG/GSS Module (AJ) (2.136.0720) or the GLS Sampler CIC
(TEI) (2.0136.0630).
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Introduction
Combustion-IC-System ￭￭￭￭￭￭￭￭ 3
2.1.2 System description
Figure 2 Overview – CIC system
The sample is combusted in the Combustion Module (AJ) / Combustion
Oven (TEI).
The gases generated during combustion are dissolved into an absorber
solution in the 920 Absorber Module and are optimized for analysis using
suitable sample preparation techniques.
In the end, the absorption solution is preconcentrated in an ion chromato-
graph and analyzed.
The entire process is controlled and monitored using MagIC Net software.
The analysis data is saved in the software's database.
2.1.3 Sequence of a determination
A determination in the Combustion IC system runs according to the fol-
lowing diagram:
2.1 The Combustion IC system ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭
4￭￭￭￭￭￭￭￭ Combustion-IC-System
Start determination
(CIC system)
Rinse absorber tube and
provide absorber solution
(920 Absorber Module)
Sample input
(Combustion Module)
Rinse c apillary f. combustion
gases w. absorber solution
(920 Absorber Module)
Absorption of
combustion gases
(920 Absorber Module)
optional: Water infeed
(920 Absorber Module)
Combustion
Fill loop with
absorption solution
(920 Absorber Module)
Matrix elimination
(930 Compact IC Flex)
Re-rinse absorber tube
(920 Absorber Module)
IC determination
(930 Compact IC Flex)
Combustion Module (AJ)/
Combustion Oven (TEI)
Combustion Module (AJ)/Combustion Oven (TEI)
Figure 3 Sequence of the determination
NOTICE
Do not mix these up!
￭Absorber solution: e.g. H2O2 solution for oxidizing sulfur oxides.
￭Absorption solution: Combustion gases dissolved in the absorber
solution.
The determination is controlled entirely by MagIC Net. You can find a
detailed description of the sequence in the online help for MagIC Net
under the title "Combustion sequence".
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