Metrohm 930 Compact IC Flex Manual de usuario

930 Compact IC Flex

930 Compact IC Flex Oven/Deg/MB

Manual – Short Instructions

8.930.8121EN / 2022-11-15

Metrohm AG

CH-9100 Herisau

Switzerland

+41 71 353 85 85

[email protected]

www.metrohm.com

930 Compact IC Flex

930 Compact IC Flex Oven/Deg/MB

2.930.2180

Manual – Short Instructions

8.930.8121EN / 2022-11-15

Technical Communication

Metrohm AG

CH-9100 Herisau

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

Disclaimer

Deficiencies arising from circumstances that are not the responsibility of

Metrohm, such as improper storage or improper use, etc., are expressly

excluded from the warranty. Unauthorized modifications to the product

(e.g. conversions or attachments) exclude any liability on the part of the

manufacturer for resulting damage and its consequences. Instructions and

notes in the Metrohm product documentation must be strictly followed.

Otherwise, Metrohm's liability is excluded.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

930 Compact IC Flex Oven/Deg/MB (2.930.2180) ￭￭￭￭￭￭￭￭ III

Table of contents

1 About this quick start guide 1

2 Introduction 2

2.1 Instrument description ......................................................... 2

2.2 Accessories and additional information ............................. 4

2.3 Symbols and conventions .................................................... 4

3 Safety 6

3.1 Intended use ......................................................................... 6

3.2 Responsibility of the operator ............................................. 6

3.3 Requirements for operating personnel ............................... 7

3.4 Safety instructions ................................................................ 7

3.4.1 General notes on safety ........................................................... 7

3.4.2 Electrical safety ........................................................................ 7

3.4.3 Tubing and capillary connections ............................................. 8

3.4.4 Flammable solvents and chemicals ........................................... 9

3.4.5 Recycling and disposal ............................................................. 9

4 Overview of the instrument 10

4.1 Front .................................................................................... 10

4.2 Rear ...................................................................................... 12

5 Installation 14

5.1 Setting up the instrument .................................................. 14

5.1.1 Packaging .............................................................................. 14

5.1.2 Checks .................................................................................. 14

5.1.3 Location ................................................................................ 14

5.2 Capillary connections in the IC system ............................. 14

5.3 Removing transport locking screws .................................. 15

5.4 Connecting the drainage tubing and leak sensor ............ 17

5.4.1 Installing the drainage tubing ................................................ 17

5.4.2 Connecting the leak sensor .................................................... 18

5.5 Column oven ....................................................................... 19

5.6 Connecting the eluent bottle ............................................. 19

5.7 Connecting the eluent degasser ........................................ 21

5.8 Installing the high-pressure pump .................................... 22

5.9 Installing an inline filter ..................................................... 22

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven/Deg/MB (2.930.2180)

5.10 Installing the pulsation absorber ...................................... 22

5.11 Injection valve ..................................................................... 22

5.12 Installing the conductivity detector .................................. 22

5.13 Connecting the sample degasser (optional) ..................... 23

5.14 Connecting the instrument to a computer ....................... 24

5.15 Connecting the instrument to the power grid ................. 25

5.16 Initial start-up ..................................................................... 26

5.17 Connecting and rinsing the guard column ....................... 28

5.18 Connecting and rinsing the separation column ............... 29

5.19 Conditioning ........................................................................ 31

6 Operation 33

Index 34

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

930 Compact IC Flex Oven/Deg/MB (2.930.2180) ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front ............................................................................................... 10

Figure 2 Rear ................................................................................................ 12

Figure 3 Removing the transport locking screws ............................................ 16

Figure 4 Installing the tubing weighting and aspiration filter .......................... 21

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 About this quick start guide

930 Compact IC Flex Oven/Deg/MB (2.930.2180) ￭￭￭￭￭￭￭￭ 1

1 About this quick start guide

This short instruction manual contains important chapters from the com-

prehensive manual. In addition to an introduction, safety instructions and

an overview of the instrument, you will also find information about instal-

ling and operating the 930 Compact IC Flex Oven/Deg/MB as well as

information regarding the warranty. The comprehensive manual can be

downloaded as a PDF file from the Internet.

Downloading the manual

You can find the detailed manual on the Internet under

http://www.metrohm.com/:

1. Enter the order number for your instrument as the search term (e.g.

2.930.2180).

2. Click on Documents.

All available documents for the instrument will be displayed.

3. Click on the PDF link to download the desired manual.

2.1 Instrument description ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven/Deg/MB (2.930.2180)

2 Introduction

2.1 Instrument description

The 930 Compact IC Flex is a robust ion chromatograph. It is distinguished

by:

￭Its intelligence: All of the functions are monitored, optimized and docu-

mented in an FDA-compatible manner. Intelligent components, such as

iColumns, save important data onto a chip.

￭Its compact design: It has a small footprint.

￭Its transparency: All components are easily accessible and located for

simple visibility and can be monitored during operation through a large

window.

￭Its safety: The wet end and the electronics are physically separated.

This prevents fluids from coming into contact with the electronics to a

large extent. A leak sensor is integrated into the wet end.

￭Its environmental compatibility.

￭Its low noise emission.

￭The intelligent MagIC Net software.

￭Its performance: Short retention times and sharp peaks when used

with the IC Conductivity Detector MB and a column with a diameter of

2 mm.

The 930 Compact IC Flex is operated using the MagIC Net software. A

USB cable is used to connect the instrument to a computer with

MagIC Net installed. The intelligent software detects the instrument auto-

matically and checks its functionality. The software controls and monitors

the instrument, evaluates the measured data and manages it in a data-

base.

The 930 Compact IC Flex Oven/Deg/MB consists of the following mod-

ules:

Housing

The sturdy housing contains the instrument's electronic components,

including their interfaces and one connector for a separation column. In

addition, the housing provides space for a conductivity detector or an

amperometric detector. Capillaries and cables can be fed into and out of

the instrument through several openings.

Leak sensor

The leak sensor detects leaking liquid that collects in the instrument's base

tray. Liquid that leaks in the instrument is routed to the base tray using

drainage tubing and detected there.

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