Inficon HAPSITE ER Manual de usuario

Operating Manual

HAPSITE® ER

074-471-P1E

INFICON

Two Technology Place

East Syracuse, NY 13057-9714

INFICON Table of Contents

074-471-P1E HAPSITE ER Operating Manual iii

Table of Contents

1 Declaration of Conformity ........................................................................................................................... 12

2 Two Year Warranty....................................................................................................................................... 14

3 Disclaimer and Copyright............................................................................................................................ 16

4 Definition of Note, Hint, Danger, Warning and Caution Paragraphs ....................................................... 17

5 Operating Manual Style Conventions......................................................................................................... 18

6 Customer Support........................................................................................................................................ 19

6.1 How to Contact Customer Support ........................................................................................................19

6.2 Returning Your Instrument to INFICON ................................................................................................. 19

7 Introduction .................................................................................................................................................. 21

7.1 System Description ................................................................................................................................21

7.2 Instrument and Accessories...................................................................................................................21

7.3 Specifications ......................................................................................................................................... 22

7.4 Instrument Overview ..............................................................................................................................22

7.5 Description of Subsystems.....................................................................................................................23

7.6 Gas Chromatograph...............................................................................................................................23

7.6.1 Membrane Isolation Valve ..........................................................................................................24

7.7 Mass Spectrometer ................................................................................................................................ 24

7.8 Vacuum System ..................................................................................................................................... 26

7.9 Electronic Systems.................................................................................................................................27

7.10 Software Systems .................................................................................................................................. 27

8 HAPSITE Components and Assemblies .................................................................................................... 28

8.1 Ship Kit Packing Lists.............................................................................................................................28

8.1.1 930-850-G5, G6, G7, G8 Ship Kit Contents................................................................................ 28

8.2 Basic Assembly......................................................................................................................................30

8.2.1 Attaching the Probe ....................................................................................................................30

8.2.2 Installing the Gas Canisters ........................................................................................................ 32

8.2.3 How to Remove a Gas Canister ................................................................................................. 37

8.2.4 Connect the Power Supply .........................................................................................................40

8.2.5 Connecting the Laptop................................................................................................................42

8.2.5.1 Connect the Laptop with the Black Crossover Cable ........................................................ 42

8.2.5.2 Connect Laptop with Wireless Connection ........................................................................ 44

8.3 Battery.................................................................................................................................................... 45

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8.3.1 Battery Charger...........................................................................................................................45

8.3.2 Battery Charger Connections and Startup .................................................................................. 45

8.3.3 Loading the Battery Charger.......................................................................................................46

8.3.4 Understanding the Battery Charger Indicators............................................................................ 47

8.3.4.1 Testing Battery................................................................................................................... 47

8.3.5 Installing the Battery ...................................................................................................................48

8.3.6 Removing the Battery .................................................................................................................48

8.4 Helpful Guidelines .................................................................................................................................. 50

9 Operate the Instrument in Portable Mode.................................................................................................. 51

9.1 Start HAPSITE ER in Portable Mode ..................................................................................................... 51

9.1.1 Emergency Mode (EMER MODE) .............................................................................................. 59

9.1.2 Concentrator Options (CONC OPTIONS)................................................................................... 63

9.1.2.1 Concentrator Cleanout....................................................................................................... 63

9.1.2.2 Skip Cleanout ....................................................................................................................67

9.1.3 Concentrator Cleanout Failure.................................................................................................... 69

9.1.4 Quick Reference SOP- Heat-up and Tune ................................................................................. 71

9.2 Select a Different Method Using the SELECT METHOD Icon ............................................................... 71

9.2.1 Change the Default Method ........................................................................................................ 75

9.2.2 Show All ...................................................................................................................................... 77

9.3 Survey Mode ..........................................................................................................................................77

9.3.1 Quick Reference SOP - Survey Method ..................................................................................... 85

9.4 ANALYZE (GC/MS) Mode with the Concentrator .................................................................................86

9.4.1 Tri-Bed Concentrator ..................................................................................................................86

9.4.2 Tenax Concentrator ....................................................................................................................86

9.4.3 Procedure for Running Concentrator Methods ........................................................................... 86

9.4.4 Quick Reference SOP - Concentrator Methods.......................................................................... 92

9.5 Detecting Hazardous Chemicals............................................................................................................92

9.6 Help Icon ................................................................................................................................................93

9.7 Info Icon .................................................................................................................................................94

9.8 EXIT Menu ...........................................................................................................................................103

9.8.1 Extended Standby.....................................................................................................................105

9.8.2 End Standby .............................................................................................................................108

10 Communications and Touch Screen Options ......................................................................................... 110

10.1 Communications ..................................................................................................................................110

10.1.1 Wireless Range......................................................................................................................... 110

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10.1.2 Turning On the Radio................................................................................................................ 110

10.1.3 Wireless Module Indicator Lights ..............................................................................................112

10.2 Setting Up Communications................................................................................................................. 112

10.3 Configuring the Instrument for Communications.................................................................................. 119

10.3.1 Turning Off the Radio................................................................................................................ 130

10.4 Wireless Information ............................................................................................................................132

10.4.1 Regulatory Compliance Information for UNITED STATES Users............................................. 132

10.4.1.1 FCC Statement ................................................................................................................ 133

10.4.1.2 FCC RF Exposure Statement .......................................................................................... 133

10.4.2 Regulatory Compliance Information for CANADIAN Users ......................................................134

10.4.2.1 Industry Canada (IC) Notes ............................................................................................. 134

10.4.3 Regulatory Compliance Information for EUROPEAN Users..................................................... 134

10.4.3.1 European Usage Restrictions .......................................................................................... 135

10.4.3.2 European EMC Compliance Statement........................................................................... 136

10.4.3.3 European Safety Compliance Statement......................................................................... 138

11 Laptop Operation ...................................................................................................................................... 139

11.1 Laptop Operation .................................................................................................................................139

11.1.1 Sampling Procedure .................................................................................................................139

11.2 Survey Mode ........................................................................................................................................ 139

11.2.1 Sampling Procedure .................................................................................................................140

11.2.2 Quick Reference SOP - Running Survey Mode........................................................................ 143

11.3 ANALYZE (GC/MS) Mode with the Concentrator ...............................................................................143

11.3.1 Tri-Bed Concentrator ................................................................................................................143

11.3.2 Tenax Concentrator .................................................................................................................. 144

11.3.3 Quick Reference SOP - Tri-Bed Concentrator Method............................................................. 148

11.4 Selecting a New Method ...................................................................................................................... 149

12 ER IQ Software ........................................................................................................................................... 152

12.1 HAPSITE Software - ER IQ.................................................................................................................. 152

12.1.1 Computer System Requirements.............................................................................................. 152

12.2 Software Installation............................................................................................................................. 152

12.2.1 System Setup Screen ............................................................................................................... 152

12.3 Introduction ..........................................................................................................................................153

12.3.1 System Startup Menu ...............................................................................................................153

12.3.1.1 File Menu ......................................................................................................................... 153

12.3.2 Functions Menu ........................................................................................................................157

12.3.3 System ...................................................................................................................................... 157

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12.3.3.1 Port Setting Tab............................................................................................................... 158

12.3.3.2 Display Tab...................................................................................................................... 159

12.3.3.3 Miscellaneous Tab........................................................................................................... 160

12.3.4 Tools Menu ............................................................................................................................... 167

12.3.4.1 Set Access Level ............................................................................................................. 168

12.3.5 View Menu ................................................................................................................................ 170

12.3.6 Window Menu ........................................................................................................................... 171

12.3.7 Help Menu................................................................................................................................. 171

12.4 Safety Database................................................................................................................................... 172

12.5 Manage File .........................................................................................................................................175

12.6 Status Icon ...........................................................................................................................................180

12.6.1 Status Properties ......................................................................................................................180

12.6.2 HAPSITE Time Zone ................................................................................................................181

12.6.3 HAPSITE Information................................................................................................................ 189

12.6.4 Pressure Flows and Temperatures........................................................................................... 190

12.6.5 NEG Status ...............................................................................................................................191

12.6.6 Functions .................................................................................................................................. 195

12.6.7 Parameters ............................................................................................................................... 196

12.6.8 Service Module ......................................................................................................................... 197

12.7 Front Panel Display Icon ...................................................................................................................... 198

12.8 HAPSITE Sensor Icon.......................................................................................................................... 199

12.8.1 Update HAPSITE Software....................................................................................................... 200

12.8.2 Bring Online .............................................................................................................................. 200

12.8.2.1 Communication Messages ..............................................................................................200

12.8.3 Disconnect ................................................................................................................................ 201

12.9 HAPSITE Icons .................................................................................................................................... 201

13 Data Review ................................................................................................................................................ 203

13.1 Chromatogram Overlay........................................................................................................................ 203

13.2 Introduction ..........................................................................................................................................205

13.3 *Data Review Toolbar .......................................................................................................................... 205

13.4 Accessing the Data Review Feature .................................................................................................... 206

13.5 Reports................................................................................................................................................. 210

13.5.1 Using the Zoom Function in the TIC/RIC Window .................................................................... 215

13.5.2 Zooming Out ............................................................................................................................. 219

13.5.3 Using the Zoom Spectrum Function .........................................................................................220

13.6 Analyzing Data Using AMDIS ..............................................................................................................222

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13.6.1 Setting the AMDIS Pathway...................................................................................................... 224

13.6.2 View Function in AMDIS ........................................................................................................... 227

13.6.3 Confirm Screen in AMDIS......................................................................................................... 228

13.7 NIST Library Searches......................................................................................................................... 230

13.8 Current Peaks ...................................................................................................................................... 235

13.8.1 Show/Update Current Peaks ....................................................................................................236

13.8.1.1 Show/Update Current Peaks Window Description ..........................................................241

13.8.1.2 Peak Search Parameters................................................................................................. 243

13.8.1.3 NIST Search Setup.......................................................................................................... 243

13.8.1.4 Report Preview ................................................................................................................ 247

13.8.2 Background Subtract ................................................................................................................251

13.8.2.1 Background Subtraction Using a Range of Points........................................................... 254

13.8.2.2 Additional Features of the Background Tool.................................................................... 255

13.8.3 Range Tool ...............................................................................................................................256

13.8.3.1 Additional Features of the Range Tool ............................................................................ 258

13.9 Displaying Reconstructed Ion Chromatograms (RIC) .......................................................................... 259

13.1

Chromatogram Subtract....................................................................................................................... 263

13.1

Right-Click Menus Within Data Review................................................................................................ 267

13.11.

Right-Clicking in the TIC Window ............................................................................................. 267

13.11.1.1Properties Menu ..............................................................................................................269

13.11.

Spectrum Window.....................................................................................................................270

13.11.

Analyzing Data Using NIST ......................................................................................................271

13.11.

NIST Database Program........................................................................................................... 272

13.11.

Grab Spectra for NIST ..............................................................................................................273

14 Tune............................................................................................................................................................. 276

14.1 Introduction to AutoTune and Manual Tune......................................................................................... 276

14.2 AutoTune.............................................................................................................................................. 276

14.2.1 Starting AutoTune from the Manual Tune Screen or Laptop Computer ...................................276

14.3 Viewing a Tune Report......................................................................................................................... 277

14.3.1 Tune Report Options................................................................................................................. 280

14.4 Performing Manual Tune...................................................................................................................... 283

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14.4.1 Manual Tune Variables .............................................................................................................283

14.4.2 *Outputs .................................................................................................................................... 284

14.4.3 *Inputs.......................................................................................................................................285

14.4.4 Other Inputs .............................................................................................................................. 287

14.4.5 *Set Access Level to Advanced ................................................................................................288

14.4.6 *Manual Tune............................................................................................................................ 288

14.4.7 *Save Tune ............................................................................................................................... 289

14.4.8 Tool Bar ....................................................................................................................................289

14.4.9 Tune Drop-Down Menu............................................................................................................. 290

14.4.1

Tune Control Panel ................................................................................................................... 292

14.4.10.1Tune Parameters ............................................................................................................. 293

14.4.1

Peak Scan Window...................................................................................................................294

14.4.11.1Peak Scan Window Control ............................................................................................. 295

14.4.1

Setting the Full Scan Range .....................................................................................................296

14.4.1

Tune and Mass Calibration Status............................................................................................ 297

14.4.1

Mass Calibration Status ............................................................................................................ 298

14.4.1

Scan Window Menu .................................................................................................................. 299

14.4.1

Tune Status Window Menu.......................................................................................................299

15 Method Editor ............................................................................................................................................. 301

15.1 The Method Editor................................................................................................................................ 301

15.2 Reloading Default HAPSITE Methods .................................................................................................303

15.2.1 Loading Default Methods ..........................................................................................................303

15.3 Default Methods ................................................................................................................................... 306

15.4 Description Page.................................................................................................................................. 307

15.5 Startup Page ........................................................................................................................................310

15.6 Inlet Page ............................................................................................................................................. 313

15.6.1 Inlet States ................................................................................................................................313

15.6.2 GC Temperature Profile............................................................................................................ 318

15.6.3 Scan Events.............................................................................................................................. 319

15.6.4 Headspace Flow Parameter .....................................................................................................320

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15.6.5 SituProbe Flow Parameter........................................................................................................ 321

15.6.6 Scan Events for SIM Methods ..................................................................................................322

15.7 Tune Page............................................................................................................................................ 322

15.7.1 Param Page ..............................................................................................................................322

15.7.2 Report Page.............................................................................................................................. 324

15.8 Full Scan Page..................................................................................................................................... 325

15.9 SIM Page .............................................................................................................................................327

15.9.1 SIM for Analyze......................................................................................................................... 327

15.9.2 SIM for Survey .......................................................................................................................... 328

15.9.3 Creating a SIM Method .............................................................................................................329

15.1

Search Page ........................................................................................................................................336

15.10.

Setting Up a Qualitative Search................................................................................................338

15.10.

Setting Up a Quantitative Search..............................................................................................342

15.10.

Peak Search .............................................................................................................................344

15.10.

Alarm.........................................................................................................................................346

15.10.

Edit Options ..............................................................................................................................348

15.10.

Template/Calibration Files ........................................................................................................ 356

15.10.

View Reports.............................................................................................................................356

15.1

Data Page ............................................................................................................................................361

15.11.

Data File Information.................................................................................................................362

15.11.

Date and Time Appendix ..........................................................................................................363

15.11.

Data Display..............................................................................................................................364

15.1

Summary Page ....................................................................................................................................365

15.1

Method Sequence ................................................................................................................................ 365

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16 Calibration................................................................................................................................................... 370

16.1 Introduction to Quantitative Analysis.................................................................................................... 370

16.2 Calibrating a Method ............................................................................................................................ 370

16.3 Definition of Terms in the Calibrate Window ........................................................................................ 390

16.3.1 Method ...................................................................................................................................... 391

16.3.2 Data Files.................................................................................................................................. 391

16.3.3 Peak Search .............................................................................................................................391

16.3.4 Analytes .................................................................................................................................... 392

16.3.5 Reports ..................................................................................................................................... 392

16.3.6 Extracted Mass Peaks .............................................................................................................. 394

16.3.7 Calibration.................................................................................................................................394

16.4 Build/Edit Template Menu .................................................................................................................... 395

16.5 ID Unknowns........................................................................................................................................ 395

16.6 Definition of Terms in the ID Unknowns Window ................................................................................. 399

16.6.1 Method ...................................................................................................................................... 399

16.6.2 Data Files.................................................................................................................................. 399

16.6.3 Peak Search .............................................................................................................................400

16.6.4 Analytes .................................................................................................................................... 400

16.6.5 Reports ..................................................................................................................................... 400

16.7 Display Function................................................................................................................................... 401

17 Maintenance ............................................................................................................................................... 402

17.1 Introduction ..........................................................................................................................................402

17.2 HAPSITE Symptom - Cause - Remedy Chart...................................................................................... 402

17.3 Saturation of the Probe and Probe Line............................................................................................... 405

17.3.1 Symptoms ................................................................................................................................. 405

17.3.2 Decontaminate Saturation ........................................................................................................405

17.4 NEG Troubleshooting........................................................................................................................... 405

17.5 Attaching HAPSITE to the Service Module .......................................................................................... 406

17.5.1 Attaching HAPSITE to the Service Module Using IQ Software................................................. 407

17.5.2 Attaching HAPSITE to the Service Module Using the HAPSITE Front Panel Controls ............ 410

17.6 Bakeout Procedure ..............................................................................................................................412

17.6.1 Reactivating the NEG Pump .....................................................................................................414

18 Part Numbers.............................................................................................................................................. 417

18.1 HAPSITE Part Numbers....................................................................................................................... 417

18.2 HAPSITE Accessories .........................................................................................................................417