GAS GC-IMS-SILOX Manual de usuario

G.A.S. Gesellschaft für

analytische Sensorsysteme mbH

GC-IMS-SILOX

USER MANUAL

GC-IMS-SILOX – User Manual

Version 1.4.0, March 2021

All data, texts, designs, images and other elements used in this user manual are

protected by copyright law. Any infringement may be subject to legal action.

Passing it on to third parties and producing copies of any kind or form –on the

whole or in parts - is not permitted without written agreement of G.A.S. Any

infringement may be subject to legal action.

G.A.S. reserves the right to realize technical changes to the product without

explicitly mentioning them.

CE-Marking according to:

International Standard EN ISO 17050-1:2004

European Union Low Voltage Directive 2006/95/EC

European Union Electromagnetic Compatibility Directive 2004/108/EC

G.A.S. Gesellschaft für analytische Sensorsysteme mbH

44227 Dortmund - Germany

2
Table of Content 
 
1Preface..................................................................................5 
1 Symbols Used in this User Manual ...........................................5 
2 Notation for Describing Dialogs and Elements in Dialogs ................6 
3 Liability and Guarantee ......................................................6 
4 Return and Disposal ...........................................................7 
5 Packing..........................................................................7 
6 Transport .......................................................................8 
7 Software Updates..............................................................8 
8 Contacting G.A.S. .............................................................8 
2Safety ................................................................................. 10 
1 Intended Usage Only ........................................................ 10 
2 Responsibilities of the Operator........................................... 10 
3 Ionization Source ............................................................ 11 
4 Explosion Protection ........................................................ 11 
5 Protection from High Voltage.............................................. 12 
3Scope of Supply and Storage Conditions ......................................... 13 
1 Scope of Supply .............................................................. 13 
2 Storage Conditions .......................................................... 14 
4Cleaning of the Housing and Maintenance ....................................... 15 
1 Cleaning of the Housing .................................................... 15 
2 Maintenance.................................................................. 15 
5Intended Use and Working Principle.............................................. 16 
1 Intended Use ................................................................. 16 
2 Calculating Concentrations ................................................ 16 
3 Working Principle and Internal Gas Flow................................. 18 
6Workflow: Physical Setup .......................................................... 21 
1 Housing of the Device....................................................... 21 
2 Device Type/Serial Number Plate on the Rear Side .................... 23 
3 Unpacking, Placement and Connections ................................. 24 
7Workflow: Initial Operation / Cleaning .......................................... 29 
1 Using the Cleaning Mode ................................................... 29 

 

 
2 Workflow ..................................................................... 29 
8Device Parameters During Measurements and Standby ........................ 32 
1 Introduction .................................................................. 32 
2 Values ......................................................................... 32 
9Workflow: Single Manual Measurement .......................................... 33 
1 Introduction .................................................................. 33 
2 Workflow ..................................................................... 34 
Workflow: Manual Calibration ..................................................... 38 
1 Introduction .................................................................. 38 
2 Workflow ..................................................................... 38 
Workflow: Running Automatic Measurements................................... 42 
1 Introduction to the Interval Mode ........................................ 42 
2 Workflow ..................................................................... 43 
Workflow: Current Loop Setup .................................................... 49 
1 Introduction .................................................................. 49 
2 Electrical Interface ......................................................... 50 
3 Configuring the Current Loop.............................................. 50 
Workflow: Tag Lists ................................................................. 53 
1 Introduction .................................................................. 53 
2 Creating and Editing Tag Lists............................................. 54 
3 Usage.......................................................................... 57 
4 Exporting Tag Lists .......................................................... 59 
5 Importing Tag Lists.......................................................... 62 
Workflow: File Transfer Setup .................................................... 66 
1 Overview...................................................................... 66 
2 Connecting to a Server in a LAN .......................................... 68 
Workflow: PDF Reports - Setup and Usage...................................... 74 
1 Introduction .................................................................. 74 
2 Workflow ..................................................................... 76 
Workflow: Firmware Upgrade ..................................................... 80 
1 Introduction .................................................................. 80 
2 Workflow ..................................................................... 81 
Graphical User Interface ........................................................... 84 
1 Introduction .................................................................. 84 

4
2 Start Page..................................................................... 85 
2.1 Overview ............................................................ 85 
2.2 Results View ........................................................ 87 
2.3 Scope View.......................................................... 88 
3 MEA Mode Start Dialog ...................................................... 89 
4 Calibration Mode Start Dialog ............................................. 90 
5 Substances and the Substance Calibration Dialog ...................... 91 
6 Interval Mode Start Dialog ................................................. 93 
7 Date and Time Input Dialogs ............................................... 95 
8 Status Bar..................................................................... 97 
9 Substances Page ............................................................. 99 
10 System Page .................................................................100 
10.1 System Page Info Tab............................................. 101 
10.2 System Page Plan Tab ............................................102 
10.3 System Page Settings Tab........................................ 103 
10.4 System Page Transfer Tab .......................................107 
10.5 The System Page Modes Tab ....................................109 
11 Current Loop Settings Dialog .............................................110 
12 Log Messages Dialog........................................................111 
13 IP Address Input Dialog ....................................................112 
14 Text Input Dialog ........................................................... 113 
15 Number Input Dialog .......................................................113 
Tag Lists File Formats.............................................................. 115 
1 Overview.....................................................................115 
2 CSV Format Specification..................................................115 
3 JSON Format Specification ................................................116 
Technical Specifications........................................................... 118 
1 Measurement Ranges....................................................... 118 
2 Device ........................................................................119 
3 Current Loop Interface ....................................................121 
4 Consumables ................................................................121 
5 Ionization Source Specifications.......................................... 122 
6 Modbus TCP Specification .................................................123 
Calculating of silicon ’Total Si’ and silica ’Total SiO2’ in GC-IMS-SILOX ... 132 
 

1Preface

1.1 Symbols Used in this User Manual

Symbol

Description

Danger

This symbol marks paragraphs that describe situations that

can potentially damage the device.

Danger –Radioactive Radiation

This symbol marks paragraphs that describe potential

dangers and damage due to exposure to radioactive

radiation.

Danger –Explosive Substances

This symbol marks paragraphs that describe potential

dangers and damage due to explosions.

Danger –High Voltage

This symbol marks paragraphs that describe potential

dangers to life and health due to electric current.

Danger - Hot Surface

This symbol marks paragraphs that describe situations in

which surface parts of the device can heat up to a point

where touching it or bringing objects close to it may be

hazardous.

Important

This symbol marks paragraphs that describe important

instructions or information that may prevent the operator

from making common mistakes.

1.2 Notation for Describing Dialogs and Elements in

Dialogs

Example:

System ›Connections ›LAN File Transfer ›Settings…›Test Connection

Describe the logical path for arriving in a particular dialog or at an element in

a dialog. In this example the path starts with the System page. On that page

the Connections page must be selected. On that page in the LAN File Transfer

row the button Settings… must be selected and in that dialog the button Test

Connection must be selected.

Example:

Gas Out, S-Free

Casing socket names, choice menu elements etc. are marked in this way.

1.3 Liability and Guarantee

This user manual describes the safe and proper handling of the device.

Usage other than described in this manual may damage the device

and/or harm persons involved.

Do not use the device for other purposes. Damages due to misuse are

not covered by the guarantee. Such damage claims will be rejected.

This user manual should be available to all personnel operating the device.

Follow the safety instructions in this manual and the national and/or local rules

and general safety regulations regarding the prevention of accidents at all

times.

Before starting to operate the device read the manual completely and

thoroughly. Make sure that all personnel operating the device understand the

instructions described.

G.A.S. does not assume any liability for damages resulting from neglect or

ignorance of the instructions in this manual or provided in other ways by G.A.S.

The graphics in this user manual are schematic and may differ from the actual

conditions. The firmware and PC software screen shots in this user manual may

slightly differ from the actual conditions.

The actual scope of supply might differ due to customization. For further

information please contact G.A.S.

1.4 Return and Disposal

For an appropriate disposal, the device and the associated equipment must be

returned to G.A.S. or to a third party authorized by G.A.S.

1.5 Packing

If no return agreement regarding the packing was agreed upon dispose the

packaging material always in an environmentally friendly way and according to

valid local regulations. If necessary, ask a recycling company.

1.6 Transport

To prevent damages to the equipment it should be moved only in the provided

carrying case.

Protective caps should be put on gas sockets in case the device is

stored or transported.

1.7 Software Updates

To receive information on available updates for the components of the system

please contact G.A.S. Gesellschaft für analytische Sensorsysteme mbH. If there

are any updates customers will be contacted by G.A.S. Gesellschaft für

analytische Sensorsysteme mbH as soon as the updates are available. Users will

be provided with information about the changes and instructions for executing

the updates.

1.8 Contacting G.A.S.

For questions concerning G.A.S. products a customer service is available:

G.A.S. Gesellschaft für analytische Sensorsysteme mbH

Otto-Hahn-Straße 15

44227 Dortmund

Germany

Phone: +49 (0) 231 / 97 42 - 65 50

Fax: +49 (0) 231 / 97 42 - 65 55

[email protected]

The telephone hotline is available from Monday to Friday from 9:00 to 16:00

hours. In urgent cases or if you use fax or email please provide a telephone

number for callbacks.

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