Buchi Syncore Manual de usuario

Operation Manual

Platform

ncore®

093008 en

Syncore Platform

Table of contents

en, Version E (43 pages) Order code

Syncore Instructions 093008

1 Scope of delivery 2

2 Safety 6

3 Function 10

3.1 The single platform 10

3.2 Syncore Analyst R-4, R-6 and R-12 11

3.3 Individual components 11

3.4 Syncore Polyvap R-4 to R-96 12

4 Putting into operation 14

5 Operation 17

5.1 The single platform 17

5.2 Safety instructions 17

5.3 Temperature and RPM 19

5.4 Programm mode: Temperature / Time steps 20

5.5 Further control parameters 22

5.6 Pre-set safety settings 23

5.7 Overview of switches 24

5.8 Signal outlets 25

5.9 After running of the programmable valve 26

5.10 RS-232 interface 26

5.11 Signal inlets 27

5.12 Adjusting the eccentricity 28

5.13 Unbalance compensation 30

5.14 Troubleshooting: the single platform 33

6 Maintenance 34

6.1 Cleaning 34

6.2 Routine inspection of the equipment (monthly) 34

6.3 Routine inspection of the equipment (annually) 35

6.4 Calibration 35

6.5 Error messages: Calibration 37

6.6 Replacement of the fuses 37

6.7 Error Messages: Hardware 38

6.8 Customer service 38

7 Taking out of Operation 39

8 Replacement Parts 40

8.1 Single platform 40

9 Appendix 41

9.1 Technical data 41

9.2 Materials used 41

9.3 FCC requirements (for USA and Canada) 42

9.4 Declaration of conformity 43

Read this Operation Manual through care-

fully before starting to use the Syncore

Product Line.

Always keep these instructions ready at

hand close to the equipment so that they

may be consulted quickly at all times. Chap-

ter 2 provides important safety instructions

that must be followed to ensure safe ope-

ration of the unit.

We reserve the right to make technical changes without

prior notice. No portions of this Operation Manual may be

reproduced in any form (including with the use of electronic

or optical systems), duplicated, or distributed without written

Syncore Platform

1 Scope of delivery

Figure 1: BUCHI Syncore Analyst R-6

Voltage

1 100V 50/60Hz

2 120V 50/60Hz

3 230V 50/60Hz

Condenser

0 None

S Type S, Standard

C Type C, Cold trap

Round receiving ﬂask,

KS 24/20,PLG

0 None

2 2000ml total volume

Rack type (incl. vacuum

cover)

4 Crystal Rack R-4 Analyst

5 Crystal Rack R-6 Analyst

6 Rack R-12 Analy

Residual volume of glass

tubes

4 1ml

5 0.3ml

6 3ml

Glass tube graduation

Y Yes

N No

1 Power system cable PNE, 1.5 m

Type CH 10010

Type Schuko 10016

Type GB 17835

Type USA 10020

Type AUS 17836

1 Scope of delivery

1.1 Conﬁguration Syncore Analyst

1A 0

in addition:

2 Cooling hoses, 1m 04133

1 Power system cable PNE, 1.5m

Type CH 10010

Type Schuko 10016

Type GB 17835

Type USA 10020

Type AUS 17836

1 Operation Manual:

German 93007

English 93008

French 93009

Italian 93010

Spanish 93011

Syncore Platform

1 Scope of delivery

Figure 2: BUCHI Syncore Polyvap R-24

1.2 Conﬁguration Syncore Polyvap

1 Power system cable PNE, 1.5 m

Type CH 10010

Type Schuko 10016

Type GB 17835

Type USA 10020

Type AUS 17836

1 Operation Manual:

German 93007

English 93008

French 93009

Italian 93010

Spanish 93011

1P 000

Voltage

1 100V 50/60Hz

2 120V 50/60Hz

3 230V 50/60Hz

Condenser

0 None

S Type S, Standard

C Type C, Cold trap

Round receiving ﬂask,

KS 24/20,PLG

0 None

1 1000ml total volume

2 2000ml total volum

Rack type (incl. vacuum cover)

0 None

1 Crystal Rack R-4

2 Crystal Rack R-6

3 Rack R-12

4 Standard Rack R-24

5 Falcon Rack R-24

6 Rack R-96

in addition:

Syncore Platform

1 Scope of delivery

Figure 3: Syncore single platform

1.3 Individual components

Single Platform

Components Order code

Syncore Single Platform 230 V 50/60 Hz 38429

Syncore Single Platform 120 V 50/60 Hz 38430

Syncore Single Platform 100 V 50/60 Hz 38431

Scope of delivery

1 Syncore Single Platform, complete Including:

1 Adjustment wrench for adjusting eccen- 38477

tricity and unbalance compensation

1 Power system cable PNE, 1.5 m

Type CH 10010

Type Schuko 10016

Type GB 17835

Type USA 10020

Type AUS 17836

1 Operation Manual:

German 93007

English 93008

French 93009

Italian 93010

Spanish 93011

Table 4: Individual components single platform

Syncore Platform

2 Safety

This unit and all its components have been built in accor-

dance with the state of the art and recognized safety rules.

Nevertheless, certain risks and dangers may be involved

when working with the unit or its individual components:

• Whenevertheunitisnotbeingusedinaccordancewith

its intended purpose, or

• Wheneverthestaffoperatingtheunithavenotlacksuf-

ﬁcient training and know-how.

2.1 Symbols

Stop

Information on hazards that can result in severe material da-

mage or serious to fatal injuries.

Warning

Information on hazards that can result in injury to one’s health

or material damage.

Caution

Information pointing out technical requirements. A failure to

follow these instructions can cause malfunctions, unecono-

mical operation, and production losses.

2.2 Requirements for the user

This unit and all accessories for the Syncore line of equipment

may be used only by laboratory staff and other individuals

who, based on their education, training, or professional

experience, are fully aware of the risks involved in their use.

Staff lacking this training or staff currently being trained need

careful instruction. These operating instructions are valid as

a basic requirement.

Syncore Platform

2 Safety

2.3 Authorized use

This unit has been designed and built as a laboratory

instrument. The authorized application for the Syncore single

platform inconjunction with accessories from the Syncore

product line is as follows:

Syncore Polyvap/Syncore single platform

with accessories:

• Parallelevaporation of solvents invarious formats and

containers across a range of temperatures from room

temperature up to + 150 °C and within a range of pres-

sures from 1 mbar up to ambient pressure.

Syncore Analyst:

• Parallelconcentrationofsolventsfrom6differentsamples

across a range of temperatures from room temperatures

up to + 100 ° (or bypassing pre-set safety settings, up to

150 °C), within a range of pressures from 1 mbar up to

ambient pressure.

Applications for the Syncore line of equipment

include:

• Parallelorganic-inorganicchemicalsynthesisintheliqui-

dor in the solid phase.

• Parallelmaterialinvestigations,digestions,preparationof

samples of from 4 to 96 samples, with sample volumes

ranging from 500 down to 1 ml.

• Parallelevaporationoffrom4to96sampleswithsample

volumes from 1 ml up to 500 ml after chemical synthesis,

after chromatography, after extraction, etc.

• Parallelconcentrationinchemicalanalysis,guaranteeing

a residual volume after the evaporation.

2.4 Unauthorized use

Any use other than those indicated above and any application

that does not correspond to the Technical Data is considered

to be improper use.

If the equipment is used in a manner not speciﬁed by the

manufacturer, the protection provided by the equipment

may be impaired.

The operator himself bears sole responsibility for any risks

arising from such use.

The following in particular are explicitly forbidden:

• The processing of samples that can explode or ignite

explosively as the result of impact, friction, heat, or spar-

king (e.g., explosives, etc.).

• Thecarryingoutofchemicalreactionsthatcanproduce

substances that can explode or ignite explosively as the

resultof impact, friction, heat, or sparking (e.g., explosives,

etc.);

• Use of the unit in rooms that require explosion-proof

equipment;

Syncore Platform

2 Safety

Symbol Meaning Location

Elemento caliente,

superﬁcie caliente

General warning

• Useofthesingleplatformwithsampleholdersorsample

containers that have not been developed for use on the

Syncore single platform.

• Workingataboveatmosphericpressure

2.5 Basic hazards

The basic hazards arise from:

• Chemicals that are toxic or cause allergic reactions, or

can, in a chemical reaction, produce compounds that are

toxic or cause allergic reactions;

• Solventmaterialswhichcanformperoxides

• Veryhotorverycoldpartsmadeofplasticsandmetals

(Burn injuries)

• Kinkedhosesorthedissolvingofhosematerialsusedto

introduce liquids, compressed gases under pressure

• Movingpartswhichrotateathighspeedaboutanaxisand

which if used in an improper way can lead to injury or the

destruction of laboratory equipment

• Glassvesselsundervacuumwhichcanimplode

• Electriccableswhichcanbedamagedorincorrectlycon-

nected

• Combustiblegasesorsolventvaporsintheareaimmedi-

ately adjacent to the Syncore.

2.6 Warning labels on housing

The following warning sticker(s) can be found on the housing

or assemblies of the Syncore:

Syncore Platform

2 Safety

2.7 Safety procedures

The regional and local laws and regulations must be obser-

ved. It is necessary to wear personal protective equipment

such as protective goggles, gloves and a laboratory

coat.

It is only permissible to assemble and dismantle certain parts

of the Syncore when such action is necessary to carry out

the functional requirements.

This activity can be performed manually or by use of the tool

which is supplied. Except for authorized maintenance per-

sonnel, the removal of protective devices and cover plates/

shrouding with the aid of a conventional tool is forbidden.

The owner of the company is responsible for the instruction

of his personnel. To assist in this context, it is possible to

order these Operating Instructions in other languages. At all

times, these Operating Instructions must be available - as a

component part of Syncore - to the operating personnel at

the point where the equipment is employed.

The owner of the company will inform the Manufacturer

immediately regarding all events having a bearing on safety

which take place while the equipment is in use.

2.8 Modiﬁcations

No modiﬁcations may be made on this unit or on spare and

accessory parts, nor is use of spare or accessory parts other

than those indicated in this Operation Manual permissible,

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