Agilent Technologies 4100 Manual de usuario

Agilent 4100 ExoScan

FTIR

Operation Manual

2 Agilent 4100 ExoScan FTIR Operation Manual

Notices

2011-2013, 2017

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Manual Part Number

0023-401

Edition

Sixth edition, October 2017

Printed in Malaysia

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Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

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WARNING

CAUTION

Contents

Agilent 4100 ExoScan FTIR Operation Manual 3

Contents

1. Introduction 5

2. Getting Started 9

Unpacking 9

Packing list 10

Options 11

Components 11

Connecting power 12

Battery 13

AC power 14

Turning on the instrument 18

Power switch LED status 18

Starting the software 19

Charging the handheld PC 20

Logging on to MicroLab Mobile for the first time 20

Performance verification 21

Diagnostic values 22

Performance validation 24

3. Analyzing Samples 27

External reflectance 27

Cleaning the sample probe 29

Collecting a background spectrum 29

Collecting a sample spectrum 30

Internal reflectance (ATR) 32

Contents

4 Agilent 4100 ExoScan FTIR Operation Manual

Cleaning the sample probe 33

Collecting a background spectrum 33

Collecting a sample spectrum 34

Using the solid sample ATR press 36

Interchanging sampling accessories 39

4. Maintenance 41

5. Spare Parts 43

6. Specifications 45

Technical 45

Safety Information 46

Environmental conditions 46

Handheld PC data station 46

Electromagnetic compatibility 47

EN55011/CISPR11 47

ICES/NMB-001 48

Introduction

Agilent 4100 ExoScan FTIR Operation Manual 5

1. Introduction

The Agilent 4100 ExoScan FTIR instrument is a portable, handheld,

battery-operated analyzer designed to measure a variety of solid and

liquid samples in locations difficult or impossible to analyze in a

laboratory. It can be used for quantitative or qualitative analysis of

materials. The system is small (17.1 x 11.9 x 22.4 cm; 6.75 in x 4.68 in

x 8.81 in), lightweight (3.2 kg; 7 lb) and packaged in a weather-

resistant enclosure suitable for outdoor use. It comes standard with

internal battery power for operation up to 4 hours or can be operated

with 110/220 volt AC power for extended use.

The 4100 ExoScan FTIR can be safely used in operating temperatures

ranging from 0 to 50 degrees Celsius (32 to 122 degrees Fahrenheit)

and in humidity environments as high as 95% for extended periods of

time.

WARNING

Fire Hazard

4100 ExoScan FTIR systems are NOT intrinsically safe. Use the system only in

atmospheres that have been tested for flammable materials. If the equipment

is used in a manner not specified in this manual, the protection provided by

the equipment may be impaired.

Introduction

6 Agilent 4100 ExoScan FTIR Operation Manual

CAUTION Although the 4100 ExoScan FTIR system is designed to withstand significant

shock and vibration found in a field environment, use caution when handling and

avoid dropping the system when it is out of the shipping case. Dropping the

system may result in equipment failure.

The 4100 ExoScan FTIR uses technology known as Fourier transform

infrared (FTIR) spectroscopy, which is the current state-of-the-art

technique for molecular compound identification and quantification.

FTIR uses an infrared (IR) light source to pass through the sample

and onto a detector, which precisely measures the amount of light

absorbed by the sample. This absorbance creates a unique spectral

fingerprint that is used to identify the molecular structure of the

sample and determine the exact quantity of a particular compound in

a mixture. In addition to the capability to measure samples onsite

that in the past were typically measured in the lab, this system is a

non-destructive tool (NDT) that allows the analysis to be performed

without damaging the sample.

The heart of the Agilent FTIR spectrometer system is a patented

Michelson interferometer design mounted on shock-dampening

mechanisms to protect the components from shock and vibration in

the field. This proprietary design is the key to successfully making

FTIR technology compact, lightweight, rugged and field-portable.

The 4100 ExoScan FTIR system can be configured for a number of

different sampling configurations to accommodate the analysis of a

range of liquids, solids, powders, pastes and gels. The various

sampling probes can be provided in a dedicated configuration or with

the capability of being interchangeable. If configured for

interchangeability, the 4100 ExoScan sample probe tips are easily

interchanged in the field by the user. Information on the optimal use

of the different sampling configurations of the 4100 ExoScan system

is listed in the following categories.

Introduction

Agilent 4100 ExoScan FTIR Operation Manual 7

Agilent 4100 ExoScan FTIR External Reflectance System: For

the chemical analysis of solid or hard surface samples, especially

thickness measurement of thin coatings and films on reflective

surfaces. Typical applications include thickness measurement,

chemical degradation of composites and analysis of anodization

of metals. The External Reflectance System uses a 45 degree

specular reflectance probe or a grazing angle specular reflectance

probe. The 45 degree probe is optimal for analysis of thin films

greater than 1 micron in thickness. The grazing angle probe is

optimal for analysis of ultrathin films less than 1 micron in

thickness. Specular reflectance is an ideal method for the

analysis of surface contamination. The grazing angle probe

should be used when very low level contamination needs to be

analyzed (nanometer thickness levels). Although primarily

intended as a specular reflectance tool, the External Reflectance

System can also be used for some diffuse reflectance

measurements, which is an ideal method for the analysis of

powders, for example.

Agilent 4100 ExoScan FTIR Internal Reflectance System: For

the chemical analysis of liquids, powders, pastes and gels. The

Internal Reflectance System uses a diamond optical sampling

probe that incorporates the attenuated total reflectance (ATR)

technique. This method is optimal for the identification of a

variety of samples and has the advantage that no sample

preparation is required to obtain the proper IR absorbance

levels. The diamond ATR probe for the 4100 ExoScan FTIR is a

single reflection ATR. The single reflection ATR sampling

technique is ideal for identification of thick or highly-absorbing

samples where small IR pathlengths are required (typically

2 micron depth of penetration).

For information about upgrading a dedicated 4100 ExoScan FTIR

system to the capability of interchangeability, contact your Agilent

sales representative or call Agilent directly.

Introduction

8 Agilent 4100 ExoScan FTIR Operation Manual

The 4100 ExoScan FTIR is equipped with a handheld PC (socket

PDA) as standard and can be interfaced to the optional laptop

computer for development of new methods and for detailed viewing

and manipulating the spectra. The 4100 ExoScan software user

interface is intuitive, simple to use and requires no specialized

technical training. The spectral display is represented with easy to

read status bars and report formats, which increase ease of use on

the smaller handheld PC display. With the touch of a button, the

system provides valuable information about the identity and amount

of chemical substances present in a material.

Getting Started

Agilent 4100 ExoScan FTIR Operation Manual 9

2. Getting Started

Unpacking 9

Components 11

Connecting power 12

Turning on the instrument 18

Starting the software 19

Performance verification 21

Unpacking

To unpack your spectrometer system:

1After receiving the Agilent 4100 ExoScan FTIR delivery, do not

immediately open the shipping container. Instead, place the

shipping case in a room-temperature environment and allow

several hours for the contents of the container to reach the room

ambient temperature. This is to avoid unnecessary condensation

on the components prior to the initial setup and installation

process.

Your 4100 ExoScan FTIR has been packed to ensure that it

arrives at your facility ready to go to work. Custom foam inserts

protect the instrument from damage during travel. Whenever

your instrument is shipped via common carrier, it needs to be re-

packed in the shipping case. Using this case, your 4100 ExoScan

can be removed and re-packed in the case in a matter of seconds,

while maintaining instrument security.

Getting Started

10 Agilent 4100 ExoScan FTIR Operation Manual

2The shipping enclosure should contain the standard items listed

below as well as any optional items ordered. Inspect the

enclosure closely to make sure all items have been removed from

the shipment packaging. Also ensure that all the items in the

packing list below have arrived undamaged and are in good

working condition. Contact Agilent immediately if any items are

found to be missing or damaged in shipment.

NOTE Keep all original packing material for storing, shipping and transporting the

system in the future.

3Remove the 4100 ExoScan FTIR system from its shipping case

and place it on its side on a flat, stable surface. The instrument

must be kept away from hot surfaces and any sources of

electromagnetic interference. If the optional docking station was

ordered, place the 4100 ExoScan in the docking station.

Packing list

One Agilent 4100 ExoScan FTIR spectrometer system

One Agilent 4100 ExoScan FTIR Operation Manual

One Socket handheld PC system (PDA)

One Agilent 4100 ExoScan FTIR AC power cable

One Agilent 4100 ExoScan FTIR external power supply

One Agilent 4100 ExoScan FTIR USB cable

One Agilent 4100 ExoScan FTIR power/USB ‘Y’ cable

One handheld PC AC power cable

One handheld PC USB cable with power connector

One Agilent 4100 ExoScan FTIR strap

One Agilent MicroLab Software CD

One shipping container

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