Agilent Technologies 850-DS Manual de usuario

850-DS

Dissolution Sampling Station

Operator’s Manual

Notices

Manual Part Number

70-9074 Rev D

March 2018

No part of this manual may be

reproduced in any form or by any means

(including electronic storage and retrieval

or translation into a foreign language)

without prior agreement and written

consent from Agilent Technologies, Inc.

as governed by United States and

international copyright laws.

Agilent Technologies, Inc.

3501 Stevens Creek Blvd.

Santa Clara, CA 95052 USA

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future

editions. Further, to the maximum extent

permitted by applicable law, Agilent

disclaims all warranties, either express or

implied, with regard to this manual and

any information contained herein,

including but not limited to the implied

warranties of merchantability and fitness

for a particular purpose. Agilent shall not

be liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or performance

of this document or of any information

contained herein. Should Agilent and the

user have a separate written agreement

with warranty terms covering the

material in this document that conflict

with these terms, the warranty terms in

the separate agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such

license.

Restricted Rights Legend

U.S. Government Restricted Rights.

Software and technical data rights

granted to the federal government

include only those rights customarily

provided to end user customers. Agilent

provides this customary commercial

license in Software and technical data

pursuant to FAR 12.211 (Technical Data)

and 12.212 (Computer Software) and, for

the Department of Defense, DFARS

252.227-7015 (Technical Data -

Commercial Items) and DFARS

227.7202-3 (Rights in Commercial

Computer Software or Computer

Software Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in damage to the product or

loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated

conditions are fully understood

and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in personal injury or death.

Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

850-DS Operator’s Manual 3

Content

1Safety 7

Electrical Hazards 8

Warning 9

Caution 9

Note 9

Information Symbols 10

2 Introduction 11

Serial Number Format 13

3 Setting Up the 850-DS 15

Initial Setup 16

Equipment Ratings / Environmental Requirements for Installation 17

Specification 18

Equipment, Parts, and Accessories As Shipped 19

Parts and Accessories 19

Connections 20

Tubing 21

Power Cord 22

Apparatus Control Cable 22

Synchronized Start 23

Initial Power Up 24

Sample Tray Installation 24

Updating 850-DS Language Screens 25

Content

4850-DSOperator’sManual

Optional Filter Module 27

Changing Trays / Needle Replacement 28

4 Operating the 850-DS 29

Startup Screen 30

Main Screen 32

Menu Screens 36

Methods 36

Method Properties (Apparatus 1/2/5/6) 38

Sample Collection Parameters (Apparatus 1/2/5/6) 40

Method Properties (Apparatus 3/7) 43

Timepoint Number Selection 46

Timepoint Parameter Entry (Apparatus 1/2/5/6) 47

Timepoint Parameter Entry (Apparatus 3/7) 48

Run Method Screen 1 49

Run Method Screen 2 50

Run Method Screen 3 52

Run Method Screen 4 53

Run Method Screen 5 53

850-DS Method Transfer (to another 850-DS) 54

Alarms 56

Calibration 57

Cleaning 61

Diagnostics 64

Diagnostics Screen 2 66

Diagnostics Screen 3 67

Diagnostic Screen 4 (Apparatus 1/2/5/6) 69

Diagnostic Screen 4 (Apparatus 3/7) 71

Instrument Settings 72

Instrument Settings Screen 2 74

Manufacturing Configuration 78

Reports 79

User Access 80

Content

850-DS Operator’s Manual 5

Dialog Screens (Blue) 83

Warning Screens (Yellow) 85

Error Screens (Red) 88

5 Maintenance and Troubleshooting 91

Preventive Maintenance 92

Clean System 92

Periodic Maintenance 92

Printer Maintenance 93

Removing a Thermal Paper Roll 93

Inserting a Thermal Paper Roll 95

Thermal Printer Test 98

Obtaining Warranty and Other Services 99

Content

6850-DSOperator’sManual

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850-DS Operator’s Manual 7

1Safety

Electrical Hazards 8

1Safety

8850-DSOperator’sManual

The Agilent 850-DS Dissolution Sampling Station has been designed and tested

so that when used properly you have an accurate, fast, flexible, and safe

instrument.

If the equipment is used in a manner not specified by the manufacturer, the

protection provided by the equipment may be impaired.

Operation of a Agilent 850-DS involves the use of aqueous liquids and various

pharmaceutical dosage forms. Unskilled, improper, or careless use of this

instrument can create shock hazards, fire hazards, or other hazards which can

cause death, serious injury to personnel, or severe damage to equipment and

property.

Information on safety practices is provided with your instrument and operation

manuals. Before using your instrument or accessories, you must thoroughly read

these safety practices.

Observe all relevant safety practices at all times.

Electrical Hazards

The dissolution apparatus contains electrical circuits, devices, and components

operating at dangerous voltages. Contact with these circuits, devices, and

components can cause death, serious injury, or painful electric shock.

Panels or covers that are retained by fasteners which require the use of a tool for

removal may be opened only by Agilent-trained, Agilent-qualified, or

Agilent-authorized service engineers. Consult the manuals or product labels

supplied with the dissolution apparatus to determine which parts are

operator-accessible.

Application of the wrong supply voltage, connection of the instrument to an

incorrectly wired supply outlet, or lack of proper electrical grounding can create a

fire hazard or a potentially serious shock hazard and could seriously damage the

instrument and any attached ancillary equipment.

Always use a three-wire outlet with ground connection which is adequately rated

for the load. The installation must comply with local, state, and federal safety

regulations.

Do not connect the instrument to the main power supply until you have made

sure that the operating voltage is correctly set for the main power supply in the

specific outlet in your laboratory to which the equipment will be connected.

1Safety

850-DS Operator’s Manual 9

Warning

WARNING

A ‘Warning’ message appears in the manual when failure to observe instructions

or precautions could result in death or injury.

Read all warnings and cautions carefully and observe them at all times.

Caution

CAUTION

A ‘Caution’ message appears in the manual when failure to observe instructions

could result in damage to equipment (Agilent supplied and / or other associated

equipment).

Note

NOTE

A ‘Note’ appears in the manual to give advice or information.

1Safety

10 850-DS Operator’s Manual

Information Symbols

A depressed power button in the front of the

unit (with green light) indicates main power

on.

An extended power button in the front of the

unit (with green light off) indicates main

power off.

Indicates single-phase alternating current

Indicates the product complies with the

requirements of one or more European Union

(EU) directives.

Indicates specific equipment meets

standards of safety. These products are safe

for use in the workplace for North America.

Indicates that this product must not be

disposed of as unsorted municipal waste.

All Agilent products that are subject to the

WEEE directive shipped after August 13,

2005 are compliant with the WEEE marking

requirements. Such products are marked

with the “crossed out wheelie bin” WEEE

symbol in accordance with European

Standard EN 50419.

For more information on collection, reuse,

and recycling systems, please contact your

local/regional waste administration, your

local distributor, or Agilent.

Indicates the product complies with

regulatory compliance requirements of New

Zealand and Australia.

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