Agilent Technologies 709-DS Manual de usuario

Agilent Technologies

708-DS / 709-DS

Dissolution Apparatus

Operator’s Manual

708-DS / 709-DS Operator’s Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

70-9058

Edition

Rev D, February 2014

Agilent Technologies, Inc.

3501 Stevens Creek Blvd.

Santa Clara, CA 95052 USA

Warranty

The material contained in this doc-

ument is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further,

to the maximum extent permitted

by applicable law, Agilent disclaims

all warranties, either express or

implied, with regard to this manual

and any information contained

herein, including but not limited to

the implied warranties of mer-

chantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or

performance of this document or of

any information contained herein.

Should Agilent and the user have a

separate written agreement with

warranty terms covering the mate-

rial in this document that conflict

with these terms, the warranty

terms in the separate agreement

shall control.

Technology Licenses

The hardware and/or software described in

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license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

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customers. Agilent provides this custom-

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Software) and, for the Department of

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cal Data - Commercial Items) and DFARS

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puter Software or Computer Software

Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

708-DS / 709-DS Operator’s Manual 3

Contents

Figures 7

Tab les 9

1Safety 11

Electrical Hazards 11

Warning 13

Caution 13

Note 13

Information Symbols 14

2 Introduction 15

Conventions Used in this Manual 17

Serial Number Format 18

3 Setting Up the 708-DS / 709-DS 19

Initial Setup 20

Unpacking Procedure 20

Environmental Requirements for Installation 22

Clearance 22

Equipment, Parts, and Accessories As Shipped 23

Parts and Accessories 23

Tubing / Cable Connections 24

Heater / Circulator Setup (708-DS) 24

Instrument Level / Water Bath Setup 25

Level Instrument 25

4 708-DS / 709-DS Operator’s Manual

Contents

DVH Power Controller Setup (709-DS) 28

Temperature Probe Installation (708-DS) 29

EVT Probe Installation (708-DS) 30

Power Cord Connections 30

708-DS / 709-DS Initial Power Up 30

Filling the Water Bath (708-DS) 31

Level Instrument - Re-verification 32

Heater / Circulator Power-up (708-DS) 32

Agilent 708-DS / 709-DS Setup 33

Vessel Isolation Chamber Installation (709-DS) 33

Vessel Installation 34

Sample Manifold Installation 35

Accessory Installation 37

Setting Basket (Apparatus 1) Heights 43

Setting Paddle (Apparatus 2) Heights 44

4 Operating the 708-DS / 709-DS 47

Main Screen - Options 48

Main Screen - Display Parameters 48

Main Screen - Sample Temperatures

Main Screen - Run 50

Main Screen - Stop 57

Main Screen - Drive Unit Up / Down 59

Manual Drive Unit Up / Down 60

Manual Sampling 61

Main Screen - Manifold Up / Down 62

Main Screen - Lock 63

Main Screen - Unlock 64

Main Screen - Remote Control 65

Main Screen - Alarms 65

Main Screen - Maintenance Due Icon 66

Contents

708-DS / 709-DS Operator’s Manual 5

Menu Screen - System Menu 67

Menu Screen - Method Editor 68

Menu Screen - Reports 77

Menu Screen - Alarms 80

Menu Screen - Instrument 82

Menu Screen - Calibration 87

Menu Screen - Diagnostics 90

Menu Screen - User Access 95

General 708-DS / 709-DS Conventions 96

Alphanumeric Data Entry 96

Numeric and Time / Date Entry 97

Parameter Limits / Ranges 98

Agilent 708-DS / 709-DS Notifications 100

Main Screen - Error Conditions 100

Dialog Screens (Green / Blue) 102

Warning Screens (Yellow) 104

Error Screens (Red) 109

5 Maintenance and Troubleshooting 115

Preventive Maintenance 116

Weekly Maintenance 116

Monthly Maintenance 116

Bi-Annual Maintenance 116

Sample Line / Paddle / Basket Care 117

Shafts 117

Baskets 118

Rinsing Sample Lines 119

Rinse Cups (Optional) 120

Vessels and Evaporation Covers 121

DVH Vessel Care (709-DS) 121

Water Bath and Temperature Probes (708-DS) 122

6 708-DS / 709-DS Operator’s Manual

Contents

Water Bath Care 122

Water Bath Temperature Probe Accuracy Test 123

Removing or Adjusting Cannulas / Probes 125

Manifold Maintenance 125

Removing the Manifold 125

Accessing the Top Cover 126

Removing Top Cover 126

Replacing the Top Cover 126

Printer Maintenance 127

Removing a Thermal Paper Roll 127

Inserting a Thermal Paper Roll (5095-0307) 130

Thermal Printer Test 133

Obtaining Warranty and Other Services 134

Index 135

708-DS / 709-DS Operator’s Manual 7

Figures

Figure 1. Unpacking 20

Figure 2. Removing the Apparatus 21

Figure 3. BATH HEATER Connector 24

Figure 4. Levelers and Stability Feet 25

Figure 5. Level-Adjustment Screw Caps 26

Figure 6. Raising the Stability Feet 27

Figure 7. DVH Power Controller 28

Figure 8. BATH TEMP Connector 29

Figure 9. Positioning the Temperature Probe 29

Figure 10. Filling the Water Bath 31

Figure 11. Vessel Bubble 34

Figure 12. Positioning the Manifold for Installation 35

Figure 13. Connecting AutoTemp 36

Figure 14. Affixing the Fasteners 37

Figure 15. Proper Sample Tubing Position 38

Figure 16. Installing Evaporation Covers on Shafts 39

Figure 17. Shaft Locking Collars 39

Figure 18. Dosage Delivery Module and Alignment Post 40

Figure 19. Inserting DDM into DDM Alignment Shaft 41

Figure 20. Attaching DDM to Alignment Post 42

Figure 21. Accessory Installation 43

Figure 22. Tightening the Shaft Locking Collar 44

Figure 23. Inserting Height Spheres 45

Figure 24. Main Screen - Display Parameters 48

Figure 25. Manual Lift Knob 60

Figure 26. Taking a Manual Sample 61

Figure 27. Agilent 708-DS / 709-DS Standard Evaporation

Cover 62

Figure 28. Rinse Cup 120

8 708-DS / 709-DS Operator’s Manual

Figures

Figure 29. Resistance Value of Temperature Probe 124

Figure 30. Near-empty Paper Roll 127

Figure 31. Accessing the Printer Handle 128

Figure 32. Open Printer Chamber 128

Figure 33. Removing the Thermal Paper Roll 129

Figure 34. Inserting a Thermal New Paper Roll 130

Figure 35. Leading Paper and Closing the Lid 131

Figure 36. Closing the Printer Chamber 131

Figure 37. Feeding Paper 132

Figure 38. Printer Test 133

708-DS / 709-DS Operator’s Manual 9

Tables

Table 1. Method - Start Options 52

Table 2. Method Properties Screen 1 69

Table 3. Method Properties Screen 2 70

Table 4. Method Properties Screen 2 72

Table 5. Menu Screen - Alarms 80

Table 6. Menu Screen - Instrument Settings Screen 1 82

Table 7. Menu Screen - Instrument Settings Screen 2 84

Table 8. Menu Screen - Instrument Settings Screen 3 85

Table 9. Menu Screen - Instrument Settings Screen 3 86

Table 10. Menu Screen - Diagnostics Screen 1 90

Table 11. Menu Screen - Diagnostics Screen 2 92

Table 12. Diagnostics - DVH Diagnostics Screen 1 93

Table 13. Numeric and Time / Date Entry 97

Table 14. Parameter Limits / Ranges 98

Table 15. Dialog Screens (Green / Blue) 102

Table 16. Warning Screens (Yellow) 104

Table 17. Error Screens (Red) 109

10 708-DS / 709-DS Operator’s Manual

Tables

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