PerkinElmer LAMBDA 265 Manual de usuario

LAMBDA 265, 365 AND 465

ASX-260/280 AND ASX-

520/560 AUTOSAMPLER

Users Guide

UV SPECTROMETERS

2 . Lambda 265, 365 and 465 ASX-260/280 AND ASX-520/560 Autosampler Users Guide

Release History

Part Number Release Publication Date

09931308 C September 2016

Any comments about the documentation for this product should be addressed to:

User Assistance

PerkinElmer

710 Bridgeport Avenue

Shelton, CT 06484-4794

U.S.A.

Or emailed to: [email protected]

Notices

The information contained in this document is subject to change without notice.

Except as specifically set forth in its terms and conditions of sale, PerkinElmer makes no

warranty of any kind with regard to this document, including, but not limited to, the

implied warranties of merchantability and fitness for a particular purpose.

PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in

connection with furnishing, performance or use of this material.

This document contains proprietary information that is protected by copyright.

All rights are reserved. No part of this publication may be reproduced in any form whatsoever or

translated into any language without the prior, written permission of PerkinElmer, Inc.

Trademarks

Registered names, trademarks, etc. used in this document, even when not specifically marked as such,

are protected by law.

PerkinElmer is a registered trademark of PerkinElmer, Inc.

Contents . 3

Table of Contents



Introduction......................................................................................5

Features................................................................................................6

Autosamplers and Peristalic Pump............................................................7

Dimensions and Specifications.................................................................8

Dimensions of AutoSampler ..............................................................8

Specifications of Peristaltic Pump.......................................................8

Safety Summary.....................................................................................9

Conventions Used in this Manual............................................................12

Notes, cautions and warnings..........................................................12

Note, attention et avertissement .....................................................12

Description......................................................................................17

Description of the Autosampler..............................................................18

Front View of Autosampler..............................................................18

Back View of Autosampler...............................................................19

Description of the Peristaltic Pump.........................................................20

Installation......................................................................................23

Installation...........................................................................................24

Interface Setup...............................................................................33

Installing the Driver of Lambda 465 .......................................................34

Setting USB Serial Ports ........................................................................36

UV Lab Software .............................................................................41

Wavelength Monitoring Measurement Procedure.....................................42

Quantification Measurement Procedure...................................................47

UV Express Software.......................................................................53

Scan and Wavelength Program Mode Measurement Procedure.................54

Quantification and Scanning Quantification Mode Measurement Procedure59

Maintenance....................................................................................65

Maintenance ........................................................................................66

4 . Lambda 265, 365 and 465 ASX-260/280 AND ASX-520/560 Autosampler Users Guide

Introduction

6 . Lambda 265, 365 and 465 ASX-260/280 AND ASX-520/560 Autosampler Users Guide

Features

The ASX 260/280 and ASX-520/560 autosamplers are designed to be study, reliable and easy

to use. They provide automated sample introduction that enables you to perform other tasks

while the Auto Sampler runs.

The ASX 260/280 and ASX-520/560 automatically introduces up to 180 and 360 samples

each when fully loaded. It contains a microprocessor that allows sequential or random

sampling, providing flexibility.

The components of autosampler are made of corrosion-resistant stainless steel alloys or

anodized aluminum. The enclosure and base are made from a high-strength aluminum alloy

that is chromated and finished with an epoxy powder coating.

The autosampler operates reliably under a wide variety of conditions. Components in the

sample flow path are made of polyetherimide (PEI) and polytetrafluoroethylene (PTFE).

When these inert, non-metallic materials are used at temperatures less than 135 °C, they

can withstand repeated exposure to the following substances.

Autosamplers and Peristalic Pump

Autosampler (ASX-260) Autosampler (ASX-520)

Autosampler (ASX-280) Autosampler (ASX-560)

Peristaltic Pump

8 . Lambda 265, 365 and 465 ASX-260/280 AND ASX-520/560 Autosampler Users Guide

Dimensions and Specifications

Dimensions of AutoSampler

Physical

Characteristic Specification

ASX-260 ASX-520

Power 100-240 VAC, 47/63 Hz

Dimensions (mm) 330 (W) x 508 (D) x 610 (H) 520 (W) x 482 (D) x 610 (H)

Weight (kg) 8.4 10.5

Tray 2 racks capacity 4 racks capacity

Physical

Characteristic Specification

ASX-280 ASX-560

Power 100-240 VAC, 47/63 Hz

Dimensions (mm) 355 (W) x 550 (D) x 620 (H) 580 (W) x 550 (D) x 620 (H)

Weight (kg) 8.1 11.7

Tray 2 racks capacity 4 racks capacity

Specifications of Peristaltic Pump

Specifications

Speed (rpm) 0.1 to 100

Flow rate* 0.0002 - 35 ml/min/channel (tubing dependent)

Motor type Stepper motors

Channels 2

Tubing i.d.(mm) 0.13 to 3.17

Temperature, operating (°C) -5 to 40

Humidity Up to 80%

Dimensions (mm) 170 (H) x 125 (W) x 193 (D)

Power 30 W, 100 – 240 VAC, 50/60 Hz

Weight (kg) 2.7

Safety Summary

The following safety symbols are used on this product.

Warning Description

Always refer to the system manual when working near locations at

which the alert mark shown on the left is attached. If the operation,

etc., is performed without heeding the advice in the System manual,

there is a risk of personal injury. In addition, the equipment

performance may be reduced. Moreover, this alert mark is sometimes

used with other marks and descriptions indicating other dangers.

Il faut toujours voir le manuel du système lors de l'exécution de travaux

près des endroits où le panneau d’alerte montré dans la colonne à

gauche est placé. Il y a un risque de blessures, si le travail est effectué

sans respecter les conseils dans le manuel du système. En outre, le

rendement de l'équipement pourrait être réduit. Par ailleurs, ce

panneau d’alerte est parfois utilisé avec d'autres panneaux comportant

les indications de danger.

Warning

When supplying power to this equipment, connect the accessory 3-pin

power cord to a 3-pin grounded power outlet. If a grounded 3-pin

outlet is not available, use a conversion adapter and ground the green

wire. If power is supplied without grounding the equipment, there is a

risk of receiving a fatal electric shock and equipment damage.

Lors de l'alimentation de l’équipement, branchez le cordon

d'alimentation accessoire à 3 broches dans une prise d’alimentation

mise à la terre à 3 broches. Si une prise mise à la terre à 3 broches

n’est pas disponible, utilisez un adaptateur de conversion en raccordant

le fil vert pour réaliser la mise à la terre. Si l'alimentation est fournie

sans mettre l'équipement à la terre, il y a un risque d’électrocution et

de dommages à l’équipement.

“On” (power)

To indicate connection to the mains, at least for mains switches or their

positions, and all those cases where safety is involves.

"On" (Sous tension)

Pour indiquer le branchement à l’alimentation du secteur, au moins

pour les interrupteurs du secteur ou leur position, et tous les autres cas

qui concernent la sécurité.

10 . Lambda 265, 365 and 465 ASX-260/280 AND ASX-520/560 Autosampler Users Guide

“OFF” (power)

To indicate disconnection from the mains, at least for mains switches or

their positions, and all those case where safety is involves.

"OFF" (Hors tension)

Pour indiquer la coupure du secteur, au moins pour les interrupteurs du

secteur ou leur position, et tous les autres cas qui concernent la

sécurité.

Repair

Warning

The user cannot repair this equipment.

DO NOT attempt to open the case or to disassemble internal parts.

Only your PerkinElmer service representative with knowledge of

electrical fire and shock hazard should service this equipment.

There are high-voltage parts in this equipment presenting a risk of

severe injury or fatal electric shock to untrained personnel.

In addition, there is a risk of damage to precision parts.

L'utilisateur ne doit pas essayer de réparer cet équipement.

NE PAS tenter d'ouvrir le boîtier ou de démonter ses pièces internes.

Seul un représentant du service PerkinElmer qui est conscient des

risques d'incendie et d’électrocution devrait réparer cet équipement.

Cet équipement contient des parties à haute tension présentant des

risques de blessure grave ou d’électrocution au personnel non qualifié.

En outre, il existe un risque d'endommagement des pièces de précision.

Falling Over

Caution

This equipment should be used in the correct position. If the equipment

is turned on its side, etc., it will be unstable and may be damaged if it

falls over as a result of receiving a slight mechanical shock.

Cet équipement doit être utilisé dans l’orientation correcte. Si, par

exemple, l'équipement est couché sur un de ses côtés, il deviendra

instable. S’il tombe à la suite d'un léger choc mécanique, il pourra être

endommagé.

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