MRC ROVA-100S Manual de usuario

LED Digital Rotary Evaporator

Operation Instructions

ROVA-100S LED Digital Rotary Evaporator

Please carefully read the Instructions, and use

the product safely under the direction of the

Instructions.

If any information of shapes and performance

indicators changes, we will not notify this

otherwise.

MRC. 1.23

Disclaimer

•The intellectual property right on the manual belongs to MRC Laboratory

Instruments Limited (hereinafter referred to as “the Company”), i.e. relevant

•Products of the company are under the patent protection countries and

regions (including obtained patents and patents being applied for).

•We elaborately prepared the manual in the attitude of being responsible for

the users. But we can’t guarantee that the contents of the manual are fully

correct. If any occasional or subsequent loss is caused by the use of the

Manual, the company will not be liable for this at all.

•The manual is a pure technical document, free of any implication or oblique

hint of any third party. Moreover, we won’t be liable for any user’s

misunderstanding upon the printer’s error(s).

•The company and any of the company’s employees will not bear any liability

for direct/indirect loss of information or stop of business (if any) caused by the

information of the manual or the product it mentions.

•The company reserves the right to change specification & price of the product.

•If any information of the manual changes, we will not notify this otherwise.

•The manual and any content of it must not be copied, abstracted or modified

in any form without the company’s written approval in advance.

Contents

Introduction........................................................................................................... 1

How to acquire help .............................................................................................. 1

Warranty ............................................................................................................... 1

1.Safety notes....................................................................................................... 2

2.Scope of application .......................................................................................... 8

3.Inspection .......................................................................................................... 9

3.1 Open-package inspection.......................................................................... 9

3.2 Package list ............................................................................................. 10

4.Control and display .......................................................................................... 11

4.1 Control..................................................................................................... 11

4.2 Display .................................................................................................... 15

5.Installation and testing ..................................................................................... 17

5.1 Installation ............................................................................................... 17

5.2 Testing ..................................................................................................... 21

6.Fault diagnosis ................................................................................................ 23

7.Maintenance and cleaning ............................................................................... 24

8.Relevant standards.......................................................................................... 26

9.Technical parameters....................................................................................... 27

Introduction

Welcome to use the Operating Instructions of Rotary Evaporator. Users are advised

to read carefully this manual before using this instrument, operate the instrument

according to the instructions contained herein and be aware of all precautions.

How to acquire help

If you encounter any problems or need help while installing or using this instrument,

please immediately contact the After-sales Service Department of the manufacturer

/ supplier.

Please prepare the following information and materials:

•Product serial number (on the instrument nameplate)

•Warranty card

•Description of problem phenomenon

•The method and operating steps you have undertaken to resolve the problem

•Your contact details including telephone number, fax number and email address.

Warranty

According to the manufacturer’s warranty clause, the warranty period of the product

is 24 months (since the purchase date) provided that it is used by the normal

operation method under the normal service conditions specified in the Manual. This

warranty does not cover any performance degradation of or damage to the

instrument due to incorrect installation or operation, unauthorized disassembly or

repair or any other violations of the operating instructions contained herein. If any

related problem described in the terms of warranty occurs, please contact the

manufacturer / supplier.

1.Safety notes

•Please carefully read the Manual before operating the product, and observe

the specifications on safe operation.

•Please properly keep the operating instructions for easy reference in case of

need.

•Please ensure only suitably trained personnel can operate this instrument.

•Please comply with the safety rules, personal safety and accident prevention

norms, especially when creating vacuum!

•According to the type of medium handled, please wear suitable protective

devices when operating the instrument; otherwise, the following dangers may

occur:

-Splatter of liquids

-Fly-out of parts

-Contamination of human body, hair or clothes by splattered substances

•Warning! Inhale of contact with toxic liquids, gases, spatters, vapor, dust,

biological or microbiological medium might cause damage to the operator.

•Place the instrument on a stable, clean, antiskid, dry & fireproof table surface.

•Make sure there is sufficient space above the instrument and the glass

assembly might exceed the height of the instrument.

•Before use, please carefully examine the instrument and accessories

especially the glass assembly for any damage. Please do not use any

damaged parts.

•Ensure the glass assembly is free of stress! Each of the following reasons

might result in damage to the glass assembly:

-Stress due to incorrect installation

-Effect of external mechanical force

-Sharp change to the ambient temperature

•Ensure the instrument will not move due to vibration when turning on the

instrument.

•Note the danger caused by the following circumstances:

- Flammable substance

- Flammable low-boiling-point medium

- Breakage of glass component

•Warning! Never distill or heat any substance whose ignition point is lower than

the temperature set for the safety of the heating bath.

•The heating bath’s safety temperature shall at least 25 °C lower than the

ignition point of the medium being handled.

•Please don’t operate or use this instrument in an explosive environment or

underwater or use this instrument to handle any dangerous substance.

•This instrument is only suitable for the medium that does not react with the

energy generated in the handling process in a way that might cause danger.

Meanwhile, the substance being handled may not produce danger due to

energy generated in any other manner such as illumination reaction.

•The instrument must be monitored all the time when operating the instrument.

•Please don’t operate this instrument under overpressure.

•To ensure the effective condensation of the motor system, please do not block

the vent of the motor system.

•Only use of the accessories in the list of “optional accessories” can guarantee

the operational safety.

•Please refer to the operating instructions for heating kettle.

•Please refer to the operating instructions for optional accessories.

•Please use this instrument in a closed fume hood or other suitable protective

device.

•Select the distilling device according to the amount to be distilled and the

distillation type. The condenser must work normally. Please monitor the flow

rate of the coolant at the outlet of the cooler.

•To prevent pressure buildup, the glass assembly shall be kept vented when

operating under normal pressure, such as keeping the condenser open.

•Please note that gases, vapor or other substances can pose danger through

overflow from the upper opening of the condensation tube. To minimize or

avoid such danger, please take suitable measures, such as connecting the

cooling tube and scrubbing bottle or other effective extraction devices

downwards.

•The glass evaporating flask may not be heated on one side. The rotating

evaporating flask must rotate at the heating phase.

•The glass assembly’ design pressure tolerance is 10mbar. The venting valve

(see the part of “Testing”) must be opened before heating and once again after

cooling. When performing vacuum distillation, the steam must be condensed

before release or released safely.

If the residue after distillation is likely to be decomposed when exposed to

oxygen, please add only gas for stress release into it.

•Warning! Please be careful be avoid the formation of peroxides, as the

decomposition of peroxides accumulated in the distillation process might result

in explosion.

Please protect any liquid forming peroxides from ray of light, especially

ultraviolet irradiation. Please be careful to examine formation of any peroxides

before distillation and to remove the peroxides if any. Many organics are easy

to form peroxides, such as methoxypyridine, diethyl ether, dioxane,

tetrahydrofuran, unsaturated hydrocarbostyril, such as tetrahydronaphthalene,

diene, isopropylbenzene, ketone and solutions of the aforesaid substances.

•Warning! The heating bath, heating medium, evaporating flask and glass

assembly might become hot in the operation process and remain hot for a

while after stop of the operation! Before further operation, please let each part

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