Micromeritics FLEX Series Manual de usuario

PRE-INSTALLATION INSTRUCTIONS AND

CHECKLIST

350-42870-01

Apr 2021

(Rev H)

FLEX™SERIES

SURFACE AND CATALYST CHARACTERIZATION ANALYZER

TRADEMARKS

Alconox is a registered trademark of the Alconox Company.

Flex is a registered trademark of Micromeritics Instrument Corporation.

FlowPrep is a trademark of Micromeritics Instrument Corporation.

MicroActive is a trademark of Micromeritics Instrument Corporation.

Micromeritics is a registered trademark of Micromeritics Instrument Corporation.

Microsoft and Windows are registered trademarks of Microsoft Corporation.

Smart VacPrep is a trademark of Micromeritics Instrument Corporation.

The software described in this manual is furnished under a license agreement and may be used or

copied only in accordance with the terms of the agreement.

____________________________________________________________________________

CORPORATE PROFILE

Micromeritics Instrument Corporation is the world’s leading supplier of high-performance systems

to characterize particles, powders and porous materials with a focus on physical properties,

chemical activity, and flow properties. Our technology portfolio includes: pycnometry, adsorption,

dynamic chemisorption, particle size and shape, intrusion porosimetry, powder rheology, and

activity testing of catalysts. The company has R&D and manufacturing sites in the USA, UK, and

Spain, and direct sales and service operations throughout the Americas, Europe, and Asia.

Micromeritics systems are the instruments-of-choice in more than 10,000 laboratories of the

world’s most innovative companies, prestigious government, and academic institutions. Our

world-class scientists and responsive support teams enable customer success by applying

Micromeritics technology to the most demanding applications. For more information, please visit

www.Micromeritics.com.

Corporate Profile

Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021 iii

Micromeritics Instrument Corporation

4356 Communications Drive

Norcross, GA / USA / 30093-2901

Phone: 1-770-662-3636

Fax: 1-770-662-3696

www.Micromeritics.com

Instrument Service or Repair

Phone: 1-770-662-3666

International — contact your local distributor or call 1-770-662-3666

[email protected]

Micromeritics Learning Center

Phone: 1-770-662-3607

www.Micro.edu

iv Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021

ABOUT THIS MANUAL

All references to 3500, Flex, or Flex Series in this document encompass the Flex,

3Flex, and Flex Confirm environments unless otherwise noted.

The following symbols or icons indicate safety precautions and/or supplemental information and

may appear in this manual:

NOTE— Notes contain important information applicable to the topic.

CAUTION — Cautions contain information to help prevent actions that may damage

the analyzer or components.

WARNING — Warnings contain information to help prevent actions that may cause

personal injury.

NOTE— Notes that apply to 21CFR11 environments only (Confirm applications).

Dynamic Analysis and Chemisorption options are not applicable when the software is

installed in 21CFR11 environments.

About this Manual

Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021 v

General Safety

GENERAL SAFETY

Do not modify this instrument without the authorization of a Micromeritics service per-

sonnel.

Toxic or flammable gases require proper venting of exhaust.

Use caution in the areas where this symbol is displayed on the instrument — such as

the heating mantles and furnace. These surfaces may be hot and could cause serious

burns. Use the gloves supplied in the accessories kit.

Any piece of laboratory equipment can become dangerous to personnel when improperly

operated or poorly maintained. All employees operating and maintaining Micromeritics

instruments should be familiar with its operation and should be thoroughly trained and instructed

on safety.

nRead the manual for any special operational instructions for the instrument.

nKnow how the instrument functions and understand the operating processes.

nWear the appropriate personal protective equipment when operating this instru-

ment — such as eye protection, lab coat, protective gloves, etc.

nWhen lifting or relocating the instrument, use proper lifting and transporting devices

for heavy instruments. Ensure that sufficient personnel are available to assist in

moving the instrument. The Flex weighs approximately 103 - 106 kg (227 - 234lb)

depending on configuration.

nAlways pay attention to the safety instructions provided on each label affixed to the

instrument and do not alter or remove the labels. When inspecting the instrument,

ensure that the safety labels have not become worn or damaged.

nThe Flex has a safety shield. Ensure it is in place when operating the instrument.

nProper maintenance is critical to personnel safety and smooth instrument oper-

ation and performance. Instruments require regular maintenance to help promote

safety, provide an optimum end test result, and to prevent costly down time. Failure

to practice proper maintenance procedures can lead to unsafe conditions and

shorten the life of the instrument.

nImproper handling, disposing of, or transporting potentially hazardous materials

can cause serious bodily harm or damage the instrument. Always refer to the

MSDS when handling hazardous materials. Safe operation and handling of the

instrument, supplies, and accessories is the responsibility of the operator.

vi Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021

INTENDED USE

Micromeritics Flex Surface Characterization Analyzer is a fully automated one, two or three

station instrument capable of high-performance physisorption and chemisorption analyses with

superior accuracy, resolution, and data reduction.

The instrument is intended to be operated by trained personnel familiar with the

proper operation of the equipment recommended by the manufacturer as well as

relevant hazards involved and prevention methods. All use, other than that described

in this manual, is seen as unintended use and can cause a safety hazard.

The instrument is intended to be used as per applicable local and national regulations.

General Safety

Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021 vii

General Safety

TRAINING

It is the responsibility of the customer to ensure that all personnel operating or maintaining the

equipment participate in training and instruction sessions. All personnel operating, inspecting,

servicing, or cleaning this instrument must be properly trained in operation and machine safety

before operating this instrument.

ENVIRONMENTALLY FRIENDLY USE PERIOD

Part Name

Hazardous Substances

Lead

(Pb)

Mercury

(Hg)

Cadmium

(Cd)

Hexavalent

Chromium

(Cr (VI))

Polybrominated

biphenyls

(PBB)

Polybrominated

diphenyl ethers

(PBDE)

Cover x o o o o o

Power

Supplies x o o o o o

Printed

Circuit

Boards

x o o o o o

Cables, Con-

nectors &

Transducers

x o o o o o

Hazardous Substances Table

o Hazardous substance is below the specified limits as described in SJ/T11363-2006.

x Hazardous substance is above the specified limits as described in SJ/T11363-2006.

The Environmentally Friendly Use Period (EFUP) for all enclosed products

and their parts are per the symbol shown here, unless otherwise marked. Cer-

tain parts may have a different EFUP (for example, battery modules) and so

are marked to reflect such. The Environmentally Friendly Use Period is valid

only when the product is operated under the conditions defined in the product

manual.

viii Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021

Table of Contents

Corporate Profile iii

About this Manual v

General Safety vi

1 Pre-installation Document Overview 1 - 1

Micromeritics Installed Instruments Only 1 - 2

2 Pre-installation Instructions 2 - 1

Unpacking and Inspection 2 - 1

Shipping Damage 2 - 1

Analyzer Space 2 - 2

Installation Configuration 2 - 3

Computer System 2 - 3

Environmental Factors 2 - 5

Power 2 - 5

Gas Supply 2 - 6

Laboratory Equipment and Supplies 2 - 10

3 Pre-installation Checklists 3 - 1

Unpacking and Inspection Checklist 3 - 1

Analyzer Space Checklist 3 - 1

Installation Configuration Checklist 3 - 2

Environmental Factors Checklist 3 - 2

Gas Supply Checklist 3 - 3

Computer System Checklist 3 - 4

Degas Unit Checklist 3 - 4

Laboratory Equipment and Supplies Checklist 3 - 5

Application Related Issues Checklist 3 - 5

Flex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021 ix

Personnel Security Clearance Checklist 3 - 5

4 Pre-installation Instructions — 21CFR11 Environments 4 - 1

5 Pre-installation Checklist — 21CFR11 Environments 5 - 1

Personnel Requirements 5 - 1

User Information Requirements 5 - 2

Users and Groups Worksheet for 21CFR11 5 - 3

6 Dates and Signatures — All Environments 6 - 1

Projected Installation Date 6 - 1

Commitment Statement and Signature Form 6 - 1

Flex 3500 Declaration of Conformity DoC - 1

xFlex Series Pre-installation Instructions and Checklist

350-42870-01 (Rev H) — Apr 2021

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