Hach Polymetron 9240 Manual rápido

DOC024.98.93034

POLYMETRON Model

9240 Multi-Channel Sodium

Analyzer

05/2018, Edition 13

Basic User Manual

Allgemeines Benutzerhandbuch

Manuel d'utilisation de base

Manual básico del usuario

Manuale di base per l'utente

Podstawowa instrukcja obsługi

Grundlæggende brugervejledning

Allmän användarhandbok

Osnovni uporabniški priročnik

Alapvető felhasználói kézikönyv

Βασικό εγχειρίδιο χρήσης

Temel Kullanıcı Kılavuzu

English..............................................................................................................................3

Deutsch.......................................................................................................................... 26

Français......................................................................................................................... 51

Español.......................................................................................................................... 75

Italiano............................................................................................................................ 99

Polski............................................................................................................................ 123

Dansk............................................................................................................................148

Svenska....................................................................................................................... 172

Slovenski..................................................................................................................... 195

Magyar......................................................................................................................... 218

Ελληνικά...................................................................................................................... 242

Türkçe...........................................................................................................................268

Specifications

Specifications are subject to change without notice.

Specification Details

Measuring range 0 to 10,000 ppb freely programmable

0 to 200 ppm with K-Kit option

Accuracy Non-cationic application: ± 0.1 ppb or ± 5% of reading, whichever is greater

Cationic application: ± 2 ppb or 5% reading, whichever is greater

Repeatability < 0.02 ppb or 1.5% reading, whichever is greater within 10°C variation

Average response

times at 25°C with

a maximum ΔT

=15°C between

channels

T90% ≤ 10 min

Concentration step from

one channel to another

Max. temp variation

(°C)

Time to reach accuracy 0.1 ppb or 5%

up down

0.1 ↔ 5 ppb 3 9 min 27 min

0.1 ↔ 50 ppb 3 11 min 41 min

0.1 ↔ 200 ppb 3 9 min 45 min

< 0.1 ↔ 1 ppb 3 29 min 36 min

0.1 ↔ 50 ppb 15 11 min 41 min

Electrode type pH glass electrode

Number of

channels

1 to 4

Interference

phosphate 10 ppm

Measurement variation less 0.1 ppb

Sample

temperature

interference

< 0.5% / °C

Typical

environment

Power station / indoor / demineralized water plant or instrumentation room

Suspended solids < 2 NTU, no oil, no grease

Temperature range

for storage

-20 to 60°C (2 to 140°F)

Relative humidity 10 to 80%

Ambient

temperature

5 to 50°C (41 to 122°F)

Sample

temperature

variation

Stabilization in 10 mins from 15°C to 30°C

Use the static heat exchanger system when the temperature difference between samples is

higher than 15°C

pH range of

sample

Non-cationic application: 6 to 10 pH

Cationic application: 2 to 10 pH

Flow rate 6 to 9 L/hour

Pressure 0.2 to 6 bar (3 - 87 psi)

Acidity Less than 250 ppm (equivalent CaCO3)

Power supply

voltage fluctuation

± 10%

English 3

Specification Details

Over voltage

category

Cat II, Class 1 (overvoltage < 1500V)

Maximum panel

dimension (H x L x

850 x 450 x 252.5mm [33.46 x 17.71 x 9.94in]

Inlet Simple fittings for 6 mm O.D. tubing or ¼" O.D. in PE-low density. ¼" OD in PHED-PTFE-

SS as option

Outlet Barbed stem for 12 mm (½" I.D.) hose

Protection rate Transmitter: IP65 (NEMA 4)

Panel: IP50 (dust protection)

Optional Enclosure: IP54 (splash water proof)

Instrument is designed to avoid DIPA vapor inside the enclosure. All DIPA vapor is

collected and sent to the instrument drain

Cell PMMA - compact (minimum tubing)

Flame rate Conform UL

Maximum weight 15 - 30 Kg

Mains power

supply

100 - 240 VAC, 50-60 Hz, ± 10%, automatic switching

Max. consumption 80 VA

Fuse 5 x 20 cartridge T2AL-250V following CEI127

Display Curve trend, Last Cal Date, Historical, Concentration, Temperature, Potential

Analog outputs Number: 6

4-20 or 0-20 mA (650 ohms)

Linear / Dual / Logarithm

Event indication

Relays 4 x Relay (conc)

1 x Warning

1 x System

Logic input Active / Inactive channels

Remote AutoCal

EMC requirements EN61326-1: EMC Directive

Note: This is a Class A product. In a domestic environment this product may cause radio interference in

which case the user may be required to take adequate measures.

NOTICE

Measurement variations of less than 5% of the full range can occur if the instrument is

subject to a strong electromagnetic field.

4 English

Specification Details

Korean

registration

User Guidance for EMC Class A Equipment

업무용을 위한 EMC 등급 A 장치에 대한

사용자 지침

사용자안내문

A 급 기기 ( 업무용 방송통신기자재 )

이 기기는 업무용 (A 급 ) 전자파적합기기로서 판매자 또는 사용자는 이 점을 주의하시기 바

라며 , 가정외의 지역에서 사용하는 것을 목적으로 합니다.

CE compliance EN61010-1: LVD Directive

International

standards

cETLus

Warranty Instrument: 1 year (EU: 2 years)

Electrodes: 6 months

General information

In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential

damages resulting from any defect or omission in this manual. The manufacturer reserves the right to

make changes in this manual and the products it describes at any time, without notice or obligation.

Revised editions are found on the manufacturer’s website.

Safety information

N O T I C E

The manufacturer is not responsible for any damages due to misapplication or misuse of this product including,

without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent

permitted under applicable law. The user is solely responsible to identify critical application risks and install

appropriate mechanisms to protect processes during a possible equipment malfunction.

Please read this entire manual before unpacking, setting up or operating this equipment. Pay

attention to all danger and caution statements. Failure to do so could result in serious injury to the

operator or damage to the equipment.

Make sure that the protection provided by this equipment is not impaired. Do not use or install this

equipment in any manner other than that specified in this manual.

Use of hazard information

D A N G E R

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.

WARNING

Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious

injury.

CAUTION

Indicates a potentially hazardous situation that may result in minor or moderate injury.

N O T I C E

Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special

emphasis.

English 5

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument

could occur if not observed. A symbol on the instrument is referenced in the manual with a

precautionary statement.

This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential

injury. If on the instrument, refer to the instruction manual for operation or safety information.

This symbol indicates that a risk of electrical shock and/or electrocution exists.

This symbol indicates the presence of devices sensitive to Electro-static Discharge (ESD) and

indicates that care must be taken to prevent damage with the equipment.

This symbol, when noted on a product, indicates the instrument is connected to alternate current.

Electrical equipment marked with this symbol may not be disposed of in European domestic or

public disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no

charge to the user.

Products marked with this symbol indicates that the product contains toxic or hazardous substances

or elements. The number inside the symbol indicates the environmental protection use period in

years.

Products marked with this symbol indicates that the product conforms to relevant South Korean

EMC standards.

6 English

Overview

Figure 1 Front and rear panels

1 User interface 7 Frame for panel mounting

2 Overflow vessel 8 Reagent canister holder

3 Measuring cell 9 Local controller box

4 Flow rate adjustment for each channel 10 Electrolyte reservoir

5 Door lock 11 Pump box

6 Reagent shelf 12 Sample inlet valves

Installation

WARNING

The analyzer should only be assembled by qualified staff. Mains power should only be connected once

installation has been completed and checked

Mounting the analyzer

WARNING

Do not connect power prior to mounting and plumbing the instrument.

CAUTION

Personal injury hazard. Instruments or components are heavy. Use assistance to install or move. Make sure that

the wall mounting is able to hold 4 times the weight of the equipment.

CAUTION

Wherever the analyzer is to be mounted, it is important to note that it must be placed in an upright position with

the transmitter at the top. It is recommended to use a spirit level to ensure that the analyzer is correctly positioned

and not leaning to one side or forward. This is essential to guarantee the accuracy of the analyzer.

English 7

Panel mounting

Mount the analyzer using the fixation holes located around the outside of the analyzer.

Wall mounting

Use the wall mounting kit to fix the instrument to the wall. The distance between the two pieces is

460 mm.

CAUTION

It is extremely important to respect this gap of 460 mm to avoid bending the cabinet out of shape while fitting.

Mains power connection

WARNING

No intervention should be made on the instrument without first switching off the power.

The electrical installation should be carried out by duly qualified personnel. A supply voltage of

100-240 VAC is acceptable without changing the configuration. The power supply terminals can be

removed from their housing to make connection easier.

For safety reasons, it is imperative to respect the working procedure below:

• Use a three-wire power cable (live + neutral + earth), sized for supplying the required power.

• The instrument should be connected to the mains via a circuit-breaker or fuse whose value should

be less or equal to 20 A. It should be located in proximity and be identified. This connection should

cut-off the live and the neutral when electrical problems occur or when the user wishes to

intervene inside the instrument. On the other hand, the earth conductor should always be

connected.

The main cabinet should be open with access to the interior.

1. Pass the power cable through the cable gland located at the back left of the bottom of the

cabinet.

2. Open the back of the local controller box (No. 11 in Figure 1 on page 7) by unscrewing the

6 screws.

3. Unscrew the two holding screws on the upper left and right side of the box, and allow it to rotate

down to reveal the back of the transmitter. The cable gland for the power cable is located left and

nearest to you.

4. Unscrew the cable gland nut, pass the power cable through it, and then up through the cable

gland and into the transmitter (No. 2). Screw back the cable gland nut to secure the power cable.

5. Open the transmitter front door by unscrewing the four holding screws.

6. Swing open the door (it is hinged to the left) to reveal the inside of the transmitter.

7. Remove the metallic shielding plate (No. 1) protecting access to the main board.

8. Remove the power supply connector (No. 3) and note where the earth, neutral and live (E, N, L)

must be connected.

9. Connect the power supply cables to the connector.

8 English

10. Put the connector back in place (No. 4).

11. Replace the metallic shielding plate, ensuring it is in front of the power cable just installed.

External communications connection

1. Run the communications cable through an external cable gland on

the bottom of the cabinet, and into the analyzer.

2. Pass it through the cable gland located right and farthest from you

on the base of the transmitter, so it appears inside the transmitter

through the left front cable gland.

3. Connect the communication cable as indicated. Connection is the

same on the CPU board for both the JBUS/ MODBUS and

PROFIBUS options.

4. Close the transmitter door and secure in place with the 4 screws.

5. Put the local controller box back in its normal position and secure in

place with the 2 holding screws.

Input/Output connections

Before using any of the cable glands, perforate first with a screwdriver. To ensure a good seal, the

external diameter of the cables should be between 5 and 7 mm. The nomenclature given in the

connections column of the following table refers to the same nomenclature that is printed on the I/O

board against each available connection.

Connections Function

Re1 to Re6 User relays - see Alarms on page 17 for more information on the relays

Re7 Warning alarm

Re8 System alarm

In2 For remote calibration

In4 to In7 By-pass channel measurement (channel 4 - 1 respectively)

Iout0 Used for the current measurement signals

Iout1 to Iout7 Can be freely linked to different parameters like measurement, temperature - refer to the section

entitled mA outputs on page 18 for details

On completion, close the local controller box (No. 11 in Figure 1 on page 7) and secure in place with

the 6 screws.

Sample tubes installation

Connecting the sample

Use new tubes for connections during installation

• Exterior Ø: 6 mm exactly (or ¼'')

• Material: polyethylene or PTFE or FEP

• Flow rate: 6 to 9 L/hour

• Pressure: 0.2 to 6 bar (8-100 psig)

• Sample acidity: sample acidity should not be more than 300 ppm CaCO3

• Temperature: 5 to 45°C

At this stage of the installation, make sure that the flow valve is closed. Connect the pipes by

inserting them into the quick release connections found on the bottom of the analyzer under the

sampling block (No. 14 in Figure 1 on page 7). Be sure that the sample line is correctly flushed

before any connection to avoid particle injection into the hydraulic system. If particulate matter is

English 9

present in the sample, pre-filtration is necessary. A filter should be inserted in the sample line. One is

available as an option. Connect one inlet and one outlet per channel.

Connecting the drain tube

The drain outlet is located on the bottom of the analyzer. A 12 x 17 mm pipe is delivered with the

analyzer and should be connected to the drain outlet at one end and the other fed to a drain for

sample evacuation.

Reagents installation

The canisters are installed in the canister holder (No. 10 in Figure 1 on page 7).

1. Prepare the reagents.

2. Install and connect the conditioning solution (diisopropylamine).

3. Install and connect the reactivation solution (blue R label).

4. If you have this option, install and connect the auto calibration solution

(yellow CAL label).

Magnetic stirrer installation

1. On the front of the panel, remove the plastic bag from the overflow vessel (No. 5 in Figure 1

on page 7).

2. Remove the magnetic stirrer from the bag and install it in the overflow vessel.

Reagents volume declaration

Note: As you will now be using the analyzer menus to input data, it may be useful to familiarize yourself with the

data entry procedures by reading the section entitled User interface on page 12.

1. Open the sample valve and check that there is no leakage in the hydraulic path.

2. Power on the analyzer.

3. Select the Menu option from the display.

4. Select MAINTENANCE/DIAG. from the main menu and press Enter.

5. Select the REAGENT CHANGES option and press Enter.

6. Set the BOTTLES FULL parameter to Yes and press Enter.

7. Press Esc to return to the MAINTENANCE/DIAG. menu.

Flow rate adjustment

1. From the MAINTENANCE/DIAG. menu select START UP and press Enter.

2. First, the system automatically primes both the calibration and reactivation tubes.

3. Check that there are no air bubbles in the reagent tubes for reactivation and auto calibration.

4. The next step allows you to regulate the sample flow rate on each measurement channel. The

name of the channel to regulate is displayed.

5. The analyzer automatically empties and refills the overflow vessel to determine the flow rate

which is displayed on screen.

6. The flow rate for each channel should be 6 to 9 L/hour.

7. Using a screwdriver, regulate the channel’s sample flow (No. 3 in Figure 1 on page 7) by turning

counter-clockwise to increase the flow rate or clockwise to decrease the flow rate.

8. The process is repeated until the flow is correctly regulated for the channel. At this point select

OK.

10 English

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