Dionex ICS-2100 Manual de usuario

ICS-2100 Ion Chromatography System

Installation Instructions

Document No. 065294

Revision 01

March 2009

Printed in the United States of America.

This publication is protected by federal copyright law. No part of this publication

may be copied or distributed, transmitted, transcribed, stored in a retrieval system, or

transmitted into any human or computer language, in any form or by any means,

electronic, mechanical, magnetic, manual, or otherwise, or disclosed to third parties

without the express written permission of Dionex Corporation, 1228 Titan Way,

Sunnyvale, California 94088-3603 U.S.A.

DISCLAIMER OF WARRANTY AND LIMITED WARRANTY

THIS PUBLICATION IS PROVIDED “AS IS” WITHOUT WARRANTY OF

ANY KIND. DIONEX CORPORATION DOES NOT WARRANT,

GUARANTEE, OR MAKE ANY EXPRESS OR IMPLIED

REPRESENTATIONS REGARDING THE USE, OR THE RESULTS OF THE

USE, OF THIS PUBLICATION IN TERMS OF CORRECTNESS, ACCURACY,

RELIABILITY, CURRENTNESS, OR OTHERWISE. FURTHER, DIONEX

CORPORATION RESERVES THE RIGHT TO REVISE THIS PUBLICATION

AND TO MAKE CHANGES FROM TIME TO TIME IN THE CONTENT

HEREINOF WITHOUT OBLIGATION OF DIONEX CORPORATION TO

NOTIFY ANY PERSON OR ORGANIZATION OF SUCH REVISION OR

CHANGES.

TRADEMARKS

AES, Atlas, Chromeleon, EluGen, and SRS are registered trademarks of Dionex

Corporation.

Microsoft, Windows, and Windows Vista are registered trademarks of Microsoft

Corporation.

PEEK is a trademark of Victrex PLC.

PRINTING HISTORY

Revision 01, March 2009

Doc. 065294-01 3/09 i

1. Facility Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

2. Unpacking the IC System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

3. Connecting an Autosampler (Optional) . . . . . . . . . . . . . . . . . . . . . . . . . . 4

3.1 Connecting an AS-DV Autosampler . . . . . . . . . . . . . . . . . . . . . 4

3.2 Connecting an AS Autosampler . . . . . . . . . . . . . . . . . . . . . . . . . 5

4. Unpacking the PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

5. Installing Chromeleon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

6. Installing the Chromeleon Software License Dongle . . . . . . . . . . . . . . 10

7. Installing the Software License . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

8. Starting the Chromeleon Server . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

9. Connecting to the Chromeleon PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

9.1 Connecting the IC System to the PC . . . . . . . . . . . . . . . . . . . . 13

9.2 Connecting Additional USB Devices . . . . . . . . . . . . . . . . . . . . 14

10. Connecting the Power Cord . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

11. Installing the ICS-2100 Device Driver . . . . . . . . . . . . . . . . . . . . . . . . . 17

12. Setting Up Chromeleon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

12.1 Creating a Timebase . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

12.2 Configuring the Device Properties . . . . . . . . . . . . . . . . . . . . . . 21

12.3 Connecting to the Panel Tabset . . . . . . . . . . . . . . . . . . . . . . . . 24

12.4 Verifying Chromeleon Communication . . . . . . . . . . . . . . . . . . 25

13. Installing and Plumbing the Columns and Suppressor . . . . . . . . . . . . . 26

13.1 Unpacking the Columns and Suppressor . . . . . . . . . . . . . . . . . 27

13.2 Setting Up the Column Heater . . . . . . . . . . . . . . . . . . . . . . . . 27

Contents

ICS-2100 Installation Instructions

ii Doc. 065294-01 3/09

13.3 Plumbing the Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29

13.4 Installing the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30

14. Connecting the Waste Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31

14.1 Installing the Waste, Gas Separator Tube . . . . . . . . . . . . . . . . .32

15. Setting Up the Eluent Reservoir . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33

16. Entering the Eluent Level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34

17. Priming the Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35

17.1 Priming the Eluent Lines with a Syringe . . . . . . . . . . . . . . . . .35

17.2 Priming the Pump Heads with the Prime Button . . . . . . . . . . . .37

18. Setting Up the Eluent Generator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38

18.1 Eluent Generator Setup for KOH, LiOH, MSA, and

NaOH Eluents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38

18.2 Eluent Generator Setup for Carbonate/Bicarbonate Eluent . . . .54

18.3 Eluent Generator Setup for Carbonate Eluent . . . . . . . . . . . . . .80

19. Equilibrating the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .97

19.1 EluGen Cartridge Backpressure Requirements . . . . . . . . . . . . .97

20. Verifying Operational Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .98

21. Connecting the Analog Output (Optional) . . . . . . . . . . . . . . . . . . . . . .100

22. Pressurizing the Eluent Reservoir (Optional) . . . . . . . . . . . . . . . . . . . .100

22.1 Connecting the Gas Source . . . . . . . . . . . . . . . . . . . . . . . . . . .101

22.2 Applying the Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102

23. Connecting the Pump Continuous Seal Wash (Optional) . . . . . . . . . .103

24. Sample Processing Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .105

25. Troubleshooting the USB Configuration Error . . . . . . . . . . . . . . . . . .106

Doc. 065294-01 3/09 1

Installation

This document provides instructions for the initial installation of the ICS-2100 Ion

Chromatography System

NOTE The order of the steps is important. It is especially

important to install the Chromeleon®Chromatography

Management System before connecting the USB cable

and turning on the system power.

1. Facility Requirements

•Make sure the installation site meets the following environmental

specifications:

Main Power: 100 to 240 Vac, 50 to 60 Hz (Auto-sensing power supply; no

manual voltage or frequency adjustment required)

Operating Temperature: 4 to 40 °C (40 to 104 °F)

Humidity: 5% to 95% relative humidity, noncondensing

•Provide a sturdy workbench for the system of a height that ensures convenient

access to the interior of the ICS-2100.

•Allow at least 15 cm (6 in) behind the system for power connections and

ventilation. For optimal performance, install the system in a draft-free

location, out of the path of air conditioning and heating vents.

•(Optional) For pressurization of the eluent reservoir, provide a clean gas

source regulated to between 0.55 and 0.83 MPa (80 and 120 psi). An air

regulator accessory (P/N 060054) is required to regulate the pressure to

between 0.03 and 0.04 MPa (5 and 6 psi).

Do not pressurize the eluent reservoir above 0.07 MPa (10 psi).

Ne mettez jamais les réservoirs d'éluants sous une pression

supérieure à 0,07 MPa (10 lb/po²).

ICS-2100 Installation Instructions

2Doc. 065294-01 3/09

•Use ASTM filtered, Type I (18-megohm) deionized water when preparing

eluent and regenerant.

2. Unpacking the IC System

1. Open the shipping box (see

Figure 1) and remove the top

layer of foam.

Figure 1. Unpacking the ICS-2100

2. Open the plastic bag that

covers the IC system (see

Figure 2).

Figure 2. IC System Enclosed in Bag

Setzen Sie den Eluentbehälter auf keinen Fall einem Druck über

0,07 MPa aus.

(Remove this foam)

Eluent

Bottle

EGC Holder

(upside down)

Unpacking the IC System

Doc. 065294-01 3/09 3

3. Set the eluent bottle on top of

the ICS-2100 (see Figure 3).

4. TURN OVER THE EGC

HOLDER, and set it on top

of the ICS-2100.

Figure 3. ICS-2100 After Installing

Eluent Bottle and EGC Holder

5. Remove the next layer of

foam and remove the Ship Kit

(P/N 064375) (see Figure 4).

6. The bottom layer of foam has

two cutouts on either side of

the module; use these as

handholds when lifting the IC

system.

Figure 4. IC System with Ship Kit

7. Lift the IC system off the bottom layer of foam and out of the box. Set it on a

workbench.

Two or more persons should lift the IC system, which weighs 30 kg

(66 lb). Lift the IC system only from each side of the cabinet bottom.

Lifting from the front door will damage the door hinges.

Au moins deux personnes peuvent soulever le chromatograph

ionique: il pèse 30 kg (66 lb). Ne soulevez le chromatograph ionique

que par chaque côté du fond de l'armoire. Son soulèvement par la

porte du panneau avant endommagera les charnières de la porte.

EGC Holder

(right-side up)

Ship

Kit

ICS-2100 Installation Instructions

4Doc. 065294-01 3/09

8. Inspect the system for any shipping damage. Remember to save the shipping

container and all packing material. You will need them in future if the IC

system is shipped.

3. Connecting an Autosampler (Optional)

To connect an AS-DV or AS Autosampler to the injection valve in the IC system,

follow the instructions in the appropriate section below.

Notes:

•If an optional auxiliary valve is installed in the ICS-2100, it can be used as the

injection valve, instead of the standard valve configured with each system.

After connecting the autosampler to the auxiliary valve (as described in the

appropriate section below), configure the valve as the injection valve in

Chromeleon. For instructions, refer to Installing the ICS-1100/1600/2100

Auxiliary Valve (Document No. 065288). The document is provided with the

valve.

•To connect an AS-HV Autosampler, refer to the instructions in the AS-HV

Autosampler Operator’s Manual (Document No. 065125). The manual is

provided on the Dionex Reference Library CD-ROM (P/N 053891).

3.1 Connecting an AS-DV Autosampler

1. Place the AS-DV to the left of the IC system on the workbench.

2. Open the IC system and the autosampler doors.

Das IC system wiegt über 30 kg. Daher sollte das Gerät nur von zwei

oder mehr Personen angehoben werden. Greifen Sie dazu an beiden

Seiten unter das Gerät. Heben Sie den Ionenchromatographen nicht

an der Vordertür an, da dadurch die Türangeln beschädigt werden

könnten.

Connecting an Autosampler (Optional)

Doc. 065294-01 3/09 5

3. Route the sample outlet line

from the AS-DV through

the left side slot, at the front

of the IC system.

4. Connect the outlet sample

line from the AS-DV to port

S(5)on the injection valve

(see Figure 5).

Figure 5. IC System Injection Valve

3.2 Connecting an AS Autosampler

NOTE Dionex recommends using AS models that do not

have injection valves. If a valve is installed in the

autosampler, it is switched at the same time as the

valve in the IC system. This causes unnecessary

wear on the autosampler valve. If your AS has an

injection valve, contact Dionex for assistance.

1. Place the autosampler to the left of the IC system on the workbench.

2. Open the IC system and the autosampler doors.

3. Route the needle seal line that extends from the autosampler inject

port through the autosampler right side slot (see Figure 6) and then

through the IC system left side slot to the injection valve.

Figure 6. AS Autosampler Drip Tray and Right Side Slot

AS-DV

Sample

Outlet Line

Insert the waste line

from the IC system

injection valve here

Route the autosampler

needle seal line to the

injection valve inside

the IC system

ICS-2100 Installation Instructions

6Doc. 065294-01 3/09

4. Connect the needle seal line to port S (5) on the injection valve (see Figure 7).

A coupler (see Figure 8) connects the green waste line from port W (6) to a

3-mm (1/8-in) ID PTFE waste line. The waste line is routed through the

tubing chase to the IC system rear panel.

The needle seal line from the AS autosampler inject port to the IC

system injection valve is specially constructed. It consists of two

tubes (one inside the other) that are sealed at the end. This seal must

be maintained.

In addition, the line is calibrated for use with the IC system. To ensure

correct autosampler function, this line MUST NOT BE CUT! If

replacement is required, refer to the AS operator’s manual for the

required part number and replacement instructions.

Figure 7. Injection Valve

Figure 8. Injection Valve Waste Line Coupler

Autosampler

Needle Seal

Line

Waste

Line

Coupler

Green

Waste

Line

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