Agilent Technologies Infinity II SFC Binary 1260 Manual de usuario

Agilent Technologies

Agilent InfinityLab LC Series

1260 Infinity II SFC Binary

Pump

User Manual

1260 SFC Binary Pump

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G4782-90000

Edition

02/2017

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

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(June 1987) or any equivalent agency regu-

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lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1260 SFC Binary Pump 3

In This Guide...

This manual covers the Agilent InfinityLab LC Series 1260 Infinity II SFC

Binary Pump (G4782A).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information about site requirements and specifications

for the binary pump.

3 Using the Pump

This chapter explains the operational parameters of the Binary Pump.

4 Optimizing Performance

This chapter gives information on how to optimize the performance of the

Binary Pump under special operational conditions.

5 Troubleshooting and Diagnostics

Overview of the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Test Functions and Calibration

This chapter explains all test functions that are available for the binary pump.

8 Maintenance

This chapter describes the maintenance and repair of the module.

41260 SFC Binary Pump

In This Guide...

9 Parts and Materials for Maintenance

This chapter lists all parts and tools that are required for maintenance and

simple repairs.

10 Identifying Cables

This chapter provides information on cables used with the Agilent InfinityLab

LC Series modules.

11 Hardware Information

This chapter provides detailed technical information about your binary pump.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal and web.

1260 SFC Binary Pump 5

Contents

1 Introduction 9

Instrument and Operation 10

Overview of the Hydraulic Path 13

Leak and Waste Handling 17

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications 28

3 Using the Pump 31

Magnets 32

Turn on/off 33

Status Indicators 34

Best Practices 35

Leak and Waste Handling 37

Hints for Successful Use of the Binary Pump 39

Setting up the Pump with the G4208A Instant Pilot 40

Setting up the Pump with the Instrument Control Interface 41

Solvent Information 46

Algae Growth in HPLC Systems 52

Prevent Blocking of Solvent Filters 53

Normal Phase Applications 55

4 Optimizing Performance 57

When to Use a Vacuum Degasser 58

When to Use the Active Seal Wash Option 59

How to Optimize the Compressibility Compensation Setting 60

5 Troubleshooting and Diagnostics 63

Overview of the Module’s Indicators and Test Functions 64

Agilent Lab Advisor Software 65

61260 SFC Binary Pump

Contents

6 Error Information 67

What Are Error Messages 69

General Error Messages 70

Module Error Messages 77

7 Test Functions and Calibration 89

Pump Leak Rate Test 90

8 Maintenance 91

Introduction to Maintenance 92

Cautions and Warnings 93

Cleaning the Module 95

Overview of Maintenance and Simple Repairs 96

Maintenance Procedures 97

Remove and Install Doors 98

Exchange the Purge Valve Frit or the Purge Valve 100

Replace the O-Ring on the Purge Valve 102

Remove the Pump Head Assembly 105

Maintenance of a Pump Head without Seal Wash 107

Maintenance of a Pump Head with Seal Wash 110

Reinstall the Pump Head Assembly 114

Seal Wear-in Procedure Channel B 115

Exchange the Seal Wash Cartridge 116

Replace Leak Handling System Parts 118

Exchange the Inlet Valve 119

Exchange the Outlet Valve 120

Exchange the Solvent Selection Valve 122

Replacing Module Firmware 124

9 Parts and Materials for Maintenance 125

Hydraulic Path with Solvent Selection Valve 126

Pump Head Assembly Channel B 128

Pump Head Assembly Channel A 130

Outlet Valve 132

Purge Valve Assembly 133

HPLC System Tool Kit 134

Active Seal Wash Option 135

1260 SFC Binary Pump 7

Contents

Solvent Cabinet 136

Bottle Head Assembly 137

Cover Parts 138

Accessory Kit 139

10 Identifying Cables 141

Cable Overview 142

Analog Cables 144

Remote Cables 146

CAN/LAN Cables 150

RS-232 Cable Kit 151

Agilent 1200 Module to Printer 152

11 Hardware Information 153

Firmware Description 154

Electrical Connections 157

Interfaces 159

Setting the 6-bit Configuration Switch 166

Early Maintenance Feedback 170

Instrument Layout 171

12 LAN Configuration 173

What You Have to Do First 174

TCP/IP parameter configuration 175

Configuration Switches 176

Initialization Mode Selection 177

Dynamic Host Configuration Protocol (DHCP) 179

Manual Configuration 182

13 Appendix 187

General Safety Information 188

Waste Electrical and Electronic Equipment Directive 194

Radio Interference 195

Sound Emission 196

Agilent Technologies on the Internet 197

81260 SFC Binary Pump

Contents

1260 SFC Binary Pump

Agilent Technologies

Introduction

Instrument and Operation 10

Introduction to the Pump 10

Principle of Operation 11

Product Description 12

Features 12

Overview of the Hydraulic Path 13

Leak and Waste Handling 17

Waste Concept 21

This chapter gives an introduction to the module and an instrument overview.

10 1260 SFC Binary Pump

Introduction

Instrument and Operation

Introduction to the Pump

The binary pump comprises two identical pumps integrated into one housing.

Binary gradients are created by high-pressure mixing. A built-in degasser is

available for applications that require best flow stability, especially at low flow

rates, for maximum detector sensitivity. The pump is capable of delivering

flow in the range of 0.1 – 5 mL/min against up to 600 bar. A solvent selection

valve allows to form binary mixtures (isocratic or gradient). Active seal wash

is available for up to three modifier solvents on channel B, while channel A is

always the CO

delivering channel.

Figure 1 Overview of the pump

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