Agilent Technologies G1330B Manual de usuario

Agilent 1100 Series

Autosampler Thermostat

Reference Manual

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Germany

Copyright Agilent

Technologies 2001

Reproduction, adaption, or

translation without prior

written permission is

prohibited, except as allowed

under the copyright laws.

Part No. G1330-90002

Edition 08/01

Printed in Germany

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The information contained in

this document is subject to

change without notice.

Agilent Technologies makes

no warranty of any kind with

regard to this material,

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the implied warranties or

merchantability and fitness

for a particular purpose.

Agilent Technologies shall not

be liable for errors contained

herein or for incidental or

consequential damages in

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furnishing, performance, or

use of this material.

WARNING

Warning Symbols Used In

This Book

The apparatus is marked with

this symbol when the user

should refer to the instruction

manual in order to protect the

apparatus against damage.

Reference Manual

Agilent 1100 Series Autosampler Thermostat

In This Book

This manual contains information about the Agilent 1100 Series thermostatted autosamplers.

Information about the autosamplers can be found in the respective Reference Manuals. This

supplemental manual describes only the parts of the autosamplers that are different from the

standard versions. The manual describes the following:

• installing the thermostatted autosampler,

• theory of operation,

• troubleshooting the ALS thermostat,

• repair procedures for the ALS thermostat,

• parts and materials for autosampler and ALS thermostat.

Contents

Theory of Operation 9

Theory of operation of mechanical hardware, electronics,

and instrument interfaces 9

Introduction to the Thermostatted Autosampler 10

ALS Thermostat Operation 12

ALS Thermostat Control and Electronics 14

Temperature Controlled Autosampler Board (TCA) 15

Electrical Connections 17

Installing the G1330B Thermostat 19

Site requirements and installation of the G1330B

thermostat 19

Site Requirements 20

Power Consideration 20

Power Cords 20

Bench Space 21

Environment 21

Unpacking the Autosampler 23

Damaged Packaging 23

Delivery Checklist 24

Optimizing the Stack Configuration 25

Controller Requirements 27

Control Module Firmware requirements 27

Agilent ChemStation Software requirements 27

Installing the G1330B Thermostat 28

Stage 1: Preparing the ALS Thermostat and Autosampler 28

Stage 2: Power Cable and Interface Cable Connection 31

Contents

Stage 3: Flow Connections 33

Stage 4: Installing the Sample Tray 34

Stage 5: Installing Tray Cover and Front Cover 36

Stage 6: Turning on the Thermostatted Autosampler 37

Stage 7: Update of Control Module Firmware 37

Stage 8: Update of the Agilent ChemStation Software 38

Transporting the Thermostatted Autosampler 40

Troubleshooting and Test Functions 41

The thermostatted autosampler‘s built-in troubleshooting

and test functions 41

Status Indicators 42

Error Messages 42

Status Indicators 43

Power Supply Indicator 44

Instrument Status Indicator 45

ALS Thermostat Error Messages 46

Fan Failed 47

Temperature Control Failed (1 - 4) 48

Temperature Sensor Failed (1 - 4) 49

Lost Contact to ALS Thermostat 50

Power Fail for ALS Thermostat Module 51

Temperature out of Range 52

Bad Cooling / Heating Performance 53

Contents

Repairing the ALS Thermostat Module 55

Instructions on repair procedures of the ALS thermostat 55

Simple Repairs 56

Exchanging Internal Parts 56

Cleaning the Thermostat 57

Using the ESD Strap 58

Overview 59

Exchanging the Power Supply Fuses 60

Removing the Top Cover and Foam 61

Exchanging Heat Exchanger Fan 63

Exchanging the Heatsink Fans 65

Exchanging the Sensors 67

Exchanging the TCA board 70

Assembling the Main Cover 73

ALS Thermostat Parts and Materials 75

Lists for identification of parts and materials 75

Main Assemblies 76

Accessory Kit G1330-68705 77

Main Assemblies 78

Foam Parts 79

Plastic Parts 80

Heat Exchanger Fan Parts 81

Contents

Specifications 83

Performance specifications of the ALS thermostat 83

Performance Specifications 84

Safety Information 90

Radio Interference 93

Sound Emission 93

Agilent Technologies on Internet 94

1Theory of Operation

Theory of operation of mechanical hardware,

electronics, and instrument interfaces

Theory of Operation

Introduction to the Thermostatted Autosampler

Introduction to the Thermostatted

Autosampler

The Agilent 1100 Series thermostatted autosampler is designed for use with

other modules of the Agilent 1100 Series LC system, with the HP 1050 Series,

or with other LC systems if adequate remote control inputs and outputs are

available. The thermostatted autosampler is controlled from the Agilent 1100

Series control module or from the Agilent ChemStation for LC systems.

The specially-designed thermostattable sample trays holds either

100 × 1.8 ml vials or two wellplates and 10 × 1.8 ml vials.

The ALS thermostat contains Peltier-controlled heat exchangers. A fan draws

air from the area above the sample vial tray of the autosampler and is then

blown through the fins of the cooling/heating module. There it is cooled or

heated according to the temperature setting. The thermostatted air enters the

autosampler through a recess underneath the specially-designed sample tray.

The air is then distributed evenly through the sample tray ensuring effective

temperature control, regardless of how many vials are in the tray.

In cooling mode condensation is generated on the cooled side of the Peltier

elements. This condensed water is safely guided into the leak system.

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