Agilent Technologies 1260 Infinity Manual de usuario
Agilent Technologies
Agilent 1260 Infinity
Thermostatted Column
Compartment
User Manual
Agilent 1260 Infinity TCC User Manual
Notices
© Agilent Technologies, Inc. 2010-2012,
2013
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Manual Part Number
G1316-90014
Edition
05/2013
Printed in Germany
Agilent Technologies
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This product may be used as a com-
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Otherwise, it is intended only for gen-
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Agilent 1260 Infinity TCC User Manual 3
In This Guide…
In This Guide…
This manual covers the Agilent 1260 Infinity Thermostatted Column
Compartments (G1316A TCC).
1 Introduction to the Column Compartment
This chapter gives an introduction to the TCC, instrument overview and
internal connectors.
2 Site Requirements and Specifications
This chapter provides information about site requirements and
specifications for the module.
3 Installing the Column Compartment
This chapter describes the installation of the thermostatted column
compartment.
4 Using the Module
This chapter explains the operational parameters of the module.
5 How to optimize the Column Compartment
This chapter provides information on how to optimize the thermostatted
column compartement.
6 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.
7 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.
4 Agilent 1260 Infinity TCC User Manual
In This Guide…
8TestFunctions
This chapter describes the TCC’s built in test functions.
9 Maintenance
This chapter describes the maintenance and repair of the TCC.
10 Parts for Maintenance
This chapter provides information on parts for maintenance.
11 Identifying Cables
This chapter provides information on cables used with the 1260 Infinity
series of HPLC modules.
12 Hardware Information
This chapter describes the detector in more detail on hardware and
electronics.
13 Appendix
This chapter provides addition information on safety, legal and web.
Agilent 1260 Infinity TCC User Manual 5
Contents
Contents
1 Introduction to the Column Compartment 9
Introduction 10
System Overview 13
Column-Identification System 16
Column Switching Valve (Optional) 18
2 Site Requirements and Specifications 21
Site Requirements 22
Physical Specifications 25
Performance Specifications 26
3 Installing the Column Compartment 27
Unpacking the Column Compartment 28
Optimizing the Stack Configuration 29
Installation Information on Leak and Waste Handling 34
Installing the Column Compartment 38
Flow Connections of the Column Compartment 41
Placing Columns 45
4 Using the Module 47
Leak and Waste Handling 48
Solvent Information 49
5 How to optimize the Column Compartment 51
Optimizing the Performance of your Column Compartment 52
6 Troubleshooting and Diagnostics 53
Overview of the Module’s Indicators and Test Functions 54
Status Indicators 56
Available Tests depending on User Interfaces 58
Agilent Lab Advisor Software 59
6 Agilent 1260 Infinity TCC User Manual
Contents
7 Error Information 61
What Are Error Messages 62
General Error Messages 63
TCC Error Messages 69
8TestFunctions 77
Thermostat Function Test 78
Pressure Test 81
Column Thermostat Temperature Calibration 82
9 Maintenance 91
Warnings and Cautions 92
Introduction to Maintenance 94
Overview of Maintenance 95
Cleaning the Module 96
Changing Column Identification Tags 97
Replacing Head Parts of Column Switching Valve 99
Correcting Leaks 102
Replacing the Module’s Firmware 103
10 Parts for Maintenance 105
Column Switching Valve 2 Position/6 Port 106
Kits 107
Plastic Parts 108
Leak Parts 109
11 Identifying Cables 111
Cable Overview 112
Analog Cables 114
Remote Cables 116
BCD Cables 119
CAN/LAN Cables 121
External Contact Cable 122
Agilent Module to PC 123
Agilent 1200 Module to Printer 124
Agilent 1260 Infinity TCC User Manual 7
Contents
12 Hardware Information 125
Firmware Description 126
Electrical Connections 129
Interfaces 131
Setting the 8-bit Configuration Switch (without On-Board LAN) 138
Instrument Layout 142
13 Appendix 143
General Safety Information 144
The Waste Electrical and Electronic Equipment (WEEE) Directive
(2002/96/EC) 147
Lithium Batteries Information 148
Radio Interference 149
Sound Emission 150
Use of Solvents 151
Agilent Technologies on Internet 152
8 Agilent 1260 Infinity TCC User Manual
Contents
9
Agilent 1260 Infinity TCC User Manual
Agilent Technologies
1
Introduction to the Column
Compartment
Introduction 10
System Overview 13
Leak and Waste Handling 13
Column-Identification System 16
Column Switching Valve (Optional) 18
This chapter gives an introduction to the TCC, instrument overview and internal
connectors.
10 Agilent 1260 Infinity TCC User Manual
1Introduction to the Column Compartment
Introduction
Introduction
Main Features
The Agilent 1260 Infinity Thermostatted Column Compartment is a
stackable temperature- controlled column compartment for LC. It is used
for heating and cooling to meet extreme requirements of retention time
reproducibility.
The main features are:
•Peltier heating and cooling from 10 degrees below ambient up to 80 °C
with high heating and cooling speeds for maximum application
flexibility and stability.
•Holds up to three 30 cm columns and optimized design gives minimum
dead volumes and maximum efficiency.
•Two independently programmable heat exchangers contribute volumes
of only 3 µL and 6 µL.
•Electronic column- identification module as standard for GLP
documentation of column type and major column parameters.
•Optional high- quality Rheodyne®column switching valve with ceramic
stator- face assemblies for prolonged lifetime.
For specifications, see “Performance Specifications” on page 26.
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