Varian ProStar 701 Nota de publicación

Varian, Inc.

2700 Mitchell Drive

Walnut Creek, CA 94598-1675/USA

©Varian, Inc. 2005 03-914947-27:Rev.2

ProStar 701 Fraction

Collector Control

Galaxie Driver Manual

ProStar 701 Fraction Collector Control Manual - 1 - 03-914947-27:2

Table of Contents

Introduction.............................................................................................. 2

General................................................................................................................................2

Installation and Configuration................................................................ 3

Installing the Driver Software...............................................................................................3

Configuring the Communication Server...............................................................................3

Configuring the Driver..........................................................................................................4

Configuring the Varian ProStar 701 Fraction Collector.................................................4

Configuring the Synopsis..............................................................................................5

Building a Method ................................................................................... 7

Creating a New Method.......................................................................................................7

Control Method Section for the Varian ProStar 701 Fraction Collector.............................10

Collector Parameters Control......................................................................................12

Fraction Collector Mode Control.................................................................................14

Rack Control ...............................................................................................................17

Collection Chain Control .............................................................................................19

Starting and Viewing an Acquisition.................................................... 21

Quick Start and Sequence.................................................................................................21

Quick Start (Single Acquisition) ..................................................................................21

Sequence....................................................................................................................23

Running Acquisition Status................................................................................................24

Viewing a Running Acquisition....................................................................................24

Status of the Varian ProStar 701 Fraction Collector...................................................24

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Introduction

General

This document describes the configuration of the Varian

ProStar 701 Fraction Collector driver. It also explains how to

build a control method for this driver, how to start and view a

running acquisition and what actions are available during an

analysis.

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Installation and

Configuration

Installing the Driver Software

To install the Galaxie Drivers software refer to the Galaxie Data

System Installation Guide.

Configuring the Communication Server

To communicate with the ProStar 701 module an

RS232_Interface or an RS232_PC communication bus must be

configured on the acquisition server.

The parameters of the bus to must be the following:

Stops 1 Stop

Baud 19200 Parity EVEN

Bits 8 Bits Flow Control NONE

Buffer Tx 4096 Buffer Rx 4096

NOTE: For more details about the configuration of an RS232_Interface or an RS232_PC

bus, refer to the Galaxie Chromatography Data System Installation’s Guide.

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Configuring the Driver

The driver software configuration is done in the Galaxie

Configuration Manager when a new chromatographic system is

created.

Configuring the Varian ProStar 701 Fraction Collector

Click on the button corresponding to the Varian ProStar

701 Fraction Collector driver and the configuration screen

appears.

Communication Window

Select from the Hardware Interface list the name of the RS232

Bus where the system has been connected.

NOTE: For more details about the RS232 Bus configuration, refer to the

Configuring the Communication Server section in this manual.

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Define the number of ProStar 701 Fraction Collector installed in

the Number of instrument spin edit. Up to four ProStar 701

Fraction Collectors can be defined.

For each fraction collector, define the address in the Fraction

Collector X ID field. Then press the

button, to connect to the instrument.

Configuring the Synopsis

In the Overview part of the system configuration, a synopsis can

be defined for the system. This synopsis depends on the

configured devices.

1. To save the configuration of these devices, click on the OK

button.

2. Right click on the system name in the bottom part of the

Galaxie Configuration Manager screen. A pop-up menu

appears: click on Stop. Then right click on the system name

again, and click on Start.

3. Go back to the System Configuration screen (Properties

wizard). A graphic of the devices that comprise the system

is displayed in the synopsis screen. To configure the

synopsis as the real instrument configuration, move each

module, and then connect it appropriately. To do this, select

one anchor for each of the two modules (the selected

anchors become red) and click on the button; a

connection tube will appear between the two anchors.

Click on the to delete a selected tube, click on the

button to delete all the tubes.

Click on to define a background color, or on to

make the background transparent.

Click on the icon to change the grid color.

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4. Once the synopsis configuration is complete, it will be

displayed in the Galaxie Chromatography Data System, in

the Systems tab. In this tab, the Overview part will show the

synopsis of the system with some parameters displayed

(temperature, flow, signal, etc.) depending on the installed

devices.

For example, the following pictures represent the synopsis

of the Varian ProStar 701 Fraction Collector:

Galaxie Configuration Manager Screen

Galaxie Chromatography Data System Screen

NOTE: Once the system has been created and correctly configured, it must be

associated with one or more projects in order to start some acquisitions. For

more details about the creation and configuration of a system, refer to the

Galaxie Configuration Manager User’s Guide.

Click on the button to print the current configuration.

ProStar 701 Fraction Collector Control Manual - 7 - 03-914947-27:2

Building a Method

Creating a New Method

The method contains parameters for instrument control, data

acquisition, chromatogram processing, and editing of final

results. To initially set up a method, it is not necessary to define

all of the sub-method sections; however, you must fill in the

instrument control section prior to starting an acquisition.

1. To create a new method, select the FILE / NEW METHOD

option from the Galaxie Chromatography Data System main

menu.

A wizard guide will appear and provide assistance during

the first steps of method creation:

ProStar 701 Fraction Collector Control Manual - 8 - 03-914947-27:2

2. Choose the system (chromatograph) associated with the

method. A method is created for a particular system. When

starting an acquisition, the name of the system that

performs the acquisition must be correct, since method

access is limited only to those methods associated with this

system.

3. Once this field is completed, click on the Next button to

move to the second step of the method creation:

ProStar 701 Fraction Collector Control Manual - 9 - 03-914947-27:2

4. Enter the New Method Name in the first field. In the

Description field, enter information concerning the method

(optional).

5. Once these two fields have been completed, click on the

OK button. The new method is created and is opened with

default parameters in the Galaxie Chromatography Data

System. The next step is the definition of each of the

method sections.

The instrument control section must be defined in order to

start an acquisition. In the following part of this guide, only

the control section for the Varian ProStar 701 Fraction

Collector is detailed. Other parameters such as Injection

Volume, Vial and Rack number may be necessary and are

defined in the acquisition section.

NOTE: For more details about the programming of each method section, turn to the

Galaxie Chromatography Data System User’s Guide.

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