Specac Quest Manual de usuario

2I-10800-10

The Quest

Single Reflection ATR Accessory

User Manual

2I-10800-10 2

List of Safety Symbols

Safety Symbol

Meaning

Caution! indicates Important information which

needs to be followed for the safe operation of

this accessory.

Caution! –Hot Surface where used indicates

the product contains heated surfaces which

need to be taken into consideration while

handling and operating this device

Caution –Possibility of Electric Shock

Indoor Use Only

2I-10800-10 3

Quest Heated Puck

User Manual

 
2I-10800-10 4 
The Quest Single Reflection ATR Accessory 
P/N GS10800 
CONTENTS 
INTRODUCTION..............................................................................5 
SAFETY ........................................................................................6 
CHECKLIST OF CONTENTS .............................................................7 
“BUBBLE NUMBERS”PART IDENTIFICATION LIST..............................8 
INSTALLATION ...............................................................................9 
1. Mounting the Quest into the Spectrometer sample 
compartment...................................................................................9 
2. Quest Puck Assembly........................................................10 
ALIGNMENT PROCEDURE FOR QUEST ATR...................................12 
1. Front Cover Removal.........................................................12 
2. Synopti-Focal Mirror System .............................................13 
3. Alignment Procedure .........................................................14 
4. Procedure to Follow from Any Accidental Mis-Alignment..16 
PURGING THE QUEST ATR OPTICAL UNIT ....................................18 
QUEST ATR CLAMP ARM AND ANVILS ..........................................20 
1. Clamp Arm Assembly ........................................................20 
2. Choice of Anvils .................................................................21 
SAMPLING USING THE QUEST ATR ACCESSORY...........................22 
1. Background Acquisition .....................................................22 
2. Solid Sampling Procedure .................................................22 
3. Liquid Sampling procedure ................................................23 
4. Cleaning Tips.....................................................................24 
QUEST SAMPLING ACCESSORIES..............................................26 
1. The Volatiles Cover........................................................26 
2. Luer Lock Liquids Anvil ..................................................27 
3. The Specular Reflectance Puck.....................................27 
QUEST ATR PART NUMBERS AND SPARES ...............................29 
QUEST ATR TECHNICAL SPECIFICATIONS .................................31 
QUEST ATR SERIAL NUMBERS.................................................32 
 
© 2021 Specac Ltd. All rights reserved. 
Benchmark and Brillian Spectroscopy are trademarks of Specac 
Ltd. Other product names mentioned herein may be trademarks 
of their respective owners. 

2I-10800-10 5

1. Introduction

Thank you for buying a Specac product. We trust it will provide you with

invaluable and excellent service in use.

The Quest Single Reflection ATR Accessory is designed for the

quantitative and qualitative analysis of solids, powders, liquids, pastes

and gum-like samples using mid-IR spectroscopy at a nominal 45°

incident angle under ambient or elevated temperature conditions.

The Quest is based upon Synopti-Focal technology –an innovative

synoptic focusing array of highly reflective gold coated mirror only optics

–in an optical unit fitted with interchangeable ATR puck assemblies

(choice of diamond, ZnSe, Ge or Si). The ATR crystal is mounted in

either a Standard (flat), Liquid or Heated Puck Assembly. For solid

samples, where good contact with the ATR crystal is required, a clamp

arm produces a highly reproducible load of 40 lbs.

The use of mirror optics maximizes the spectral range as follows:

ATR Crystal

Notes

Range (cm-1)

Diamond

AR Coated

7800 - 400

Non-AR Extended Range

10000 - 10

ZnSe

AR Coated

7800 - 500

Non-AR heated puck

7800 - 500

AR coated

5500 - 500

Non-AR coated

8333-1350 and

500-33

Arrow (Si wafer)

Thin Wafer

8333-33

Specular Reflectance measurements are also possible by the use of a

specular reflectance puck at a nominal 45 ° angle.

2I-10800-10 6

2. Safety

Caution! Always use personal protective equipment (PPE)

when operating this device and follow local safety operating

procedures and practices with respect to potential toxic and

flammable sample substances.

Make sure that all samples intended to be used with the ATR are

chemically compatible with the accessory surfaces, including:

•The ATR crystal material (diamond, ZnSe, Ge, or Si)

•The indium sealing material around the crystal.

•Stainless-steel used in the puck and anvil components.

•Anodized aluminum & Viton O-ring in the volatiles cover.

•For Arrow only: polypropylene slide, thermoelastic seal (SBS-

SEBS), anodized aluminum puck.

Safety data sheets (SDS) are available in the product support section of

the Specac web site where required and are provided with each crystal

type. As an alternative please contact your Specac representative for

further details.

It is recommended to wear suitable gloves and eye protection PPE at all

times when using this device.

Important! This manual should be read in conjunction with

the Arrow QS user manual where applicable.

Important! This manual should be read in conjunction with

the manual for the heated puck and USB temperature

controller where applicable.

2I-10800-10 7

3. Checklist of Contents

The Quest ATR Accessory is provided in its own specific packaging.

The items that require checking upon delivery depend on which Quest

ATR system has been ordered.

Please check for the following standard items:

1 x Quest ATR Accessory including optical unit

1 x Flat anvil P/N GS10820

1 x Pellet anvil P/N GS10821

1 x Pair of purge bellows P/N GS10707

1 x Volatiles cover P/N GS10825

1 x Ball driver 3.0 mm (for optical unit cover plate removal)

1 x Ball driver 2.5 mm (for mirror adjustment in optical unit)

1 x Benchmark™ baseplate for your FTIR spectrometer

1 x USB manual

Along with any Puck assemblies included with your order, which may

include:

ATR Flat puck (choice of diamond, ZnSe, Ge or Si)

ATR Liquid puck (choice of diamond, ZnSe, Ge or Si)

Arrow Puck and 100 Slides

Heated puck (choice of diamond or Znse)

(consult relevant manuals for checklist of parts)

Specular Reflectance Puck

Carefully remove your Quest ATR Accessory and ATR puck

assembly(s) from the packaging in readiness for use.

 
2I-10800-10 8 
4. “Bubble Numbers” Part Identification 
List 
 
 
1) Optical unit thumb screw. (Figure 5-1). 
2) Location slot of ATR puck assemblies (Figure 5-3). 
3) Location pin on top surface of the optical unit (Figure 5-4). 
4) Magnetic catch for ATR puck assemblies (Figure 5-4). 
5) Front cover plate of optical unit (Figure 6-1). 
6) Captive screw of front cover plate (Figure 6-1). 
7) Grub screw for M6 mirror rotation (Figure 6-3). 
8) Cap head screw for M6 mirror tilt (Figure 6-3). 
9) Grub screw for M3 mirror rotation (Figure 6-3). 
10) Cap head screw for M3 mirror tilt (Figure 6-3). 
11) Grub screw for M1 mirror rotation (Figure 6-3). 
12) Cap head screw for M1 mirror tilt (Figure 6-3). 
13) Aperture port on optical unit (Figure 7-1). 
14) Purge tube location port in front cover plate (Figure 7-1). 
15) Curved grip plate for purge tubing in front cover plate (Figure 7-2). 
16) Purge bellow (Figure 7-3). 
17) Flat or Pellet Anvil (igure 8-3). 
18) Clamp arm assembly (igure 8-3). 
19) Anvil storage port (igure 8-3). 
20) Torque screw knob (igure 8-3). 
21) Volatiles cover (Figure 10-1). 
22) Luer Lock Liquids anvil (Figure 10-3). 
23) Specular reflectance puck (Figure 10-4). 
24) Reference mirror for specular reflectance puck (Figure 10-4). 

2I-10800-10 9

5. Installation

5.1. Mounting the Quest into the Spectrometer sample

compartment

Figure 5-1: Quest ATR Accessory –Optical Unit and ATR Puck Assembly

The Quest ATR Accessory is supported on a Benchmark™ baseplate

when installed into a spectrometer. A Benchmark™ baseplate has three

pillars across the front for location/fixing and a fourth to the rear for

support only. The thumb screw (1) at the front of the Quest ATR optical

unit screws into the front central pillar, while the outer studded pair locate

in slots beneath the Quest unit.”

Note: Install the Benchmark™ baseplate in the spectrometer first

before locating the Quest ATR Accessory.

Fixing holes and studs in the Benchmark™ baseplate will vary

depending upon the make and model of the spectrometer. Refer to the

Benchmark™ baseplate Installation Guide/User Manual.

2I-10800-10 10

5.2. Quest Puck Assembly

5.2.1. Quest ATR Puck Assemblies Identification

Top and underside views of the Quest ATR Flat and Liquid puck

assemblies are shown in Figure 5-2 and Figure 5-3.

Figure 5-2: Top view of Quest ATR Diamond Crystal puck: Standard (left) and

Liquids (right) Puck Assembly

Figure 5-3: Underside view of Quest ATR Diamond Crystal

Puck Assembly

ATR Crystal

ATR

Crystal

Serial Number

Label

Crystal Puck

Identification

Label

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