Peak Scientific Precision Series Manual de usuario

Precision Nitrogen User Manual Rev 4 RSID 226 EN 21/12/17

Precision Nitrogen (All Models)

User Manual

Contents

Change History 3

How to use this Manual 3

Introduction 4

Warranties and Liabilities 5

Safety Notices 6

Symbols 6

Safety Notice to Users 6

Declaration of Conformity 7

Environmental Declaration 8

Technical Speciﬁcation 9

Unpacking 11

Fittings Kit Contents 12

Unpacking Instructions 12

Installation 13

Generator Environment 13

Generator Overview 14

Nitrogen General Dimensions 14

Nitrogen Trace General Dimensions 15

Nitrogen Rear Connections 16

Nitrogen Trace Rear Connections 17

Electrical Connection 18

Air Purity 19

Class 1 Particulate 19

Class 4 Water 19

Class 1 Oil 19

Start-Up Sequence 20

On Demand Gas 20

Unusual Operation 20

Connecting to the application 21

Tubing Lengths 21

Service Requirements 22

Service Schedule 22

Peak Protected 23

Cleaning 24

Troubleshooting 25

Page 2

Page 3

Change History

Rev Comment Name Date

1 Release Liam Couttie 14/12/2016

2 Technical Speciﬁcation Update Liam Couttie 08/02/2016

3 Nitrogen Headspace Added Liam Couttie 06/09/2016

4 Product Overview Correction Liam Couttie 21/12/2017

How to use this Manual

This manual is intended for end users and has been written as a reference document

where you can skip to the relevant information.

Users can refer to the contents page to ﬁnd the relevant information.

Please review each of the following sections carefully.

Thank you for selecting Peak Scientiﬁc to meet your gas generation needs, and should

you require any further assistance or support please do not hesitate to contact Peak

Scientiﬁc or the Peak Partner from which you purchased your generator.

Page 4

Introduction

Precision is a modular system with differing ﬂow rates that allows you to add multiple

generators as your gas and analysis demands change. The Precision Series will keep

your gas ﬂowing with consummate accuracy and reliability, whatever your needs, while

ﬁtting neatly into any lab space.

The Precision Nitrogen, Headspace and Nitrogen Trace Generators provide a constant

and consistent source of Nitrogen for detector make-up gas for GC applications, as

well as headspace vial pressurization, purge and trap, tube conditioning for thermal

desorption and sample blow down. In addition to these applications, the Precision

Nitrogen Trace model can be used for carrier gas in GC applications as it also removes

hydrocarbons by means of catalytic oxidation.

Other features include:

• Generates Nitrogen on demand from compressed air.

• Regenerative PSA Carbon Molecular Sieve to ensure Oxygen and Moisture removal.

• Minimum maintenance with only a ﬁlter change per annum.

• Small and Stackable.

With the Precision Nitrogen based on proven technology, it removes moisture and

oxygen to leave Ultra High Purity Nitrogen. The Nitrogen Trace further removes

Hydrocarbons (as Methane) to <0.05ppm.

To ensure these generator models meet our high expectations with regards to reliability

and performance, we have tested them extensively at our manufacturing plant and with

end users around the world to ensure reliability and longevity of the system.

Page 5

Warranties and Liabilities

1. The Company warrants that it has title to the Goods.

2. Subject to the provisions of this clause the Company warrants that the Goods

shall comply in all material respects with any speciﬁcation referred to in the Order

Conﬁrmation (as the same may be amended) and shall, subject thereto, be free

from defects in material and workmanship for the lesser of a period of twelve

months from the date of delivery or thirteen months from the date of dispatch

from the factory.

3. Save as provided in this clause and except where the Goods are sold to a person

dealing as a consumer (within the meaning of the Unfair Contract Terms Act

1977) all warranties, conditions or other terms implied by statute or common

law are hereby expressly excluded save to the extent they may not be lawfully

excluded. When the Goods are sold to a consumer within the meaning of the Unfair

Contract Terms Act 1977 their statutory rights are not affected by the provisions of

this clause.

4. In the event of the Customer making a claim in respect of any defect in terms of

clause 2 hereof the Customer must.

1. Reasonably satisfy the Company that the Goods have been properly installed,

commissioned, stored, serviced and used and without prejudice to the generality

of the foregoing that any defect is not the direct or indirect result of lack of repair

and/or servicing, incorrect repair and/or servicing, use of wrong materials and/or

incorrect spare parts

2. Allow the company to inspect the Goods and/or any installation and any relevant

packaging as and when reasonably required by the Company.

5. Subject to the Company being notiﬁed of any defect as is referred to in sub-

clause 2 hereof within a reasonable time of it becoming apparent and subject always

to the terms of sub-clause 4 hereof, the Company shall, in its option, replace or

repair the defective Goods or refund a proportionate part of the Price. The Company

shall have no further liability to the Customer (save as mentioned in sub-clause 6

hereof).

6. The Company shall be liable to indemnify the Customer in respect of any claim

for death or personal injury to any person in so far as such is attributable to the

negligence or breach of duty of the Company or any failure by the Company to

comply with the provisions of sub-clause 2 hereof.

7. Save as provided in sub-clause 2 hereof the Company shall not be liable in respect

of any claim by the Customer for costs, damages, loss or expenses (whether direct,

indirect, consequential or otherwise) or indemnity in any respect howsoever arising

including, but not by way of limitation, liability arising in negligence (other than

pursuant to clause 6 above) that may be suffered by the Customer or any third

party.

Page 6

Safety Notices

Peak Scientiﬁc Instruments cannot anticipate every possible circumstance which may

represent a potential hazard. The warnings detailed within this manual refer to the most

likely potential hazards, but by deﬁnition cannot be all inclusive. If the user employs

an operating procedure, item of equipment or a method of working which is not

speciﬁcally recommended by Peak Scientiﬁc, the user must ensure that the equipment

will not be damaged or become hazardous to persons or property.

Symbols

This manual uses the following symbols to highlight speciﬁc areas important to the safe

and proper use of the generator.

A WARNING notice denotes a hazard. It calls attention to an operating procedure,

process or similar, which if not correctly performed or adhered to, could cause

personal injury or in the worst case death. Do not proceed beyond a WARNING

notice until the indicated conditions are fully understood or met.

A CAUTION notice denotes a hazard. It calls attention to an operating procedure,

process or similar, which if not correctly performed or adhered to, could cause

damage to the generator or the application. Do not proceed beyond a CAUTION

notice until the indicated conditions are fully understood or met.

Caution, risk of electric shock. Ensure power to the generator has been removed

before proceeding.

Safety Notice to Users

These instructions must be read thoroughly and understood before

installation and operation of your Peak Generator. Use of the generator

in a manner not speciﬁed by Peak Scientiﬁc MAY impair the SAFETY

provided by the equipment.

When handling, operating or carrying out any maintenance, personnel

must employ safe engineering practices and observe all relevant local

health and safety requirements and regulations. The attention of UK

users is drawn to the Health and Safety at Work Act 1974, and the

Institute of Electrical Engineers regulations.

If the equipment is used in a manner not speciﬁed by the manufacturer,

the protection provided by the equipment maybe impaired.

Page 7

Declaration of Conformity

We Peak Scientiﬁc Instruments Ltd.

Of Fountain Crescent, Inchinnan, Renfrewshire, PA4 9RE

Declare that:

Equipment: Nitrogen Generator

Models: Precision Nitrogen 250cc, 600cc, 1000cc, Headspace

Precision Nitrogen Trace 250cc, 600cc, 1000cc

To which this declaration relates, is in conformity with the applicable EC directives,

harmonized standards, and other normative requirements.

• Low Voltage Directive 2006/95/EC

EN 61010-1: 2010 Electrical Equipment for measurement, control and laboratory use.

• Electromagnetic Compatibility Directive 2004/108/EC

EN 61326-1: 2013 Electrical Equipment for measurement, control and laboratory use.

• FCC47 CFR Part 15 Class B

Unintentional radiators; Conducted and Radiated emissions limits.

All evaluation, testing and certiﬁcation issued by:

Nemko Canada Inc.

303 River Road, Ottawa

Ontario, Canada

K1V 1H2

Signed: Name: Chris Pugh

Date: 26/10/2015 Position: Engineering & Operations Director

Page 8

Environmental Declaration

We Peak Scientiﬁc Instruments Ltd.

Of Fountain Crescent, Inchinnan, Renfrewshire, PA4 9RE

Declare that:

Equipment: Nitrogen Generator

Models: Precision Nitrogen 250cc, 600cc, 1000cc, Headspace

Precision Nitrogen Trace 250cc, 600cc, 1000cc

Is fully compliant with the following Directives

• 2012/19/EU WEEE (Waste of Electrical and Electronic Equipment)

• 2011/65/EU RoHS 2 (Restriction of Hazardous Substance)

Peak Scientiﬁc Instruments Ltd fully complies with its obligations towards the European

WEEE (Waste of Electrical and Electronic Equipment) Directive 2012/19/EU. These

obligations are being met within the B2B compliance group.

Peak Scientiﬁc Instruments Ltd has developed all reasonable ‘due diligence’ controls to

ensure that our products comply with the principles and requirements of the European

recast RoHS (Restriction of Hazardous Substances) Directive 2011/65/EU. Similar

directives in the United States and China, for example, have also been captured within

this program.

Where a speciﬁc certiﬁcate of compliance is required, this can be requested, on

a product serial number basis, directly from Peak Scientiﬁc Instruments Ltd, by

contacting us through our website on www.peakscientiﬁc.com

Signed: Name: Chris Pugh

Date: 10/06/2015 Position: Engineering & Operations Director

Page 9

Technical Speciﬁcation

Precision Nitrogen

Environment

250cc 600cc 1000cc

Minimum Operating Ambient Temperature 5°C (41°F)

Maximum Operating Ambient Temperature 35°C (95°F)

Maximum Altitude 2000 m

Maximum Relative Humidity 70% Non-Condensing

Minimum Storage Temperature* -20°C (-4°F)

Maximum Storage Temperature* 60°C (140°F)

Inlet Conditions

Inlet Air Pressure Min-Max 6.9-8.3 bar (100-120 psi)

Minimum Air Inlet Flow 35 l/min

Minimum Air Inlet Quality ISO 8573-1:2010 Class[1.4.1]

Particles <0.01µm

Generator Outlets

Maximum Gas Output Pressure 5.5 bar (80 psi)

Maximum Outlet Flow Rate 250cc 600cc 1000cc

Start-up time 1.5 Hours

Particles <0.01µm

Phthalates NONE

Suspended Liquids NONE

Gas Outlets 1 x ¼” BSPP

For optimum performance from your Precision Nitrogen generator, the inlet gas supply pressure should be

30PSI greater than the required output pressure.

Electrical Requirements

Voltage 100-240v

Frequency 50/60 Hz

Current 0.4-0.2A

Input Connection C14 Plug

Power Cord (Supplied) C13 Socket to Local Connection

Pollution Degree 2

Insulation Category II

General

Dimensions cm (inches) WxDxH 38.0 (14.9) x 54.0 (21.2) x 25.6 (10.0)

Generator Weight Kg (lbs) 21 (46.2) 26 (57.3)

Shipping Weight Kg (lbs) 24 (53) 29 (64)

Page 10

Technical Speciﬁcation

Precision Nitrogen Headspace

Environment

Minimum Operating Ambient Temperature 5°C (41°F)

Maximum Operating Ambient Temperature 35°C (95°F)

Maximum Altitude 2000 m

Maximum Relative Humidity 70% Non-Condensing

Minimum Storage Temperature* -20°C (-4°F)

Maximum Storage Temperature* 60°C (140°F)

Inlet Conditions

Inlet Air Pressure Min-Max 8.3-8.6 bar (120-125 psi)

Minimum Air Inlet Flow 18 l/min

Minimum Air Inlet Quality ISO 8573-1:2010 Class[1.4.1]

Particles <0.01µm

Generator Outlets

Maximum Gas Output Pressure 6.9 bar (100 psi)

Maximum Outlet Flow Rate 250cc

Start-up time 3 - 3.5 Hours

Particles <0.01µm

Phthalates NONE

Suspended Liquids NONE

Gas Outlets 1 x ¼” BSPP

For optimum performance from your Precision Nitrogen generator, the inlet gas supply pressure should be 30PSI greater than the

required output pressure.

Though the Precision Headspace Generator delivers nitrogen at a purity suitable for most non- trace applications, we would

recommend the installation of oxygen and hydrocarbon traps for analysis at lower detection limits (<1000ppm).

Electrical Requirements

Voltage 110-230v ±10%

Frequency 50/60 Hz

Current 0.37 -0.17 A

Input Connection C14 Plug

Power Cord (Supplied) C13 Socket to Local Connection

Pollution Degree 2

Insulation Category II

General

Dimensions cm (inches) WxDxH 38.0 (14.9) x 54.0 (21.2) x 25.6 (10.0)

Generator Weight Kg (lbs) 21 (46.2)

Shipping Weight Kg (lbs) 24 (53)

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