Malvern MicroCal iTC200 Manual de usuario

User Guide

MicroCal iTC200 Washing Module

2MicroCal iTC 200Washing Module User Guide

MicroCal iTC200 Washing Module MAN0582

MicroCal iTC 2003

Table of Contents

Installation Kit Contents ............................................................................................................................................................ 2

Part 1: Bottle Preparation ........................................................................................................................................................ 7

Part 2: Fluid Connections ......................................................................................................................................................... 8

Part 3: Hardware Connections ............................................................................................................................................. 15

Part 4: Electrical Connections and Grounding ............................................................................................................. 17

Part 5: Washing Module Basic Operation ....................................................................................................................... 19

Part 6: Washing Module Maintenance .............................................................................................................................. 23

Part 7: Washing Module Troubleshooting ....................................................................................................................... 27

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4 MicroCal iTC 200Washing Module User Guide

Important user information

Intended use

MicroCal iTC 200is an isothermal titration calorimeter designed for biomolecular interaction studies

in research applications.

MicroCal iTC 200Washing module is intended for research use only, and shall not be used in any

clinical procedures, or for diagnostic purposes.

Prerequisites

In order to operate the system in the way it is intended, the following prerequisites must

be fulfilled:

•You should have a general understanding of the use of a personal computer running

Microsoft™ Windows™ in the version provided with your product.

•You should understand the concepts of isothermal titration calorimetry.

•You must read and understand the Safety Instructions as outlined in

MicroCal iTC 200 Operating Instructions .

•The instrument and software must be installed, configured and calibrated as outlined

in MicroCal iTC 200Operating Instructions by Malvern Instruments personnel.

Safety notices

This user documentation contains WARNINGS, CAUTIONS and NOTICES concerning the

safe use of the product with meanings as defined below.

Notes and tips

A Note is used to indicate information that is important for trouble-free and optimal use of the product.

Tip: A tip contains useful information that can improve or optimize your procedures.

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Note:

MicroCal iTC 200Washing Module User Guide 5

About this manual

Purpose of the user manual

This user manual provides instructions needed to run MicroCal iTC200 and to analyze

isothermal titration calorimetry (ITC) data. This user manual is a complement to

MicroCal iTC 200 Operating Instructions.

Typographical conventions

Software items are identified in the text by bold italic text. A colon separates menu levels,

thus File:Open refers to the Open command in the File menu.

Hardware items are identified in the text by bold text (e.g., Power switch).

Text entries that MicroCal iTC software generates or that the user must type are represented

by a monotype typeface (e.g., C:\Origin70\Samples

Regulatory information

For regulatory information regarding MicroCal iTC 200 washing module refer to MicroCal iTC

Operating Instructions or the MicroCal iTC200User Manual

Associated documentation

Introduction

This section lists the user documentation that is delivered with MicroCal iTC200 and related

literature that can be downloaded or ordered from Malvern Instruments.

User documentation

The user documentation for MicroCal iTC 200consists of:

•MicroCal iTC 200Operating Instructions

•MicroCal iTC 200User Manual

•MicroCal iTC 200Washing Module User Manual (this manual)

Related literature

Additional downloadable material can be found at: www.malverninstruments.com/microcal

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200

6 MicroCal iTC 200Washing Module User Guide

Installation Instructions:

MicroCal iTC200 Washing Module with Bottle Adapter

Background:

The bottle adapter allows the MicroCal iTC 200 washing module to be used with full-size bottles.

Prior models of the washing modules used 30 mL vials that required frequent filling.

Kit Contents:

1 washing module with 1 Hub with cable (ASY501700 )

1 Filling Port Adaptor (ASY020506)

1 Cleaning Device (ASY020513)

1 Syringe Needle Cleaning Tube Assembly (ASY020512)

1 Waste Bottle Tube (ASY020555)

1 Drip Tube, Syringe, Wash Module (MSP021321

1 Drip Tube, Cleaning Device,WM (MSP25013)

1 Power Supply, Wall Mount, 12 VDC (PWS020326)

1 005 O-Ring for Cleaning Device & Adapter (ORG0005V-0 10)

2 USB Cable, Short (CBL020330)

1 Waste Bottle Assembly (Gray Cap) (ASY021615)

1 Water Bottle Assembly (Blue Cap) (ASY021396)

1 Buffer Bottle Assembly (White Cap) (ASY021397)

1 Methanol Bottle Assembly (Red Cap) (ASY021398)

1 Filling Port Adapter with Needle (ASY501340)

1 Extra Tubing Set – One set of 5 per pack (KIT020599)

3 Bottle Tubing, External (ASY021608)

1 Replacement Filter –set of 5 per pack (29-0068-42)

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MicroCal iTC 200Washing Module User Guide 7

Part 1: Bottle Preparation

Note: Turn the MicroCal iTC 200 off and disconnect it from power before proceeding.

1. Remove the four bottles from their packaging. Using

the standard tubing, the bottles will need to be

located within about three feet (1m) of the washing

module.

The bottle with the blue top

(ASY021396) will be used for water.

The bottle with the red top

(ASY021398) will be used for methanol.

The bottle with the white top

(ASY021397) will be used for buffer.

The bottle with the grey top

(ASY021615) will be used for waste.

2. The waste bottle assembly includes

two waste lines. Set them aside.

3. Remove the three tygon tubing assemblies

(ASY021608) from the ir packaging and screw them

onto the tops of the red, white and blue bottles.

4. Set the four bottles aside in a safe location near the cell unit.

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8 MicroCal iTC 200Washing Module User Guide

Part 2: Fluid Connections

1. Remove the cleaning device (ASY020513) from

its packaging.

2. Connect the line from the top of the device into

the C3 port on the left side of the washing

module. Turn the nut on the red plumbing

connector until it is finger tight.

3. Connect the line that originates at the side of

the device to the C4 port on the left side of the

washing module. Turn the nut on the red

plumbing connector until it is finger tight.

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MicroCal iTC 200Washing Module User Guide 9

4. Place the cleaning device into the center hole at

the back of the washing module.

5. Two waste lines were set aside in Part 1, Step 2.

Select one of the waste lines based on how far

the waste bottle will be located from the

washing module. Then connect it to the C5 port

on the washing module. Turn the nut on the red

plumbing connector until it is finger tight.

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10 MicroCal iTC 200Washing Module User Guide

6. Place the washing module on top of the cell

unit. When properly positioned, the feet on the

washing module will fit into the depressions on

the top of the cell unit to keep it from sliding off.

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