Foss Soxtec 1047 Manual de usuario

Copyright 2001/ All rights reserved
FOSS TECATOR AB, Box 70, S-26321 Höganäs, Sweden
Tel Int +46 42 361500, Fax +46 42 343150
Soxtec®1047 System
Hydrolyzing Unit
User Manual
1000 3315 / Rev. 2.2
1047011b


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1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden

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1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden

Table of Contents
1 PRECAUTIONS AND PROCEDURES
1.1 Intended use..............................................................................................1
1.2 Safety precautions.................................................................................1
2 INTRODUCTION
2.1 Performance data...................................................................................3
3 PREPARATIONS FOR USE
3.1 Unpacking and checking ....................................................................4
3.2 Installation .................................................................................................5
3.2.1 Installation requirements ............................................................................5
3.2.2 Fuses .................................................................................................................5
3.2.3 Installation instructions................................................................................5
4 OPERATION
4.1 Preliminary preparation.....................................................................6
4.2 Pre-extraction ...........................................................................................7
4.3 Hydrolysis ..................................................................................................8
4.4 Drying............................................................................................................9
4.5 Solvent extraction .................................................................................9
4.6 Calculation................................................................................................10
5 MAINTENANCE
5.1 Change of vacuum valve ................................................................11
5.2 Change of condenser .........................................................................11
5.3 Change of filter seal, upper ..........................................................11
5.4 Change of the lower thimble holder........................................12
5.5 Change of the vacuum tube ..........................................................12
5.6 Change of fuses.....................................................................................12
6 TECHNICAL SPECIFICATIONS
6.1 Safety...........................................................................................................13
6.2 Environmental conditions...............................................................13
6.3 Lifting instructions..............................................................................13
7 Foss Tecator APPLICATION NOTES SYSTEM
8 ACCESSORIES AND SPARE PARTS
8.1 Accessories ...............................................................................................15
8.2 Spare parts ...............................................................................................15
8.3 Manufacturer’s name and address............................................15
9 SAFETY INFORMATION 1047 (GB) ................................17
9 SICHERHEITSINFORMATIONEN 1047(DE) ..............20
9 SIKKERHEDSINFORMATION 1047(DK) .....................24
9 INFORMACION DE SEGURIDAD 1047 (ES)............28
1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden

9 TURVALLISUUSOHJEET 1047 (FIN)................................32
9 INSTRUCTIONS DE SECURITE 1047(FR)....................36
9ËÇØÇ ÌÅÔÑÙÍ ÁÓÖÁËÅÉÁÓ 1047 (GR)......................40
9 ÖRYGGISLEIÐBEININGAR 1047(IS)..............................45
9 INFORMAZIONI DI SICUREZZA 1047(IT).................48
9 VEILIGHEIDSINFORMATIE 1047(NL)...........................52
9 SIKKERHETSINFORMASJON 1047(NO).....................56
9 INFORMAÇÕES DE SEGURANÇA 1047(PT) ...........59
9 SÄKERHETSINFORMATION 1047(SE)..........................63
1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden

The 1047 Hydrolyzing Unit is designed for
laboratory use analysing parameters as
specified in Foss Tecators Application Notes.
Please read these operating instructions
carefully and act accordingly.
For safety reasons people not familiar with
these operating instructions must not use the
instrument.


2INTRODUCTION
Crude Fat is generally defined as sample constituents soluble in
appropriate organic solvents, such as diethyl ether, petroleum
ether or chloroform. The main constituents in Crude Fat are
triglycerols and free fatty acids. In certain Sample types, however,
some of the fat, or lipids, are bound as lipoproteins,
liposaccharides or metal salts. Solvents are not capable of
breaking such bonds, therefore hydrolysis is used to transform
these lipids into extractable forms.
The 1047 Hydrolyzing Unit in combination with Soxtec System
HT enables total fat extractions to be performed in a simple way
in a variety of Sample types.
2.1 Performance data
Sample size 0.5-5 g
Measuring range 0-100% fat
Capacity per batch 6 per unit
Speed of hydrolyzing cycle 20-60 min
1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden
3
STEC004A
Fig. 1 The procedure for fat determination with 1047 Hydrolyzing Unit and 1043 Soxtec Extraction Unit.

3PREPARATIONS FOR USE
3.1 Unpacking and checking
Unpack the 1047 Hydrolyzing Unit and its accessories with care.
Remove all packing material.
Use the parts list, packed together with the instrument and check
that you have received all parts. Use Fig.2 to identify the
different parts. If any parts are missing, contact your Foss Tecator
representative.
1. Hydrolyzing Unit 2. Sample Tube (set of 6)
3. Glass Thimbles (set of 6) 4. Glass Thimble Holder (set of 6)
5. Water Spray Device 6. Beaker
7. Tube Stand 8. Reflector
9. Cleaning rod 10. Glass Thimble adaptor (set of 6)
11. Celite 12. Tube 8/11 L= 2 m
13. Tube 6/11 L= 2 m 14. Spray bottle, red
15. Cotton 16. Glass Thimble seals (set of 6)
17. Water Aspirator Pump 18. Hydrolysis Stand
19. Manual 22. Mains cable
1047 Soxtec System Hydrolyzing Unit, User Manual, Rev. 2.2, Part no 1000 3315, Foss Tecator AB, Sweden
4
1047011A
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