Endress+Hauser Liquistation CSF33 Manual de usuario

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Products Solutions Services

BA00489C/07/EN/15.13

71217984

Valid as of:

Softwareversion 01.04.00

Operating Instructions

Liquistation CSF33

Automatic sampler for liquid media

Calibration

About this manual

This manual describes how to calibrate the distribution arm and the sample volume.

This manual does not include the following:

• Setup/General settings

--> Operating Instructions BA00479C "Commissioning"

• Display/Operation

--> Operating Instructions BA00479C "Commissioning"

•Inputs

--> Operating Instructions BA00487C "Operation & settings"

•Outputs

--> Operating Instructions BA00487C "Operation & settings"

• Sampling programs

--> Operating Instructions BA00487C "Operation & settings"

• Additional functions

--> Operating Instructions BA00487C "Operation & settings"

• Data management

--> Operating Instructions BA00487C "Operation & settings"

•Expert

--> Internal Service Manual

•Diagnostics

--> Operating Instructions BA00488C "Maintenance & diagnostics"

Endress+Hauser

Liquistation CSF33

Table of contents

1 Calibrating the distribution

arm . . . . . . . . . . . . . . . . . . . . . . . . 4

2 Calibrating the sample volume 5

2.1 Vacuum pump . . . . . . . . . . . . . . . . . . . . . . 5

2.2 Peristaltic pump . . . . . . . . . . . . . . . . . . . . . 7

Index. . . . . . . . . . . . . . . . . . . . . . . 8

Calibrating the distribution arm Liquistation CSF33

4Endress+Hauser

1 Calibrating the distribution arm

It is only possible to calibrate the distribution arm in the version with multiple bottles.

The distribution arm must be calibrated if:

• The distribution arm motor has been replaced

• Error message "F236 Distribution arm" appears on the display

1. Select the number of bottles in the "Setup/Basic setup" menu.

2. Proceed as follows to calibrate the distribution arm:

3. Afterwards perform a distribution arm test in the "Diagnostics/Systemtest/Reset/Distribution

arm" menu.

Path: Menu/Calibration active

Function Options Info

Distribution arm

Go to ref. point Action The reference run is started. The reference point is

in the middle at the front.

For versions with distributor plate, the reference

point is at the arrow in the middle of the plate. For

versions with distribution assembly the reference

point is between bottle number 1 and the last one.

With Adjust you can correct the distribution arm if the unit does not move to the reference point correctly. Use

the two arrow keys to correct the position.

Liquistation CSF33 Calibrating the sample volume

Endress+Hauser 5

2 Calibrating the sample volume

2.1 Vacuum pump

The desired sample volume is set by manually adjusting the dosing tube.

a0013896

Fig. 1: Vacuum pump

1Outlethose

2Dosingchamber

3Dosingchambercover

4 Air hose connection

5 Lock for intake hose

6 Thread adapter nut for intake hose

Proceed as follows to calibrate the sample volume:

1. Check the sample volume set under Menu/Setup/General settings/Sampling/Dosing

volume.

2. Release the thread adapter nut on the intake hose (item 6).

3. Turn the intake hose to the "open" position at the hose lock (item 5) and remove the hose

from above.

4. Release the air hose (item 4) and remove the dosing chamber (item 2) from the front along

with the outlet hose (item 1).

5. Open the bayonet lock (item 3) and open the dosing chamber.

1

2

6

3

4

5

Calibrating the sample volume Liquistation CSF33

6Endress+Hauser

1. Release the 2mm Allen screw with the key provided.

2. Set the sample volume by adjusting the dosing tube. Secure the dosing tube with the screw.

Use the white scale (A) to dose without pressure.

Use the blue scale (B) to dose with pressure.

3. Reinstall the parts in reverse order. Make sure that the contacts of the conductivity sensors

are in the correct position.

4. Check that the dosing tube is set correctly by triggering a manual sampling routine.

a0014128

Fig. 2: Vacuum pump

1

2

3

Dosing tube

Allen screw

Air hose connection

1

2

3

Liquistation CSF33 Calibrating the sample volume

Endress+Hauser 7

2.2 Peristaltic pump

In order to calibrate the sample volume, a measurement beaker with a volume of at least

200 ml is required.

Proceed as follows to calibrate:

Path: Menu/Calibration active

Function Options Info

Sample volume

1-point calibration

Distributor position Options

- Front

- Bottle x

- Back

Select the distributor position.

Sample volume 20 to 2000 ml

Factory setting

100 ml

Set the sample volume.

Start sampling Action The progress of the sampling operation is

displayed.

Check whether the sample volume is correct. Use No to enter the sample volume actually taken, e.g. 110 ml.

Use Yes to repeat the sampling.

2-point calibration

Use 2-point calibration for levels that fluctuate greatly.

The second sampling point must be either higher or lower (height difference of at least 1 m).

Distributor position Options

- Front

- Bottle x

- Back

Select the distributor position.

Sample volume 20 to 2000 ml

Factory setting

100 ml

Set the sample volume.

Start 1. sampling Action The progress of the sampling operation is

displayed.

Check whether the sample volume is correct. Use No to enter the sample volume actually taken, e.g. 110 ml.

Use Yes to repeat the sampling.

Start 2. sampling Action The progress of the sampling operation is

displayed.

Check whether the sample volume is correct. Use No to enter the sample volume actually taken, e.g. 110 ml.

Use Yes to repeat the sampling.

Liquistation CSF33

8

Index

C

Calibration

Distribution arm . . . . . . . . . . . . . . . . . . . . . . . 4

Sample volume . . . . . . . . . . . . . . . . . . . . . . . . 5

D

Distribution arm calibration . . . . . . . . . . . . . . . . 4

S

Sample volume calibration . . . . . . . . . . . . . . . . . 5