Distek Evolution 6300 Manual de usuario
Operation
Manual
Evolution
Dissolution Test
System
6100
6300
Evolution Dissolution Test System
Operation Manual
Document # 3861-0001
Distek, Inc.
121 Nort Center Dr. • Nort Brunswick, NJ 08902
P one 732.422.7585 • Fax 732.422.7310
ttp://www.distekinc.com
Notice
This document contains proprietary information. All ri hts are
reserved. No part of this document may be photocopied,
reproduced or translated without the prior written consent of
Distek, Inc.
Distek, Inc.
121 North Center Drive
North Brunswick, NJ 08902-4905
Tel. (732) 422-7585
Fax. (732) 422-7310
Website: http://www.distekinc.com
“Dow Corning” is a registered trademark of Dow Corning Corporation, USA.
CenterC ek, Heig tC ek, RPMC ek, S aftC ek and TempC ek are trademarks of Distek,
Inc.
T e Distek logo is a registered trademark of Distek, Inc.
All ot er company and product names are trademarks or registered trademarks of t eir
respective olders.
Document Revision History
Rev Date Notes
A June 2003 Initial Release
B December 2003 See Distek C ange Notice 0405
C October 2004 Updated for Firmware Rev. 2.13. See Distek C ange Notice
0456.
D June 2005 Updated Appendix A: Spare Parts & Accessories. See Distek
C ange Notice 0508.
E September 2005
Removed Certificate of Compliance from Manual. Certificate
is a separate file on manual CD. See C ange Notice 0516.
Page B-1: Step # 5.3 – c ange “0.3V” to “2.0 V” and “0.5 V”
to “3.0 V”
Page D-2 and D-3 – add note to bottom of page - “Asterisk (*)
in Temperature Profiles denotes out of USP specification”
F May 2007 See Distek C ange Notice 0580. Updated for FW Rev. 2.15.
Operation Manual: Evolution Series
Contents
About this Manual......................................................................... i
Purpose .................................................................................. ii
Audience ................................................................................ ii
Contents................................................................................. ii
Prerequisites............................................................................iii
Documentation .........................................................................iii
Conventions.............................................................................iii
1Introduction ..................................................................... 1-1
Overview .............................................................................. 1-2
Specification.......................................................................... 1-2
P ysical Site Considerations........................................................ 1-4
Environmental Considerations ..................................................... 1-5
Distek & t e WEEE Directive (Waste Electrical & Electronic Equipment) 1-5
Ambient Laboratory Temperatures ............................................. 1-5
Ambient Laboratory Humidity ................................................... 1-6
Air Quality Considerations ....................................................... 1-7
Operation Warnings and Notes..................................................... 1-8
General Instrument Overview .....................................................1-11
2Installation....................................................................... 2-1
Unpacking ............................................................................. 2-2
Leveling t e Evolution System ..................................................... 2-3
Installing t e T ermocirculator (Evolution 6300 Only) ......................... 2-6
Placement and Connections ..................................................... 2-7
Filling t e Water Bat ............................................................ 2-8
Priming t e Pump ................................................................. 2-8
Operation Manual: Evolution Series
Positioning t e Vessels .............................................................2-10
Paddle and Basket Installation ....................................................2-11
Paddle Blade Installation........................................................2-11
Basket Installation ...............................................................2-11
C ecking Paddles, Baskets and S afts for Straig tness.....................2-12
C ecking S aft Centering .......................................................2-12
Paddles and Basket Heig t Adjustment..........................................2-12
Initial Heig t Setting for Paddles and Baskets: ..............................2-13
Quick C ange Heig t Adjustment Knob (Paddles or Baskets)..............2-14
Installing t e Calibration Probe...................................................2-14
Installation C eckout...............................................................2-15
RPM Control .......................................................................2-15
Test Duration .....................................................................2-15
Temperature Control ............................................................2-16
Time and Date ....................................................................2-16
3Operation ........................................................................ 3-1
Control Keypad ....................................................................... 3-4
ESC/DEL Button.................................................................... 3-4
RUN/STOP Button ................................................................. 3-4
Arrow Keys ......................................................................... 3-4
ENTER Button ...................................................................... 3-4
+ Button ............................................................................ 3-5
- Button............................................................................. 3-5
Stir LED ............................................................................. 3-5
Heat LED............................................................................ 3-5
Sleep LED........................................................................... 3-5
produKEY ........................................................................... 3-5
Startup Screens....................................................................... 3-5
System Administration .............................................................. 3-6
System Setup....................................................................... 3-7
Advanced Options .............................................................. 3-8
Unit Address ..................................................................... 3-8
TCS Address (Evolution 6300 Only)........................................... 3-9
Pre eat (Evolution 6300 Only) ................................................ 3-9
Temperature Control (Evolution 6300 Only)............................... 3-10
Beep Mode ...................................................................... 3-10
Heig t Switc Setting ......................................................... 3-10
Printer S aring Configuration (Evolution 6100 Only) ..................... 3-11
About Window.................................................................. 3-12
User Configuration ...............................................................3-12
Login Procedures .............................................................. 3-13
Creating a New Account ...................................................... 3-14
C anging t e Privileges of an Existing Account ........................... 3-15
C anging a Password .......................................................... 3-15
Deleting an Account........................................................... 3-16
Temperature Calibration........................................................3-16
Operation Manual: Evolution Series
Calibrate Using Evolution Calibration Probe............................... 3-18
Calibrate Using TempC ek Digital T ermometer ......................... 3-19
Calibrate Using NIST-Traceable Reference T ermometer ............... 3-19
Calibrate calPROBE Using TempC ek Digital T ermometer ............. 3-20
Calibrate calPROBE Using NIST-Traceable Reference T ermometer... 3-21
Display Screens ......................................................................3-21
Temperature Screen .............................................................3-21
Temperature and RPM Screen ..................................................3-22
Current Met od...................................................................3-23
Report History ....................................................................3-23
Printing a Saved Report .........................................................3-24
Working wit Met ods (Automatic Mode) .......................................3-24
Selecting a Met od to Run ......................................................3-24
Sorting t e Met od List..........................................................3-25
Programming a New Met od....................................................3-25
Running a Simultaneous Drop wit Paddles ..................................3-27
Running a Simultaneous Drop wit Baskets...................................3-28
Running a Staggered Drop wit Paddles ......................................3-28
Running a Staggered Drop wit Baskets.......................................3-28
Open/View an Existing Met od.................................................3-29
Modify a Saved Met od ..........................................................3-30
Deleting a Met od................................................................3-30
Copy a Saved Met od to a New Name.........................................3-30
Printing Met od Parameters....................................................3-31
Working in Manual Mode ...........................................................3-31
Controlling Vessels Individually (Evolution 6100 Only) .....................3-32
Controlling All Vessels ...........................................................3-33
TCS Activation (Evolution 6300 Only) .........................................3-35
Running a Manual Mode Test ...................................................3-35
Using t e produKEY.................................................................3-36
Saving a Met od to t e produKEY..............................................3-36
Viewing Met ods on t e produKEY.............................................3-37
Saving a Met od from t e produKEY to t e Instrument ....................3-37
Running a Met od from t e produKEY ........................................3-37
Deleting Met ods from t e produKEY .........................................3-38
Printing a Met od from t e produKEY.........................................3-38
Using a Premiere 5100 produKEY ..............................................3-38
Using t e calKEY ....................................................................3-38
Storing Calibration Data.........................................................3-39
Restoring Calibration Data ......................................................3-39
Printouts..............................................................................3-40
Serial Port Control ..................................................................3-40
4Maintenance..................................................................... 4-1
General Information ................................................................. 4-2
Emptying t e Water Bat & TCS (Evolution 6300 Only) ........................ 4-3
Removing t e Water Bat (Evolution 6300 Only)................................ 4-4
Operation Manual: Evolution Series
Re-installing t e Water Bat (Evolution 6300 Only) ............................ 4-5
Replacing t e Water Bat and TCS Tubing (Evolution 6300 Only) ............ 4-5
5Troubles ooting................................................................. 5-1
Troubles ooting ...................................................................... 5-2
Error Messages.......................................................................5-15
Warning Messages...................................................................5-17
General Messages ...................................................................5-18
Service................................................................................5-19
Appendix A : Spare Parts and Accessories ...................................... A-1
Appendix B : Pre-Installation Considerations: Electrical Power SupplyB-1
Appendix C : CE Declaration of Conformity .................................... C-1
Appendix D : Sample Printouts from Parallel Printer ......................... D-1
About T is Manual
Operation Manual: Evolution Series
i
About this Manual
About T is Manual includes information about w at is contained in t is manual and
t e conventions used.
Purpose .................................................................................. ii
Audience ................................................................................ ii
Contents................................................................................. ii
Prerequisites............................................................................iii
Documentation .........................................................................iii
Conventions.............................................................................iii
About T is Manual
Operation Manual: Evolution Series
ii
Purpose
T is manual covers t e installation, routine operation, maintenance and repair of
your Evolution Dissolution Test System. It as information regarding t e
commands, menus, indicators and controls. C apter 1 provides an overview of t e
system. C apter 2 covers unpacking, installation, and qualification of t e system.
C apter 3 as operation and programming information. C apters 4 and 5 cover
maintenance and troubles ooting. Please read C apters 1, 2 and 3 before
proceeding.
Audience
T is manual is written for any person responsible for maintaining, operating or
troubles ooting t e Distek Evolution Dissolution Test System.
Contents
T is manual is divided into c apters. T e pages of t e manual are numbered
providing easy navigation to assist in finding information quickly.
T e following list describes t e material covered in eac c apter:
C apter 1 - Introduction Provides a general overview and
warnings about t e instrument.
C apter 2 - Installation Describes ow to unpack and properly
install t e unit.
C apter 3 - Operation Describes t e functionalities of t e
system and ow to run t e unit.
C apter 4 - Maintenance Explains t e steps necessary to
maintain t e unit.
C apter 5 - Troubles ooting Provides a troubles ooting c art and
description of error messages to assist
t e user if a problem arises.
Appendix A – Spare Parts and
Accessories
Provides a table of recommended and
optional spare parts.
Appendix B - Pre-Installation
Considerations: Electrical Power
Supply
Recommendation information
pertaining to electrical power supply.
Appendix C - CE Declaration of
Conformity
CE Declaration of Conformity
certificate.
Appendix D - Certificate of
Compliance
Certificate of Compliance
Appendix E - Sample Printouts from
Parallel Printer
Sample printouts for a parallel printer.
About T is Manual
Operation Manual: Evolution Series
iii
Prerequisites
T is manual assumes t at you understand t e principles of dissolution testing.
Documentation
T is manual contains important information regarding t e safe operation,
maintenance and repair of your Distek Evolution Dissolution Test System.
Conventions
T e following table contains Warnings, Cautions and Notes t at are used
t roug out t e document for your protection. Please read t is section before
using t e Evolution Dissolution Testing System.
“WARNING” statements are used in t is manual to prevent
injury to personnel.
"CAUTION: Risk of Electric Shock" statements are used to
prevent injury w en ig voltage is present.
“CAUTION” statements are used to prevent damage to
equipment.
“NOTES” contain elpful information.
REQUIRED
ACTION
“REQUIRED ACTION” is used w ere necessary to distinguis
t e action needed from Warnings, Cautions and Notes.
Este manual sirve para los siguientes modelos
1
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